Open Access. Powered by Scholars. Published by Universities.®

Social and Behavioral Sciences Commons

Open Access. Powered by Scholars. Published by Universities.®

University of Wollongong

Faculty of Engineering and Information Sciences - Papers: Part A

Series

Synthesis

Articles 1 - 18 of 18

Full-Text Articles in Social and Behavioral Sciences

Ambient Controlled Synthesis Of Advanced Core-Shell Plasmonic Ag@Zno Photocatalysts, Jinyan Xiong, Qiao Sun, Jun Chen, Zhen Li, S X. Dou Jan 2016

Ambient Controlled Synthesis Of Advanced Core-Shell Plasmonic Ag@Zno Photocatalysts, Jinyan Xiong, Qiao Sun, Jun Chen, Zhen Li, S X. Dou

Faculty of Engineering and Information Sciences - Papers: Part A

Plasmonic Ag@ZnO core-shell hybrids, including hetero-nanowires and hetero-nanoparticles, have been synthesized at room temperature for application in photocatalysis. The morphology, size, crystal structure, and composition of the products were investigated by X-ray diffraction, scanning and transmission electron microscopy, X-ray photoelectron spectroscopy, and ultraviolet-visible spectroscopy. It was found the concentration of Zn(NO3)2·6H2O and the amount of water play crucial roles in the formation of Ag@ZnO core-shell hybrids. The resultant Ag@ZnO core-shell hybrids exhibit much higher photocatalytic activity and stability towards degradation of organic contaminants than pure ZnO nanocrystals under solar light irradiation. The one-dimensional (1D) core-shell hetero-nanowires prepared under optimal conditions …


Reproducing Personal Sound Zones Using A Hybrid Synthesis Of Dynamic And Parametric Loudspeakers, Jacob Donley, Christian H. Ritz, Bastiaan (Willem) Kleijn Jan 2016

Reproducing Personal Sound Zones Using A Hybrid Synthesis Of Dynamic And Parametric Loudspeakers, Jacob Donley, Christian H. Ritz, Bastiaan (Willem) Kleijn

Faculty of Engineering and Information Sciences - Papers: Part A

This paper proposes a hybrid approach to personal sound zones utilising multizone soundfield reproduction techniques and parametric loudspeakers. Crossover filters are designed, to switch between reproduction methods, through analytical analysis of aliasing artifacts in multizone reproductions. By realising the designed crossover filters, wideband acoustic contrast between zones is significantly improved. The trade-off between acoustic contrast and the bandwidth of the reproduced soundfield is investigated. Results show that by incorporating the proposed hybrid model the whole wideband bandwidth is spatial-aliasing free with a mean acoustic contrast consistently above 54.2dB, an improvement of up to 24.2dB from a non-hybrid approach, with as …


Sodium Borohydride Hydrazinates: Synthesis, Crystal Structures, And Thermal Decomposition Behavior, Jianfeng Mao, Qinfen Gu, Zaiping Guo, Hua-Kun Liu Jan 2015

Sodium Borohydride Hydrazinates: Synthesis, Crystal Structures, And Thermal Decomposition Behavior, Jianfeng Mao, Qinfen Gu, Zaiping Guo, Hua-Kun Liu

Faculty of Engineering and Information Sciences - Papers: Part A

Metallic borohydride hydrazinates are novel boron- and nitrogen-based materials that appear to be promising candidates for chemical hydrogen storage. Herein, sodium borohydride hydrazinates, including NaBH4·N2H4 and NaBH4·2N2H4, were synthesized via a facile solution synthesis approach based on the solid-liquid reaction between NaBH4 and hydrazine in tetrahydrofuran (THF) solution. The crystal structure of NaBH4·2N2H4 was solved to a monoclinic structure with unit cell parameters a = 8.4592(2) Å, b = 11.7131(2) Å, c = 6.4584(1) Å, and β = 100.0777(14)°, with space group A1a1 (9). Each …


Facile Synthesis Of Coaxial Cnts/Mnox-Carbon Hybrid Nanofibers And Their Greatly Enhanced Lithium Storage Performance, Zunxian Yang, Jun Lv, Haidong Pang, Wenhuan Yan, Kun Qian, Tailiang Guo, Zaiping Guo Jan 2015

Facile Synthesis Of Coaxial Cnts/Mnox-Carbon Hybrid Nanofibers And Their Greatly Enhanced Lithium Storage Performance, Zunxian Yang, Jun Lv, Haidong Pang, Wenhuan Yan, Kun Qian, Tailiang Guo, Zaiping Guo

