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Effects Of Strong Surface Energy Anisotropy On Stationary And Migrating Grain-Boundary Grooves, Donghong Min Jan 2005

Effects Of Strong Surface Energy Anisotropy On Stationary And Migrating Grain-Boundary Grooves, Donghong Min

LSU Doctoral Dissertations

Grain-boundary migration controls grain growth and is important in materials processing and synthesis. When a grain boundary ends at a free surface, a groove will develop at the tip to reduce the combined surface and grain-boundary energies. This groove may hinder the grain boundary movement and its effect needs to be understood. Previous studies have solved the groove profile for stationary or migrating grain boundaries by assuming small groove slopes with isotropic surface free energy. This work extends the analysis to finite slopes with isotropic or anisotropic surface free energy.
We first study migrating grain-boundary grooves with isotropic surface energy …

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Teacher Beliefs And Practices Survey: Operationalizing The 1997 Naeyc Guidelines, Kyung-Ran Kim Jan 2005

Teacher Beliefs And Practices Survey: Operationalizing The 1997 Naeyc Guidelines, Kyung-Ran Kim

LSU Doctoral Dissertations

This study examined the psychometric properties of a revised measurement, the Teacher Beliefs and Practices Survey, devised for teachers of 3- to 5-year-old children. The measure was designed to reflect the concepts of DAP (developmentally appropriate practices) as presented in the revised 1997 NAEYC guidelines and consisted of 2 scales. Three hundred seventy five surveys completed by public kindergarten teachers in Southeast Louisiana were utilized in the study. Reliability was examined using internal consistency method. Cronbach¡¯s ¥á was .858 for the Beliefs Scale and .787 for the Instructional Activities Scale. Validity of the measure was examined in its content, criterion, …

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Wavelet Sets With And Without Groups And Multiresolution Analysis, Mihaela Dobrescu Jan 2005

Wavelet Sets With And Without Groups And Multiresolution Analysis, Mihaela Dobrescu

LSU Doctoral Dissertations

In this dissertation we study a special kind of wavelets, the so-called minimally supported frequency wavelets and the associated wavelet sets. Most of the examples of wavelet sets are for dilation sets which are groups. In this work we construct wavelet sets for which the dilation set, D, is of the form D=MN, where the product is direct, and so D is not necessarily group. In the second part of this dissertation we construct multiwavelets associated with MRA's and we generalize the rotations in the dilation sets to Coxeter groups.

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Medical Image Enhancement, Alina Monica Trifas Jan 2005

Medical Image Enhancement, Alina Monica Trifas

LSU Doctoral Dissertations

Each image acquired from a medical imaging system is often part of a two-dimensional (2-D) image set whose total presents a three-dimensional (3-D) object for diagnosis. Unfortunately, sometimes these images are of poor quality. These distortions cause an inadequate object-of-interest presentation, which can result in inaccurate image analysis. Blurring is considered a serious problem. Therefore, “deblurring” an image to obtain better quality is an important issue in medical image processing. In our research, the image is initially decomposed. Contrast improvement is achieved by modifying the coefficients obtained from the decomposed image. Small coefficient values represent subtle details and are amplified …

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Enantioselective Syntheses And Chemical Investigations Of Plant-Derived Bioactive Volatile Compounds, Anne Marie Sauer Jan 2005

Enantioselective Syntheses And Chemical Investigations Of Plant-Derived Bioactive Volatile Compounds, Anne Marie Sauer

LSU Doctoral Dissertations

Research, inspired by nature, provides ample opportunity for discovery, ingenuity, and creative endeavor. For these reasons, the work and accomplishments presented herein focus on the total syntheses and related investigations of a variety of natural product derivatives, specifically (+)-nootkatone and jasmone. While the former consists of several independent projects: (a) an enantioselective synthetic route to (+)-nootkatone and derivatives, (b) examination of the valencane ring system, (c) determination of the absolute configuration of (+)-nootkatone, and (d) rearrangements of various sesquiterpenoid derivatives; the latter focuses on the construction ofƒndelta, epsilon-unsaturated carbonyl compounds, hetero Pauson-Khand substrates, via [3,3]-sigmatropic rearrangements.

