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The Indole Acetic Acid Oxidase Of Hygrophorus Conicus., Dilip N. Patel

Masters Theses

"The purpose of this investigation was to determine an assay method for measuring the activity of the indole acetic acid oxidase present in Hygrophorus conicus. This enzyme converts tryptamine or indole acetic acid (IAA) into oxindole acetic acid (OIAA).

An assay method for measuring the activity of the enzyme was developed based on the spectrophotometric measurement of tryptamine, IAA, and OIAA. Several other assay methods were tried. The colorimetric method of Gordon and Weber ^(l4) was found to be useful for a quantitative determination of IAA and was insensitive to OIAA. Paper chromatography proved to be useful as a qualitative …

A New Method For The Evaluation Of Metal Primers., Bhalchandra Dave

Masters Theses

"Corrosion is the destructive attack of metal by chemical or electrochemical reaction with its environment. Rusting is usually the term applied to the corrosion of iron-base alloys with formation of corrosion products consisting largely of hydrous ferric oxides. Non-ferrous metals therefore, corrode but do not rust. ^(l4) More than 40 per cent of the world's production of steel and iron is destroyed by rusting which costs about six billion dollars every year. In 1954 the American Petroleum Industry, Subcommittee on Corrosion, published a preliminary estimate that corrosion was costing 2 the petroleum refining industry between eleven and nineteen cents per …

Forced Convection Heat Transfer Coefficients And Induction Heating, Max Edwin Light

Masters Theses

“The purpose of this study was to design and build an apparatus to experimentally determine the convective heat transfer coefficients for water flowing in a horizontal tube at turbulent flow. Also it was planned to use the apparatus to investigate the spatial dependence of energy deposition by induction heating.

An instrument and measuring techniques were developed that gave reasonable correlations between experimentally determined heat transfer coefficients and values calculated from generally accepted heat transfer relationships developed by other experimenters. Most of the calculated values were within ± 10% of the experimental values for a wide range of flow rates.

It …

The Effects Of Granular Size On The Thermal Conductivity Of Sand, Kanubhai M. Patel

Masters Theses

"The thermal conductivity of granular materials can be determined by the Thomas method. This method was used here to determine the effects of granular size on the thermal conductivity of sand. A river sand was secured and screened. The sand retained between the Tyler Standard Screen Scale, mesh 10 and 14, 14 and 28, 28 and 40, 40 and 48, 48 and 60, and below mesh 60, was used for tests.

The thermal conductivity for the above six samples obtained by the author coincide fairly well with published data.

It is reported in the International Critical Tables that the thermal …

The Effect Of Moisture Content On The Action Of Sea Coal In Molding Sands., Robert J. Endres

Masters Theses

"An assumption was made that an increase in moisture content in the sand would result in an increase in the amount of volatile matter retained in a sand, clay, water, and sea coal mixture which had been subjected to the heat of molten iron. Because of a lack of positive evidence to support this assumption, it was concluded that the volatile matter retained within the sample is independent of the moisture content.

It was also shown that the volatile products do not travel back through the sand, away from the mold-metal interface. Rather, the volatiles escape from the sand and …

The Removal Of Residual Organic Materials From Sewage Plant Effluents Using Continuous Foam Flotation., Ajab S. Malik

Masters Theses

"This investigation was conducted to determine the feasibility of using a continuous foam flotation process for the removal of soluble organic materials from sewage treatment plant effluents. All effluents contained alkyl benzene sulfonates (ABS), derived from synthetic detergents. The studies were conducted on a laboratory scale. The reduction in the chemical oxygen demand was used as a measure of the effectiveness of the removal of the organic materials. In addition, ABS determinations were employed to study the fate of the detergent.

A flotation cell, equipped with the means of controlling the air and liquid flow rates, was used. Air flow …

The Resolution Of Two Known Signals In White Gaussian Noise., Peter Cheng-Fang Wang

Masters Theses

"The problem of resolving two signals F1(t) and F2(t) in white Gaussian noise n(t) is treated here as a problem in statistical decision theory. We assume a situation in which one of two similar signals is present and an observer is asked to make a decision concerning which of the signals is present with a tolerable probability of error. The observer is allowed to use the best system which he can design for this particular purpose. Of course, this observation will be disturbed by noise and therefore, the observer is led to ambiguous selections. It is apparent that the optimum …

Optimum Zero-Memory Nonlinear Filter, Benjamin Shaw-Hu Wang

Masters Theses

“The purpose of this report is to review the basic work described by Zadeh insofar as systems of class N₁ are concerned and to apply his general results to a specific problem in which a non-linear filter is mandatory simply because the linear filter is essentially ineffective. The ineffectiveness stems from the fact that the autocorrelation function of the signal plus the noise has essentially the same variational character as the signal alone. Therefore, the transfer function of the linear filter turns out to be simply a constant. Thus, the output of the linear filter is just an attenuated …

The Imperfect Structure Of Ti-, Zr-, And Hf- Nitrides Containing An Excess Of Nitrogen., Chester A. Faunce

Masters Theses

"Chemical analyses were made on all three nitrides using oxidation, Kjeldahl, dissolution and gas evolution techniques, and the chemical formulae were calculated. They are as follows: Ti_0•931^N, Zr_0•970^N, and Hf_0•792^N.