Faculty of Engineering and Information Sciences - Papers: Part A

Carbon nanotubes (CNTs)/MnOx-Carbon hybrid nanofibers have been successfully synthesized by the combination of a liquid chemical redox reaction (LCRR) and a subsequent carbonization heat treatment. The nanostructures exhibit a unique one-dimensional core/shell architecture, with one-dimensional CNTs encapsulated inside and a MnOx-carbon composite nanoparticle layer on the outside. The particular porous characteristics with many meso/micro holes/pores, the highly conductive one-dimensional CNT core, as well as the encapsulating carbon matrix on the outside of the MnOx nanoparticles, lead to excellent electrochemical performance of the electrode. The CNTs/MnOx-Carbon hybrid nanofibers exhibit a high initial reversible capacity of …


Ontological Meta-Analysis And Synthesis Of Hipaa, Arkalgud Ramaprasad, Thant Syn, Khin Than Win Jan 2014

Ontological Meta-Analysis And Synthesis Of Hipaa, Arkalgud Ramaprasad, Thant Syn, Khin Than Win

Faculty of Engineering and Information Sciences - Papers: Part A

We present ontological meta-analysis and synthesis of HIPAA (Health Insurance Portability and Accountability Act) as a method for reviewing, mapping, and visualizing the research literature in the domain cumulatively, logically, systematically, and systemically. The method will highlight the domain's bright spots which are heavily emphasized, the light spots which are lightly emphasized, the blind spots which have been overlooked, and the blank spots which may never be emphasized. It will highlight the biases and asymmetries in the domain's research; the research can then be realigned to make it stronger and more effective. We present an ontology for HIPAA, map the …


High Di-Electric Constant Nano-Structure Ceramics Synthesis Using Novel Electric Discharge Assisted Mechanical Milling And Magneto Ball Milling And Its Properties, Azrin A. Chowdhury, Andrzej Calka, David Wexler, Konstantin Konstantinov Jan 2014

High Di-Electric Constant Nano-Structure Ceramics Synthesis Using Novel Electric Discharge Assisted Mechanical Milling And Magneto Ball Milling And Its Properties, Azrin A. Chowdhury, Andrzej Calka, David Wexler, Konstantin Konstantinov

Faculty of Engineering and Information Sciences - Papers: Part A

The conventional method to prepare functional oxides is ceramicpowder- based processing typically via solid-state reaction of microcrystalline starting powders at high temperatures. Disadvantages of this approach include the high temperatures of reaction, limited degree of product chemical homogeneity and difficulties in achieving rapid sintering. Various chemicalbased processing routes have been developed to prepare powders of more homogeneous composition, improved reactivity and sintering ability at low temperatures. Regardless of the route chosen to synthesise complex oxides, almost all of them require lengthy heat treatment schedules that usually exceed 10 h, as well as multi-stage processing steps. We describe two approaches to …


Additive-Free Synthesis Of 3d Porous V2o5 Hierarchical Microspheres With Enhanced Lithium Storage Properties, Chaofeng Zhang, Zhixin Chen, Zaiping Guo, Xiong Wen Lou Jan 2013

Additive-Free Synthesis Of 3d Porous V2o5 Hierarchical Microspheres With Enhanced Lithium Storage Properties, Chaofeng Zhang, Zhixin Chen, Zaiping Guo, Xiong Wen Lou

Faculty of Engineering and Information Sciences - Papers: Part A

A facile synthesis of novel 3D porous V2O5 hierarchical microspheres has been developed, based on an additive-free solvothermal method and subsequent calcination. Due to their unique structure, these V2O5 microspheres display a very stable capacity retention of 130 mA h g (1) over 100 cycles at a current rate of 0.5 C, and show excellent rate capability with a capacity of 105 mA h g (1) even at the 30 C rate. The good electrochemical performance suggests that this unique hierarchical V2O5 material could be a promising candidate as a cathode material for lithium-ion batteries.


Synthesis And Optimization Of Pedot:Pss Based Ink For Printing Nanoarrays Using Dip-Pen Nanolithography, Michal Wagner, Cathal O'Connell, David G. Harman, Ryan Sullivan, Ari Ivaska, Michael J. Higgins, Gordon G. Wallace Jan 2013

Synthesis And Optimization Of Pedot:Pss Based Ink For Printing Nanoarrays Using Dip-Pen Nanolithography, Michal Wagner, Cathal O'Connell, David G. Harman, Ryan Sullivan, Ari Ivaska, Michael J. Higgins, Gordon G. Wallace

Faculty of Engineering and Information Sciences - Papers: Part A

Due to the current interest in organic printable electronics, Dip-Pen Nanolithography (DPN) is increasingly being explored as a method to pattern electroactive materials such as conducting polymers (CPs) on the micro- and nanoscale. In general, printing process depends strongly on the ink-substrate properties and fundamental forces required to drive and stabilize the ink transfer to the substrate. Controlling these parameters is especially difficult when operating under the nanometer confinements of the DPN probe. For the printing of CPs, one step towards addressing these challenges is rational ink design, as the use of existing commercial-based inks may not be suitable for …


