Digital Commons Network^™

A Study Of The Solubility Of Gold In Aluminum And The Extent Of The Al₂Au Phase., Kuldip Singh Chopra

Masters Theses

"The lattice constant of pure aluminum (99.998%) at 25° C 0 was determined to be 4.04953 A and the limit of solubility of gold in aluminum at 58O° c was found to be about o.4 weight percent gold. The minimum of the lattice constant was observed at O.75 weight percent gold. No change in the lattice constant with time was found.

The Al₂Au phase has a range from 77.66 to 78.94 weight percent gold with the theoretical composition of Al₂Au nearly in the middle of the phase. The thermal coefficient of expansion, the density and the …

Influence Of Porosity On The Fracture Stresses Of Electrical Porcelain., Edward Anton Snajdr

Masters Theses

"Spherical pores were induced in a typical quartz electrical porcelain body. Three levels of pore size and four levels of concentration were studied. Large strength sample sizes were employed using a three-point loading and diametral loading method. Data for induced quartz particles is also included"--Abstract, p.ii

Mathematical Techniques In The Solution Of Boundary Value Problems., Vincent Paul Pusateri

Masters Theses

"This study was undertaken to present a summary of mathematical techniques as applied to the solution of boundary value problems in partial differential equations.

The techniques that were presented can be considered to be some of the most popular in applied science.

The salient features of the study are that different techniques can present different analytical expressions for a solution to the same boundary value problem, and from the viewpoint of computation and accuracy one solution may prove more desirable than the other.

The study also indicates that in boundary conditions where finite discontinuities exists, a slight perturbation to remove …

The Construction And Evaluation Of A Small Scale Laboratory Fermentor For Batch And Continuous Studies., Robert Murray Logan

Masters Theses

"The purpose or this investigation was to design and construct a suitable apparatus for the aerobic culture or microorganisms to be used for preliminary batch studies and eventually, continuous fermentations.

The general design of the apparatus was patterned after small scale equipment described in the literature. Construction or the apparatus was carried out in the shop of the Department of Chemical Engineering and Chemistry. All of the necessary machining was done by the author.

The aeration-agitation system was evaluated by the use or the sulfite oxidation rate determination. The oxygen transfer rate provided by the apparatus was round to be …

Effect Of Stiffness Ratio On Stresses In A Rigid Frame., James Juh-Ling Tang

Masters Theses

"The elastic center method has been used to analyze several rigid frames with different geometric configurations and with component members of variable cross-sections. The basic approach is to divide the frame into small segments to solve this problem. From this analysis the best frame which is in the range of an economical design may be obtained for a given loading condition"--Abstract, p.2

Compensator Design For Unity Feedback Systems On The Digital Computer., Ping Liang

Masters Theses

"In control systems engineering it is frequently necessary to compensate a fixed plant whose transfer function cannot be changed. Usually the characteristics of the resulting system are established in terms of steady state and transient performance specifications. Generally it is necessary to insert a compensator which permits the system to satisfy the specifications as well as to provide an absolutely stable system.

In this thesis a method is developed to determine the transfer function of the compensator. Each system performance specification can be expressed in a differentiable inequality form composed of the system closed-loop gain, zeros, and poles. First, the …

Linear System Transfer Function Identification, Tuh-Kai Koo

Masters Theses

“An approach using a high speed special purpose digital computer to identify the transfer function of a linear system is presented in this thesis. The data for computation are obtained by measuring the system response and its derivatives periodically with a periodic test signal (impulse) input.

The order of the system is first determined by evaluating the rank of a Hankel matrix. Then, the transfer function is determined by solving two sets of system equations.

Theoretical analysis is emphasized in the study. Two examples are given for the purpose of illustrating the theory

Small Signal Gain Analysis For A Seven Cavity Klystron Amplifier., William E. Hord

Masters Theses

"The problem was to find a suitable method of using the digital computer to calculate the small signal gain characteristics of a seven cavity klystron amplifier. Background material relevant to the problem was reviewed. The differential equations for small signal conditions in a gridless gap klystron were developed. These equations were then solved and put in a matrix form suitable for digital computer analysis. Suggestions for additional development were proposed"--Abstract p. ii

Pattern Calculations On A Loaded Spiral Antenna., Jose Briceno

Masters Theses

"The purpose of this thesis is to calculate and p lot the radiation patterns o f a ferrotron-loaded spiral antenna made of semicircles. In particular, this work is confined to a balanced spiral free to radiate in all directions.