The lattice constant of all the nitride samples was determined at 25°C. The Ti_0•931^N sample obtained from Union Carbide Company had a lattice parameter of 4.23986± 0.00007A⁰, while the sample from W. Germany, Ti_1.0^N in the as received condition had a lattice parameter of 4.24027 t 0.00003A⁰• A second lattice parameter determination was …

The Anodic Dissolution Of Cadmium In Aqueous Solution, Yun-Chung Sun

Masters Theses

"The increasing importance of prevention of corrosion in industry has stimulated extensive studies on the fundamental behavior of metals in corrosive media.

The basic mechanism of the anodic dissolution of metals such as cadmium, magnesium, and zinc in salt solutions is not completely known. Several mechanisms have been proposed by different investigators, but evidence is still lacking to draw unquestionable conclusions to explain the discrepancies which often arise between coulometric data and weight loss of metal electrodes in certain salt solutions.

The purpose of this investigation was to obtain experimental data for anodic dissolution of cadmium in various electrolytes and …

Sonic Flow Meter., Daniel E. Wilson

Masters Theses

"The purpose of this thesis was to construct a device to measure the velocity of air employing sound waves. The principle of operation of the device is that the time interval required for the sound wave to travel between two points in the duct is a function of the fluid velocity. This time interval was measured both with the air flowing and with the air stationary. An equation was derived such that the mean velocity of the flowing air could be calculated by knowing the two-time intervals.

The mean velocity determined by this device was compared to the mean velocity …

The Design, Construction, And Calibration Of An Angular Accelerameter., Walter Earl Palm

Masters Theses

"The purpose of this work was to design, construct, and calibrate an angular accelerometer for continuous operation. The design uses four symmetrically placed springs connecting a ring and hub. Strain gages are mounted on the springs in a Wheatstone bridge arrangement. When the entire unit is subjected to an angular acceleration, the ring deflects causing an output voltage. This voltage is proportional to the deflection which is shown to be a function of the angular acceleration. The accelerometer was constructed to operate at frequencies up to 120 cps. The calibration was accomplished by using a simple harmonic motion input"-- Abstract, …

Radiation Characteristics Of A U-Slot Antenna., Richard Paul Brueggemann

Masters Theses

"The radiation equations for a simple rectangular slot antenna are derived as a function of the field distribution in the slot. The electric field distribution in the slot is then formulated as a function of the aperture dimensions. The U-shaped slot antenna is described as an extension of the rectangular slot theory and the actual field is measured in the slot for comparison.

The far field equations a.re derived for the U-slot antenna similar to those for the rectangular slot antenna and are evaluated using the formulated distributions in the slot for antennas of two different electrical sizes. The equations …

Generalized Programs For Heat Transfer Analysis., Ceylung Chu

Masters Theses

"This report presents numerical methods for calculating temperature distributions in any physical system in which heat transfer is taking place. The syste.11 may be at either a steadystate condition or a transient condition. The temperature distribution may itself be or primary interest, or it may be used further to calculate the flow or heat or thermal stress.

The system under investigation is divided into a certain number of subdivisions, or so-called "regions". A reference point (node point) will be taken as representative for the region which includes that point. The temperature at the "node point11 is taken to be the …

Compensator Design For Unity Feedback Systems Using An Analytical Method, Chang-Yu Wu

Masters Theses

“In control systems engineering it is frequently necessary to compensate a fixed plant whose transfer function cannot be changed. Usually the characteristics of the resulting system are established in terms of steady-state and transient performance specifications. Generally it is necessary to insert a compensator which insures stability as well as satisfies the specifications.