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Radiative Transfer Modeling Of Thermal Infrared Emissivity Spectra: Applications To Martian Regolith Observations, Karly Mariah Pitman Jan 2005

Radiative Transfer Modeling Of Thermal Infrared Emissivity Spectra: Applications To Martian Regolith Observations, Karly Mariah Pitman

LSU Doctoral Dissertations

Satellite and rover remote sensing of planetary regolith surfaces, in the form of thermal infrared emissivity spectra taken at nadir and off-nadir angles of emergence from the surface, requires use of theoretical models for interpretation of constituent grain physical properties. However, such models have remained in stasis in recent years, with nearly a ten-year gap in significant advances. To date, no radiative transfer model (semiempirical, exact, or hybrid solution) has been able to adequately predict the nadir emissivity behavior of simple mineral assemblages. Few measurements have been attempted in the laboratory or field regarding directional emissivity effects of planetary regoliths; …

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Virtual Strings For Closed Curves With Multiple Components And Filamentations For Virtual Links, William Schellhorn Jan 2005

Virtual Strings For Closed Curves With Multiple Components And Filamentations For Virtual Links, William Schellhorn

LSU Doctoral Dissertations

The theory of filaments on oriented chord diagrams can be used to detect some non-classical virtual knots. We extend existing filament techniques to virtual links with more than one component and give examples of virtual links that these techniques can detect as non-classical. Given a signed Gauss word underlying an oriented chord diagram, we describe how to construct a finite sequence of integers that encodes all of the filament information for the diagram. We also introduce a square array of integers called a MIN-square that summarizes the filament information about all of the signed Gauss words having a given Gauss …

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Use Of Orthogonal Arrays, Quasi-Monte Carlo Sampling And Kriging Response Models For Reservoir Simulation With Many Varying Factors, Subhash Kalla Jan 2005

Use Of Orthogonal Arrays, Quasi-Monte Carlo Sampling And Kriging Response Models For Reservoir Simulation With Many Varying Factors, Subhash Kalla

LSU Master's Theses

Asset development teams may adjust simulation model parameters using experimental design to reveal which factors have the greatest impact on the reservoir performance. Response surfaces and experimental design make sensitivity analysis less expensive and more accurate, helping to optimize recovery under geological and economical uncertainties. In this thesis, experimental designs including orthogonal arrays, factorial designs, Latin hypercubes and Hammersley sequences are compared and analyzed. These methods are demonstrated for a gas well with water coning problem to illustrate the efficiency of orthogonal arrays. Eleven geologic factors are varied while optimizing three engineering factors (total of fourteen factors). The objective is …

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A Slope-Dependent Disjoining Pressure For Lennard-Jones Liquid Films, Taeil Yi Jan 2005

A Slope-Dependent Disjoining Pressure For Lennard-Jones Liquid Films, Taeil Yi

LSU Master's Theses

A molecule in a bulk liquid is subject to intermolecular forces. A molecule in a thin liquid film may experience additional intermolecular forces, if the thin film thickness h is less than roughly 100 nm. The additional forces arise from the molecule's proximity to different materials or phases sandwiching the thin film. The effect of these intermolecular forces at the continuum level is captured by disjoining pressure &Pi. Since dominates at small film thickness, it determines the stability and wettability of thin films. To leading order, Π = Π (h) because thin films are generally uniform. This form, however, can …

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Effect Of Estradiol-17b On The Gonadal Developemnt Of Diploid And Triploid Female Eastern Oysters, Roberto Quintana Jan 2005

Effect Of Estradiol-17b On The Gonadal Developemnt Of Diploid And Triploid Female Eastern Oysters, Roberto Quintana

LSU Master's Theses

Declines in annual oyster landings and problems associated with seasonal reduction of oyster meat yields have increased interest for development of techniques to produce oysters with enhanced growth characteristics. Research interest has been focused on developing improved lines by induction of polyploidy. The goal of the present study was to evaluate the enhancement of gonadal development of triploid oysters, by the use of the hormone estradiol 17-â (E2) to produce viable eggs for the development of tetraploid broodstocks. Previous studies with the Pacific oyster, Crassostrea gigas, have shown: (1) the need to use the larger eggs of triploid females to …

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Winter Bird Use Of The Chinese Tallow Tree In Louisiana, Michael John Baldwin Jan 2005