The current distribution used in the evaluation of the vector potential is taken from a synthesized current obtained from experimental information on a ferrotron-loaded spiral antenna at a frequency of operation of 200 MC.

The calculated patterns of the spiral antenna are in general single lobed in a direction perpendicular to the plane of the antenna. The beamwidth varies from 62° …

Infrared Modulation Using The Field-Effect Properties Of Germanium., Lloyd E. Brunkhorst

Masters Theses

"The absorption of infrared radiation, by free carriers in germanium, has been used to amplitude modulate infrared radiation. In the experiment, a space charge layer consisting of free carriers is established at the inner surface of a germanium sample by using the field-effect technique. Infrared radiation of a wavelength to which the germanium is transparent is then Internally reflected from this surface. The infrared radiation passes twice through the space charge layer for each internal reflection. With each pass through the space charge layer, the amplitude of the transmitted infrared is decreased. Amplitude modulation of the transmitted infrared is accomplished …

Application Of Photoelasticity To The Stability Of Slopes In Open-Pit Mines., Aly Hemedah Gomah

Masters Theses

"A study of the stability of wall slopes in open pit mines was performed by preparing photoelastic epoxy-resin models representing open pit mines with various slope angles. The models were loaded centrifugally, using the 'locked-in' stress technique. Due to the relatively large sizes of the models, stress distributions could not be recorded with the photographic equipment available. Therefore, fringes and isoclinics were plotted directly on the models themselves. The fringes were used to calculate the shear stress concentrations at arbitrary points in the model from known stresses at control points in the models. The type of slope failure that was …

Permeation Of Water Vapor Through Linear Polymer Films, Mohammed S. Rifai

Masters Theses

"Film formation from thermoplastic resin solutions Is Influenced by secondary intermolecular forces. Consider what may happen when organic coatings change from a liquid to a solid state. In the liquid state it is logical to consider the linear polymer molecules as agglomerates being dispersed in the volatile component rather than being present In solution. These molecular agglomerates are referred to as micelles. They have various degrees of orientation depending on the extent and the location of dipole forces in both polymer and solvent molecules.

When a coating is applied the solvent starts to evaporate and the micelles are driven closer …

An Electrolytic Polishing And Recrystallization Study Of Zinc And Zinc Alloys., Roy Ashley Smith

Masters Theses

"A Unitron hot stage and polarized light were used to enable direct observation of recrystallization in high purity (99.99 per cent) zinc and high zinc content alloys. Electrolytic polishing was investigated in an attempt to prepare unetched surfaces which would show good structural contrast under polarized light and thus permit structural changes occurring during recrystallization to be observed.

Kinetic data obtained from a sequence of photographs during each recrystallization trial showed typical sigmoidal isothermal reaction curves characteristic of a nucleation and growth process. It was determined that rates of nucleation and grain growth are a maximum over the same time …

Permeability Of Organic Protective Coatings And Relation To Film Thickness, Bipin N. Doshi

Masters Theses

“Special types of coating systems are used to protect industrial products and structures against corrosion. Many millions of dollars are spent each year for these coatings. The ability of protective coatings to reduce or inhibit corrosion depends on a variety of factors such as dry film thickness, resistance to permeation of ions and vapors, temperature, pressure, structure of binder, nature of pigment, electrolytic resistance, and many others.

The initial work done by Larry Inglis on the permeability of coatings and it's relation to thickness of coating films showed that the permeability, as determined by under film corrosion, was independent of …

A Study Of The Relative Electric Resistance Of Commercial Steels And Pure Iron, William Eugene Wistehuff

Masters Theses

"The change in relative electric resistance of five commercial steels, Armco Ingot Iron and Pure Iron were studied over the temperature range of 800°C to 1100°C in an attempt to correlate the phenomena of hot or red shortness with a change in the Electric resistance .

The results from the above resistance measurements were compared with mechanical tests of the same steels to show that at the point at which the iron sulfide liquid forms there is a definite change in the slope of the electric resistance vs temperature curve.