Mixed-Metal (Li, Al) Amidoborane: Synthesis And Enhanced Hydrogen Storage Properties, Guanglin Xia, Yingbin Tan, Xiaowei Chen, Zaiping Guo, Hua-Kun Liu, Xuebin Yu Jan 2013

Mixed-Metal (Li, Al) Amidoborane: Synthesis And Enhanced Hydrogen Storage Properties, Guanglin Xia, Yingbin Tan, Xiaowei Chen, Zaiping Guo, Hua-Kun Liu, Xuebin Yu

Faculty of Engineering and Information Sciences - Papers: Part A

Mixed-metal (Li, Al) amidoborane has been synthesized via mechanical ball milling of ammonia borane with lithium hexahydridoaluminate in different molar ratios. The reversible dehydrogenation properties of the thus-synthesized metallic amidoborane and its mixtures with ammonia borane in different ratios were systematically investigated in comparison with neat ammonia borane (AB). On the basis of thermogravimetric analysis and mass spectrometry results, the thus-synthesized mixed-metal amidoborane was shown to release around 10 wt% hydrogen below 200 degrees C, with an effective suppression of volatile side products. Furthermore, a synergistic effect between metallic amidoborane and ammonia borane has been identified, which leads to the …


Rapid Synthesis Of Free-Standing Moo3/Graphene Films By The Microwave Hydrothermal Method As Cathode For Bendable Lithium Batteries, Lukman Noerochim, Jia-Zhao Wang, David Wexler, Zhong Chao, Hua-Kun Liu Jan 2013

Rapid Synthesis Of Free-Standing Moo3/Graphene Films By The Microwave Hydrothermal Method As Cathode For Bendable Lithium Batteries, Lukman Noerochim, Jia-Zhao Wang, David Wexler, Zhong Chao, Hua-Kun Liu

Faculty of Engineering and Information Sciences - Papers: Part A

Highly flexible, binder-free, MoO3 nanobelt/graphene film electrode is prepared by a two-step microwave hydrothermal method. Graphene is first prepared by an ultra-fast microwave hydrothermal method and then mixed with MoO3 solution to synthesize the MoO3 nanobelt/graphene composite, which exhibits the combination of stacked graphene sheets and uniform MoO3 nanobelts with widths of 200-500 nm and lengths of 5-10 μm. The charge-discharge measurements show that the as-synthesized MoO3/graphene hybrid materials demonstrate excellent rate capability, large capacity, and good cycling stability compared to the pure MoO3 film. An initial discharge capacity of 291 mAh g-1 can be obtained at 100 mA g-1, …


Facile Synthesis Of Hierarchical Networks Composed Of Highly Interconnected V2o5 Nanosheets Assembled On Carbon Nanotubes And Their Superior Lithium Storage Properties, Ruixiang Yu, Chaofeng Zhang, Qing Meng, Zhixin Chen, Hua-Kun Liu, Zaiping Guo Jan 2013

Facile Synthesis Of Hierarchical Networks Composed Of Highly Interconnected V2o5 Nanosheets Assembled On Carbon Nanotubes And Their Superior Lithium Storage Properties, Ruixiang Yu, Chaofeng Zhang, Qing Meng, Zhixin Chen, Hua-Kun Liu, Zaiping Guo

Faculty of Engineering and Information Sciences - Papers: Part A

Hierarchical networks with highly interconnected V2O5 nanosheets (NSs) anchored on skeletons of carbon nanotubes (CNTs) are prepared by a facile hydrothermal treatment and a following calcination for the first time. Benefiting from these unique structural features, the as-prepared CNT@V2O5 material shows dramatically excellent electrochemical performance with remarkable long cyclability (137-116 mA h g-1 after 400 cycles) at various high rates (20 C to 30 C) and very good rate capability for highly reversible lithium storage. The excellent electrochemical performance suggests its promising use as a cathode material for future lithium-ion batteries.


Encoding Navigable Speech Sources: A Psychoacoustic-Based Analysis-By-Synthesis Approach, Xiguang Zheng, Christian Ritz, Jiangtao Xi Jan 2013

Encoding Navigable Speech Sources: A Psychoacoustic-Based Analysis-By-Synthesis Approach, Xiguang Zheng, Christian Ritz, Jiangtao Xi

Faculty of Engineering and Information Sciences - Papers: Part A

This paper presents a psychoacoustic-based analysis-by-synthesis approach for compressing navigable speech sources. The approach targets multi-party teleconferencing applications, where selective reproduction of individual speech sources is desired. Based on exploiting sparsity of speech in the perceptual time-frequency domain, multiple speech signals are encoded into one mono mixture signal, which can be further compressed using a standard speech codec. Using side information indicating the active speech source for each time frequency instant enables flexible decoding and reproduction. Objective results highlight the importance of considering perception when exploiting the sparse nature of speech in the time-frequency domain. Results show that this sparsity, …