Winter Bird Use Of The Chinese Tallow Tree In Louisiana, Michael John Baldwin

LSU Master's Theses

Chinese tallow (Triadica sebifera) is a non-native invasive tree that is of particular concern in the Southeastern United States. It has become naturalized in a variety of habitats and can be found in monospecific stands. The use of tallow woodlands by overwintering birds is poorly documented. I compared use of tallow woodlands to use of bottomland hardwood forests by birds in the Mermentau River Basin, Louisiana. Species richness and evenness were greater in the bottomland hardwood sites. Three species were more abundant in tallow woodlands, six species were more common in bottomland hardwoods, and six species exhibited no difference between …

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Zeta Functions Of Finite Graphs, Debra Czarneski Jan 2005

Zeta Functions Of Finite Graphs, Debra Czarneski

LSU Doctoral Dissertations

Ihara introduced the zeta function of a finite graph in 1966 in the context of p-adic matrix groups. The idea was generalized to all finite graphs in 1989 by Hashimoto. We will introduce the zeta function from both perspectives and show the equivalence of both forms. We will discuss several properties of finite graphs that are determined by the zeta function and show by counterexample several properties of finite graphs that are not determined by the zeta function. We will also discuss the relationship between the zeta function of a finite graph and the spectrum of a finite graph.

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The Genetics Of Speciation By Reinforcement, Daniel Ortiz-Barrientos Jan 2005

The Genetics Of Speciation By Reinforcement, Daniel Ortiz-Barrientos

LSU Doctoral Dissertations

Reinforcement occurs when natural selection strengthens behavioral discrimination to prevent costly interpopulation matings, such as when matings produce sterile hybrids. This evolutionary process can complete speciation, thereby providing a direct link between Darwin’s theory of natural selection and the origin of new species. My dissertation presents the first study on the genetics of reinforcement. This study is framed in a conceptual body that explains how genomic architecture, selection and recombination, interact to facilitate divergence in the presence of gene flow. In addition, in my dissertation I produced a dense recombination map for D. pseudoobscura, which together with the genome sequence …

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Aspects Of The Life History, Ecophysiology, Bioenergetics, And Population Dynamics Of The Cownose Ray, Rhinoptera Bonasus, In The Northern Gulf Of Mexico, Julie Ann Neer Jan 2005

Aspects Of The Life History, Ecophysiology, Bioenergetics, And Population Dynamics Of The Cownose Ray, Rhinoptera Bonasus, In The Northern Gulf Of Mexico, Julie Ann Neer

LSU Doctoral Dissertations

The cownose ray, Rhinoptera bonasus, is an elasmobranch commonly observed throughout the Gulf of Mexico. Cownose rays appear to be sensitive to water temperature. I performed laboratory experiments and collected field data to obtain basic life history information, and used the information to configure an individual-based bioenergetics model. The bioenergetics model was coupled to a matrix projection model, and the coupled models were used to predict how warmer and cooler water temperatures, compared to current conditions, would affect the growth and population dynamics of the cownose rays. The life history study determined weight at age, maturity by weight, and fecundity …

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A Case Study Inquiry Into The Relative Impact Of Balanced Reading Instruction On Hispanic Students In A Highly Culturally Diverse Elementary School, Rita Ramirez Jan 2005

A Case Study Inquiry Into The Relative Impact Of Balanced Reading Instruction On Hispanic Students In A Highly Culturally Diverse Elementary School, Rita Ramirez

LSU Doctoral Dissertations

This research explores the relative impact of Balanced Reading instruction upon Hispanic students in a highly culturally diverse elementary school. This case study inquiry focuses on Hispanic students learning to read in English in kindergarten, first and third grade, how these Hispanic students are affected by the classroom setting within the context of the Balanced Reading instructional framework of each respective grade, and what are the similarities and differences in the learning methodologies and strategies that impact the learning curve of these Hispanic students. The researcher collects qualitative data to determine the methods and strategies found to be most effective …

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The Stable Isotope Stratigraphy And Paleosols Of North America's Most Southern Exposure Of Late Paleocene/Early Eocene Fossiliferous Continental Deposits: Documenting The Initial Eocene Thermal Maximum In Big Bend National Park, Texas, Paul David White Jan 2005