In this thesis an analytical method is developed to determine the transfer function of the compensator in order to satisfy the following set of specifications. The fixed system is assumed to contain one non-linearity, saturation. The input to the saturable device is constrained in a statistical …

Microscopic Observations On Etched Surfaces Of Zinc Single Crystals And On Anodic Disintegration., Yun Wang

Masters Theses

"The technique used to grow single zinc crystals was based on the Bridgman method. Zinc-gold, zinc-aluminum, and zinc-magnesium alloys were prepared and their single crystals were grown. Four crystallographic planes of the single zinc crystals were used for both chemical and anodic etching. The zinc alloys were etched more easily by acids than the purest (99.999%) zinc. The etching patterns changed for the different crystallographic planes of the single zinc crystals.

The appearance of particles during anodic dissolution of the single zinc crystals depended on time, acid concentration and current density. The partial disintegration of single zinc crystals is promoted …

The Characteristics Of Radial Strain Propagation Induced By Explosive Impact In Jefferson City Dolomite., Choon K. Quan

Masters Theses

"Blasting effects depend largely on peak radial strains propagated in rock media by explosive impact. To improve blasting design and control of secondary effects (e.g., structural fatigue), an equation for peak radial strain propagation induced by explosions was developed as follows: Emax = K e^-αr /r

An instrumental technique was designed to test the validity of the equation in the Jefferson City dolomite. Results showed ii that for 1-lb charges of 60% ammonia-gelatin explosive, peak strains, at any distance r, were reduced in amplitude in accordance with an exponential decay function of the type Emax = 281 e^{-0.026r …}

The Effect Of A Lubricant On Tool-Workpiece Interface., Kenneth Eugene Spencer

Masters Theses

"The purpose of this study was to compare the effects of cutting fluids and the method of application to an orthogonal cutting process.

The cutting operation was performed on a lathe. The fluids use d were compressed air and a solution of emulsifiable oil and water.

The flooding of the area was produced by directing a copious supply of fluid over the cutting a rea. The directed stream was obtained by pumping the fluid through a small hole drilled into the tool holder, immediately above and behind the tool face, which directed the fluid at the tool-chip interface.

The results …

The Effect Of An Induction Field On Transducers., Ratilal S. Patel

Masters Theses

"This report presents the results of an experimental investigation on the effect of an induction field on transducer output. Various types of transducers; strain gages, thermocouples, and thermistors, were used. The changes in the output of these transducers were measured for various induction field conditions.

Measurements must often be made where strong electrical fields are present. Strain gages are used to measure the stresses in electrical machinery. Thermocouples and thermistors used for measuring the temperature of materials undergoing heat treatment with an induction heater are also subjected to an induction field.

The general experimental procedure was the same throughout the …

Anodic Dissolution And Disintegration Of Indium, Thallium, And Indium-Cadmium Solid Solutions And Valency Of The Ions Going Into Solution., Richard Lloyd Martin

Masters Theses

"Indium was found to form only In⁺³ ions when dissolving anodically in aqueous acid solutions. Thallium dissolves anodically in acid solutions giving Tl⁺¹ ions only. The reason why Faraday's law is not being formed is that the anode undergoes partial disintegration producing small metallic particles.

Disintegration of these anodes depends on several factors: the nature and concentration of the corrosive medium, the surface condition of the anode, the current density, and the temperature of the corrosive solution. Disintegration may be due to different mechanisms depending on the nature of the electrolyte" -- Abstract, p. ii

A Study Of Cation Exchange And Soil Properties, Arthur G. Follett

Masters Theses

“The objective of this investigation is to study the effect of clay content and cation exchange capacity on the liquid and plastic limits of a soil system in the natural, flocculated, and dispersed states. Putnam and Clarksville natural soils found extensively in Missouri and a synthetic soil composed of Kaolin clay and Clarksville fine sand and silt were tested.

The results of the investigation indicate that a general relationship exists between the high cation exchange capacity of a soil and the extreme variances of the liquid and plastic limit values for the flocculated and the dispersed states. The cation exchange …

The Toxic Effects And Fate Of Selected Pesticides In Natural Water., Donald Lee Evans

Masters Theses

"The extensive application of synthetic organic pesticides in the United States has created many problems, particularly with respect to fish life. While a number of investigations have been undertaken to determine the toxicity of several pesticides to various species of fish, a great deal of research work is needed before the problem is completely understood.