Also studied was a discontinuity in the electric resistance vs …

A Study Of The Haeffner Effect In Mercury, James Nicholson Baysden

Masters Theses

"In 1953, E, Haeffner reported that when he passed a direct electric current through a capillary tube filled with mercury, he obtained a separation in the isotopes of mercury with the heavier isotopes being enriched at the negative terminal and the lighter isotopes at the positive terminal. This effect has since been referred to as the Haeffner Effect, Since the original experiment with mercury, other investigators have observed this effect in many other liquid metal systems.

This investigation of the Haeffner Effect in mercury involves the use of a radioactive isotope of mercury (Hg 203) as a tracer to follow …

Parameters In Ablation Heat Sheilds, Franklin Chang Liang Lin

Masters Theses

"The desired result of this paper is a method of determining temperature distribution and burn off rate in a semi-infinite rod or shield subjected to a large heat flux. The possible methods of determination were investigated, and it was felt that an analytical approach turned out to be the most feasible.

The analytical analysis employed involves the use of the Fourier's general equation for one dimensional heat flow. Transformations from stationary to moving coordinates reduces the problem from unsteady state to steady state boundary conditions. The resulting equations can be applicable to the extent for the heat flow problems involving …

Determining Design Freedom Of Linear Feedback Control Systems, Harley D. Brixey

Masters Theses

“The problem confronted in this thesis is to develop a method or procedure to be used in determining the amount of design freedom that is available in any given linear feedback control system by working with the signal flow-graph representation of the system.

Literature was reviewed that deals with basic signal flow-graph theory and degrees of design freedom. Signal- flow-graph theory that forms a foundation for the development is presented.

The development consists of starting with an essential signal-flow graph of order one. The sensitivity and transmittance functions are written for this essential graph in terms of graph symbols; then …

Interaction Curve For A Beam Column., Mahendra Khushalchand Sanghavi

Masters Theses

"The theoretical interaction curve for a circular section is established. Experimentally the interaction curve f or a beam-column with a varying circular cross section, is established. The effect of stress history is discussed, and the comparisons of different interaction curves are made"--Abstract p.i

An Engineering Evaluation Of Surficial Soils Of Dent County, Missouri, William L. Durham

Masters Theses

“This study is the report of an investigation to: Determine the engineering characteristics of Dent County, Missouri soils using a pedologic soil association map for areal extrapolation of soil test data; and, Evaluate the feasibility of determining the engineering characteristics of all Ozark Region soils by the same method.

During the course of the study, the geology and pedology of the county was investigated and a sampling and testing program formulated. Pedologic soil types in each soil association area were sampled, tested in the laboratory, and the results interpreted.

The results obtained showed that the engineering characteristics of the soil …

A Numerical Approach To A Sturm-Liouville Type Problem With Variable Coefficients And Its Application To Heat Transfer And Temperature Prediction In The Lower Atmosphere., Troyce Don Jones

Masters Theses

No abstract provided.

A New Method Of Making Stainless Steel Powder By Electrochemical Disintegration, Mohammed Maher Saad

Masters Theses

"This paper describes a new method of making austenitic stainless steel (18/8) powder by electrochemical disintegration. The method used an external direct current applied to a heat-treated stainless steel anode, and a platinum cathode in an electrolyte of an aqueous solution of 20% HNO₃ and 1% H₂SO₄ by weight respectively.

Special attention has been paid to the size distribution of sieve and sub-sieve sizes, and the following ranges were found: approximately one-half lies between the limits of 200 and 325 mesh, and one third is finer than 325 mesh, with the remainder about +200 mesh, average …

A Rc Active Delay Time Network., Robert Sun-Wu Han

Masters Theses

"This thesis presents a method for performing an approximate synthesis of a variable delay time network by using RC elements and active analog computer circuits. The delay networks discussed here can provide delay times which range from zero to 96 milliseconds for inputs with frequencies which range between zero 2nd 5 cycles per second.