The Stable Isotope Stratigraphy And Paleosols Of North America's Most Southern Exposure Of Late Paleocene/Early Eocene Fossiliferous Continental Deposits: Documenting The Initial Eocene Thermal Maximum In Big Bend National Park, Texas, Paul David White

LSU Doctoral Dissertations

A chemostratigraphic section across the Paleocene/Eocene boundary, using the stable isotopes of carbon and oxygen, has been developed for North America's most southern exposure of early Paleogene continental deposits in which the boundary is constrained by fossil mammals. A negative carbon excursion has been identified within C24r. The range in d13C values is from -8.1 to -13.2‰. Until the development of the chemostratigraphic section it was uncertain if the earliest Eocene was recorded in Big Bend. An early Wasatchian (Wa1) fossil site occurs stratigraphically higher than the carbon excursion and has yielded the stratigraphically lowest Hyracotherium in the …

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Synthesis, Characterization And Application Of Polymeric Surfactants In Micellar Electrokinetic Chromatography: Use Of Ionic Liquids As Modifiers, Simon M. Mwongela Jan 2005

Synthesis, Characterization And Application Of Polymeric Surfactants In Micellar Electrokinetic Chromatography: Use Of Ionic Liquids As Modifiers, Simon M. Mwongela

LSU Doctoral Dissertations

The goal of the research presented in this dissertation is to synthesize, characterize, and apply a novel chiral amino acid-based surfactant and achiral sulfate-based surfactants for the effective separations of chiral and achiral compounds in micellar electrokinetic chromatography (MEKC). The first part of this research involves novel synthesis, characterization, and application of polysodium oleyl-L-leucyl-valinate (poly-L-SOLV) for the separation of chiral compounds in MEKC. Surface tensiometry, proton nuclear magnetic resonance, infrared spectroscopy, densitometry and analytical ultracentrifugation were used as the characterization techniques. Optimal MEKC separating conditions were established by varying surfactant concentration, buffer concentration and pH, applied voltage, and capillary temperature. …

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Dynamical Systems With Time Delay, Norma Ortiz Jan 2005

Dynamical Systems With Time Delay, Norma Ortiz

LSU Doctoral Dissertations

In this dissertation, we study necessary conditions and weak invariance properties of dynamical systems with time delay. A number of results have been obtained recently that refine necessary conditions of optimal solutions for nonsmooth dynamical systems without time delay. In this dissertation, we examine the extension of some of these results to problems with time delay. In particular, we study the generalized problem of Bolza with the addition of delay in the state and velocity variables and refer to this problem as the Neutral Problem of Bolza. We consider the relationship between the generalized problem of Bolza with time delay …

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Power And Memory Optimization Techniques In Embedded Systems Design, Atef Khalil Allam Jan 2005

Power And Memory Optimization Techniques In Embedded Systems Design, Atef Khalil Allam

LSU Doctoral Dissertations

Embedded systems incur tight constraints on power consumption and memory (which impacts size) in addition to other constraints such as weight and cost. This dissertation addresses two key factors in embedded system design, namely minimization of power consumption and memory requirement. The first part of this dissertation considers the problem of optimizing power consumption (peak power as well as average power) in high-level synthesis (HLS). The second part deals with memory usage optimization mainly targeting a restricted class of computations expressed as loops accessing large data arrays that arises in scientific computing such as the coupled cluster and configuration interaction …

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Ecotoxicology Of Metal-Hydrocarbon Mixtures In Benthic Invertebrates, Kurt A. Gust Jan 2005

Ecotoxicology Of Metal-Hydrocarbon Mixtures In Benthic Invertebrates, Kurt A. Gust

LSU Doctoral Dissertations

Metal-hydrocarbon mixtures are becoming increasingly prevalent in natural environments due to expanding industrial activity and urbanization. The ecotoxicology of metal-hydrocarbon mixtures in benthic environments is of particular concern because both classes of contaminants partition to sediments and can thereby exert toxic effects in benthic organisms. Mixtures of dissimilar chemicals (including metals and hydrocarbons) are broadly hypothesized to elicit independent toxic effects however; this hypothesis has little supporting data. The purpose of this dissertation was to test this hypothesis for metal-hydrocarbon mixtures using environmentally relevant exposures and to determine mechanisms for observed interactive effects. Sediment and water-only bioassays were conducted employing …