The individual toxicities of DDT, BHC, 2.,4-D, and Sevin to western golden shiners were determined by means of the bioassay procedure at a t empera t ure Of 16oc. The four chemicals studied were found to be toxic to the test fish with Median Tolerance …

A Study Of Crystallization Of Synthetic Fluor-Glaucophane Compositions, Kartini Tjokroatmodjo

Masters Theses

"The ability to form a stable glass and the crystallization properties of four compositions close to that of glaucophane, Na₂Mg₃Al₂Si₈O₂₂(OH)₂ studied. Three glasses were compared with a fourth glass containing no fluorine. The crystallization products of all four glasses were examined between the temperature range 600 - 1200°C. The crystallization products of the three fluorine containing glasses were similar, consisting of mica below 1000°C and of mica, fluor-glaucophane, enstatite and forsterite above 1000°C. In the fluorine free glass, enstatite was the only crystalline phase present below 1000°C, however, forsterite …

Studies Of An Electrical Method For Generating Ultrasonic Waves, Yung-Yien Huang

Masters Theses

“Ultrasonic waves have proved very valuable in the observation of both the velocity and the absorption coefficient of sound in various media. From the velocity measurements of ultrasonic waves in metals, it is possible to obtain elastic constants, such as the compressibility, and the specific heat. Also, the observed attenuation depends greatly on the type and structure of the material. One of the widely used methods for investigation of the internal losses in solid state physics is the pulse-echo technique. This method is being used almost exclusively in internal friction investigation"--Introduction, page 1.

Estimating Bench Design Parameters For Open-Cut Excavation, Rajni K. Gandhi

Masters Theses

"There are no direct relationships available that provide a basis for bench design of multiple-bench, open-cut earth excavations in competent materials when power shovels are employed. This study was undertaken to determine if mathematical design expressions could be developed when the production rate, material's properties, and equipment operating characteristics were known.

It was found that all bench dimensions were a function of the bench height, which in turn was controlled by the required rate of production. The investigation revealed that suitable relationships could be developed to guide in the control of bank stability, choice of shovel capacity, determination of the …

The Anodic Dissolution And Disintegration Of Gallium And Aluminum And The Initial Valency Of The Ions Entering Aqueous Solutions., Kenneth Anderson Poush

Masters Theses

Gallium dissolved very slowly in dilute acids like HC1, H₂SO₄and HCIO₄. The rate was substantially accelerated if the metal was connected with a platinum electrode in the same solution. From the volume of the hydrogen developed the trivalency of gallium ions going into solution was calculated. This same ionic charge was obtained from coulometric measurements using gallium-amalgam as the anode. The initial ionic charge of aluminum dissolving from an aluminum amalgam anode was evidenced as being plus three by coulometric measurements.

Gallium and aluminum anodes were found to partially disintegrate while the current flowed. …

Properties And Perfection Of Zr-H Solid Solutions At Room Temperature., Dirk Heinrich Wiebe

Masters Theses

"The lattice constants of α. - Zr with 122 ppm H are a₂₅ = 3.23622 ± o. 00005 Å and c₂₅ = 5 .1526 ± 0. 0003 Å. The thermal expansion coefficients of α - Zr are found to be α_a =4.6 x 10^-6(⁰C^-1) and α_C =11,0 x 10^-6(⁰C^-1) in the range between 15 and 55°c.

The solid solubility limit in the Zr - H system at room temperature and independent of the H pressure was determined by the parametric x-ray method to be …

Estimation And Tabulation Of Bias Coefficients For Regression Analysis In Incompletely Specified Linear Models., Harry Kerry Edwards

Masters Theses

"There is often some uncertainty as to the exact number of predictors to include in the specification of the linear model when the theory of regression analysis is applied to specific data. To aid the experimenter in defining the correct number of predictors, a bias function that estimates the deviation of a linear model from the true model has been defined.

The writer has derived an accurate, economical, numerical method for calculating the bias function associated with an incompletely specified linear model and has tabulated bias function coefficients for a reasonable number of doubtful predictors"--Abstract, page ii.

A Parameter Perturbation Procedure For Obtaining A Solution To Systems Of Nonlinear Equations., James Carlton Helm

Masters Theses

"For simultaneous nonlinear equations the convergence of the known functional iterative procedures is dependent upon a good initial approximation to the desired roots. In this paper the restriction on the choice of the initial approximation has been circumvented by dividing each problem into a number of subsidiary problems in accordance with a parameter perturbation procedure. The study presents a discussion of the algorithm and the conditions for convergence. The discussion, also, includes the problems which were solved using the parameter perturbation procedure"--Abstract, p. ii

A Study On Estimating Parameters Restricted By Linear Inequalities, William Lawrence May

Masters Theses

“A comparison of two methods for estimating parameters restricted by linear inequalities in linear statistical models was made.

The first method consisted of finding the least squares estimates of the parameters disregarding the restrictions, and then forcing those parameters that were outside of their allowable ranges to the nearest endpoints of those ranges.

The second method made use of quadratic programming to minimize the same sum of squares that the first method minimized while keeping the parameters inside or at the endpoints of their allowable ranges.

The quadratic programming gave better estimates of the parameters in the sense that the …