Basically, the procedure involves approximating the delay time transfer function, e^-jwTd , by the ratio of two polynomials each of which is represented by a finite series of terms. The ratio is then shown to be easily synthesized by RC elements and analog computer circuits. …

Mineralogy, Petrography, And Ceramic Properties Of Lower Cabaniss Underclays In Western Missouri, Anthony C. Tennissen

Doctoral Dissertations

The mineral and chemical components, the petrography, and the ceramic properties of the Weir-Pittsburg, Tebo, and Mineral underclays In Barton, Vernon, St. Clair, sod Henry Counties of western Missouri have bean Investigated by x-ray diffraction, differential thermal, spectrographic, microscopic, and certain ceramic testing techniques. The underclays are composed principally of little, kaolinite, end mixed-layer illite-montmorillonite. Illite is the dominant mineral. The principal non-phyllosilicate minerals are quarts sad pyrite. The under clays are mineralogically similar to the underlying shales and contain clay pallets which also are mineralogically similar to the underclays and shales in which they are found. The clay appears …

An Equilibrium Study Of The System Bi-S-H₂, Don Hie Lee

Masters Theses

"An experimental study has been conducted to determine the equilibrium behavior of the system Bi-S-H₂. The system was studied by equilibrating H₂-H₂S gas mixtures with Bi(l)- Bi₂S₃(s) two-phase mixtures at temperatures of 500°, 600°, 700° and 750°C in a circulating type equilibrium apparatus. The equilibrium gas mixtures were analyzed by a Fisher Gas Partitioner with a reproducibility of approximately 0.06 %.

A linear free energy equation has been derived from the results with an average deviation of ± 1 Kcal. This deviation is well within the accepted experimental accuracy for …

A Simplified Method Of Estimating Drilling And Blasting Costs Of A Highway Through-Cut Excavation In Rock, Donald J. Roberts

Masters Theses

"The development of cost estimating methods has been the most neglected phase of highway engineering. Overlooked in particular has been the development of an easily understood and easily applied method of estimating the costs of the drilling and blasting operations involved in a highway through-cut excavation in rock.

This investigation developed such a method by adapting and applying recent developments in the blasting planning field. The study was limited to small diameter blastholes and excavations in lifts of less than thirty feet. Normal efficient construction practices were presumed.

It was found from the investigation that the blast geometry and, subsequently, …

Separation Of Radioactive Fission Products By Electrodialysis Using Aminopolycarboxylic Acids., Harry C. Hershey

Masters Theses

"The development of nuclear fission reactors to convert nuclear energy into electrical energy for use in industry, public utilities, military applications, and space exploration has resulted in ever increasing quantities of radioactive waste solutions. Significant reductions in nuclear fuel costs will be obtained when economical processes have been developed for recovery and purification of valuable fission products which are contained in radioactive waste solutions and are in demand for many research applications.

The United States Atomic Energy Commission has supported exhaustive studies to recover fission products by processes involving the more common unit operations such as extraction, distillation, crystallization, and …

The Measurement Of The Life-Time Of The 62P3/2 State Of Thallium, Danny Hale Sokolowski

Masters Theses

The measurement of the lifetime of the metastable 6²P_3/2 state of thallium is discussed. Time-sampling equipment techniques and instantaneous methods of display on an oscilloscope for measuring the lifetime are explained. The lifetime is measured as a function of mercury vapor pressure. The decay of the 5350 A thallium line is also measured to give an indication of the effect of the imprisonment of the 3776 A resonance line. This decay of the 5350 A line is also in a mercury atmosphere"--Abstract, page ii.

Spin Relaxation Of Optically Pumped Rubidium., Kenneth Brian Steinbruegge

Masters Theses

"This Thesis is intended to be a self-contained guide to the theory and experimental procedures of optical pumping in one of its most usual applications. A particular study is made of optical pumping of rubidium vapor and results are given stating the most efficient temperature range in which to produce large populations of optically oriented rubidium atoms. The thermal relaxation time for optically orientated rubidium for a particular system is given and the effect of trapped resonance radiation is considered in the interpretation of the experimentally obtained curves"--Abstract, p. ii

Analysis Of Problems In The Performance Of A Natural Gas Storage Reservoir., Gerald Eugene Henderson

Masters Theses

"A digital computer technique is presented for predicting two parameters of underground natural gas storage reservoir performance: (1) the prediction of reservoir pressures and volumes, and (2) the prediction of optimum flow rate and pressure drawdown for a single well in accordance with the theory of water coning.

The outlined procedure for predicting gas storage reservoir pressures and volumes was not effective for the field studies, although certain conclusions have been drawn which should be beneficial in further studies.

The procedure for predicting optimum gas flow rate and pressure drawdown from a well without production of bottom water involved first …