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Broadcast In Sparse Conversion Optical Networks Using Fewest Converters, Tong Yi Jan 2005

Broadcast In Sparse Conversion Optical Networks Using Fewest Converters, Tong Yi

LSU Doctoral Dissertations

Wavelengths and converters are shared by communication requests in optical networks. When a message goes through a node without a converter, the outgoing wavelength must be the same as the incoming one. This constraint can be removed if the node uses a converter. Hence, the usage of converters increases the utilization of wavelengths and allows more communication requests to succeed. Since converters are expensive, we consider sparse conversion networks, where only some specified nodes have converters. Moreover, since the usage of converters induces delays, we should minimize the use of available converters. The Converters Usage Problem (CUP) is to use …

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Dragos Tanasescu's Treaties Of Pianistic Technique, Lucian B. Zidaru Jan 2005

Dragos Tanasescu's Treaties Of Pianistic Technique, Lucian B. Zidaru

LSU Doctoral Dissertations

This study examines Dragos Tanasescu's fingering system and technical exercises presented in Treatise of Pianistic Technique. The Treatise contains four books, each one dedicated to a segment of technical problems. Tanasescu's main contribution to the piano technique is the applications of math permutation formulas to create all possible arrangements of fingering patterns. His treatise continues previous technical approaches of A. Kullak, F. Liszt, J. Pischna and E. Dohnanyi. Earlier methods organize the technical material by one principle: fingerings. The purpose of this study is to illustrate the characteristics of Tanasescu's fingering system presented in Treatise of Pianistic Technique, and provide …

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Separation And In Situ Catalytic Testing Of A Dirhodium Tetraphosphine Catalyst, Bobby Lloyd Barker Jan 2005

Separation And In Situ Catalytic Testing Of A Dirhodium Tetraphosphine Catalyst, Bobby Lloyd Barker

LSU Doctoral Dissertations

Attempts to study the asymmetric hydroformylation abilities of [rac-Rh2(nbd)2(et,ph-P4)](BF4)2 were made through the separation of the enantiomers of et,ph-P4 using a chiral HPLC column. Efforts were also made to optimize the NiCl2 separation chemistry for the methyl analogue of et,ph-P4 for use in asymmetric hydroformylation. A study of hydroformylation of olefins using [rac-Rh2(nbd)2(et,ph-P4)](BF4)2 in ionic liquids was also performed, leading directly to the important (and unexpected) effect of increased hydrogen pressure on [rac-Rh2(nbd)2(et,ph-P4)](BF4)2 in the acetone/water system to …

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Synthetic Development And Application Of Compounds With Biological Relevance, Jeffery Caleb Clark Jan 2005

Synthetic Development And Application Of Compounds With Biological Relevance, Jeffery Caleb Clark

LSU Doctoral Dissertations

Nature has provided a vast number of compounds that have medicinal application. The use of these compounds provided by nature however, is limited by the amount of a specific compound that nature provides. The synthesis of these molecules and their derivatives provides an even greater number of compounds for biological screening. Various pyrroles, the heterocyclic building blocks of porphyrins, can be prepared synthetically over several steps. The implementation of carboranes on pyrrole rings intrinsically provides substrates that can be converted into porphyrins bearing carborane substituents. The condensation of these carboranylpyrroles with carboranylaldehydes provides carboranylporphyrins bearing a higher order of carborane …

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Capillary And Microchip Gel Electrophoresis Using Multiplexed Fluorescence Detection With Both Time-Resolved And Spectral-Discrimination Capabilities: Applications In Dna Sequencing Using Near-Infrared Fluorescence, Li Zhu Jan 2005

Capillary And Microchip Gel Electrophoresis Using Multiplexed Fluorescence Detection With Both Time-Resolved And Spectral-Discrimination Capabilities: Applications In Dna Sequencing Using Near-Infrared Fluorescence, Li Zhu

LSU Doctoral Dissertations

Increasing the information content obtainable from a single assay and system miniaturization has continued to be important research areas in analytical chemistry. The research presented in this dissertation involves the development of a two-color, time-resolved fluorescence microscope for the acquisition of both steady-state and time-resolved data during capillary and microchip electrophoresis. The utility of this hybrid fluorescence detector has been demonstrated by applying it to DNA sequencing applications. Coupling color discrimination with time-resolved fluorescence offers increased multiplexing capabilities because the lifetime data adds another layer of information. An optical fiber-based fluorescence microscope was constructed, which utilized fluorescence in near-IR region, …

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The Effectiveness Of Student Support Services At A Research Extensive University In The South, Eric Lyle Penalber Jan 2005

The Effectiveness Of Student Support Services At A Research Extensive University In The South, Eric Lyle Penalber

LSU Doctoral Dissertations

The primary purpose of this study was to determine the influence of level of participation in services provided by the Student Support Services (SSS) Program on the grade point average, retention, and the six-year graduation rate of first-time entering freshmen who also entered the SSS program at a research extensive university in the South. Participants in the study were one hundred, fifty-two (152) SSS students who entered this university in the fall of 1996 and fall of 1997. Tinto’s (1987) longitudinal model of institutional departure was used as the conceptual framework for this study. Services provided by the SSS program …

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Physically Based Multiscale-Viscoplastic Model For Metals And Steel Alloys: Theory And Computation, Farid H. Abed Jan 2005

Physically Based Multiscale-Viscoplastic Model For Metals And Steel Alloys: Theory And Computation, Farid H. Abed

LSU Doctoral Dissertations

The main requirement of large deformation problems such as high-speed machining, impact, and various primarily metal forming, is to develop constitutive relations which are widely applicable and capable of accounting for complex paths of deformation. Achieving such desirable goals for material like metals and steel alloys involves a comprehensive study of their microstructures and experimental observations under different loading conditions. In general, metal structures display a strong rate- and temperature-dependence when deformed non-uniformly into the inelastic range. This effect has important implications for an increasing number of applications in structural and engineering mechanics. The mechanical behavior of these applications cannot …

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Automatic Segmentation Of Magnetic Resonance Images Of The Brain, Kirk V. N. Spence Jan 2005

Automatic Segmentation Of Magnetic Resonance Images Of The Brain, Kirk V. N. Spence

LSU Doctoral Dissertations

Magnetic resonance imaging (MRI) is a technique used primarily in medical settings to produce high quality images of the human body’s internal anatomy. Each image is of a thin slice through the body, with the typical distance between slices being a few millimeters. Brain segmentation is the delineation of one or more anatomical structures within images of the brain. It promotes greater understanding of spatial relationships to aid in such tasks as surgical planning and clinical diagnoses, particularly when the segmented outlines from each image slice are displayed together as a surface in three-dimensions. A review of the literature indicates …

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Synthesis Of Symmetric And Asymmetric Water-Soluble Porphyrin Derivatives, Caroline Owendi Ongayi Jan 2005

Synthesis Of Symmetric And Asymmetric Water-Soluble Porphyrin Derivatives, Caroline Owendi Ongayi

LSU Doctoral Dissertations

Novel symmetric and asymmetric water-soluble tetrabenzoporphyrin are synthesized in relatively good yields. These compounds are synthesized by the condensation of butanopyrrole with several aldehydes that contain masked water solubilizing groups followed by metal insertion, oxidation and demetallation and deprotection of the masked solubilizing groups. The biological evaluation (in vitro and in vivo) studies are described in addition to the photophysical evaluations of the corresponding compounds. A novel versatile route to the syntheses of novel free-bases and metallo-benzoylbiliverdin is discussed. The treatment of metal free-dodecasubstituted porphyrin with sodium nitrite and trifluoroacetic acid at room temperature in the presence of oxygen affords …

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Global Asymptotic Controllability Implies Input-To-State Stabilization, Michael Malisoff, Ludovic Rifford, Eduardo Sontag Dec 2004

Global Asymptotic Controllability Implies Input-To-State Stabilization, Michael Malisoff, Ludovic Rifford, Eduardo Sontag

Faculty Publications

The main problem addressed in this paper is the design of feedbacks for globally asymptotically controllable (GAC) control affine systems that render the closed-loop systems input-to-state stable (ISS) with respect to actuator errors. Extensions for fully nonlinear GAC systems with actuator errors are also discussed. Our controllers have the property that they tolerate small observation noise as well.

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