In Situ One-Step Synthesis Of A 3d Nanostructured Germanium-Graphene Composite And Its Application In Lithium-Ion Batteries, Chao Zhong, Jia-Zhao Wang, Xuan-Wen Gao, David Wexler, Hua-Kun Liu Jan 2013

In Situ One-Step Synthesis Of A 3d Nanostructured Germanium-Graphene Composite And Its Application In Lithium-Ion Batteries, Chao Zhong, Jia-Zhao Wang, Xuan-Wen Gao, David Wexler, Hua-Kun Liu

Faculty of Engineering and Information Sciences - Papers: Part A

A germanium-graphene nanocomposite material with three-dimensional nanostructures has been synthesized by an efficient one-step, in situ, and aqueous-based method. The electrochemical properties of the germanium-graphene nanocomposite have been evaluated by galvanostatic discharge-charge cycling, cyclic voltammetry, and electrochemical impedance spectroscopy. Results show that the germanium-graphene nanocomposite has a much more stable cycling performance than that of the pure germanium, with a capacity of about 832 mA h g-1 after 50 cycles. The rate capability is also improved significantly. The superior performance is attributed to the graphene content, which increases the material's conductivity, enlarges the specific surface area, delivers enough sites to …


Synthesis Of Mn3o4-Encapsulated Graphene Sheet Nanocomposites Via A Facile, Fast Microwave Hydrothermal Method And Their Supercapacitive Behaviour, Li Li, Kuok Hau Seng, Zhixin Chen, Hua-Kun Liu, Ivan P. Nevirkovets, Zaiping Guo Dec 2012

Synthesis Of Mn3o4-Encapsulated Graphene Sheet Nanocomposites Via A Facile, Fast Microwave Hydrothermal Method And Their Supercapacitive Behaviour, Li Li, Kuok Hau Seng, Zhixin Chen, Hua-Kun Liu, Ivan P. Nevirkovets, Zaiping Guo

Faculty of Engineering and Information Sciences - Papers: Part A

Well-crystallized Mn3O4-anchored reduced graphene oxide (rGO) nanocomposites have been successfully synthesized via a facile, effective, energy-saving, and scalable microwave hydrothermal technique for potential application as supercapacitor material. Integrating these nanostructures resulted in a strong synergistic effect between the two materials, consequently leading to a hybrid composite with higher specific capacitance compared to the bare Mn3O4 nanoparticles. The results from different sorts of characterization indicate that the Mn3O4 particles were deposited and anchored on graphene sheets. The capacitance value of the rGO(31.6%)–Mn3O4 nanocomposite reached 153 F/g, much higher than that of the bare Mn3O4 (87 F/g) at a scan rate of …


A Synthesis Of A Knowledge Management Framework For Sports Event Management, Azizul Rahman Abdul Ghaffar, Ghassan Beydoun, Jun Shen, Will Tibben, Dongming Xu Jan 2012

A Synthesis Of A Knowledge Management Framework For Sports Event Management, Azizul Rahman Abdul Ghaffar, Ghassan Beydoun, Jun Shen, Will Tibben, Dongming Xu

Faculty of Engineering and Information Sciences - Papers: Part A

Due to rapid social development in Asia, sports events have grown larger and many new countries are also hosting them for their first time. In addition to required increase in expenditures and more efficient management, various instances of inadequate planning highlighted the needs for more effective and better sustainable structures to support knowledge transfer between organizers, from one event to the next. The research presented in this paper aims to facilitate the deployment of systematic knowledge management practices to sports event management, to enable sustainable planning. The research in this paper synthesizes is carried out on the Malaysian Games as …


Synthesis And Electrochemical Properties Of Sn-Sno2/C Nanocomposite, Chuanqi Feng, Meiyu Dan, Chaofeng Zhang, Zaiping Guo, Shiquan Wang, R Zeng Jan 2012

Synthesis And Electrochemical Properties Of Sn-Sno2/C Nanocomposite, Chuanqi Feng, Meiyu Dan, Chaofeng Zhang, Zaiping Guo, Shiquan Wang, R Zeng

Faculty of Engineering and Information Sciences - Papers: Part A

A Sn-Sn02/C nanocomposite was synthesized using the electrospinning method. Thermal analysis was used to determine the content range of Sn and Sn02 in the composite. The composite was characterized by X-ray diffraction, and the particle size and shape in the Sn-SnOiC composite were determined by scanning and transmission electron microscopy. The results show that the Sn-Sn02/C composite takes on a nanofiber morphology, with the diameters of the nanofibers distributed from 50 to 200 nm. The electrOChemical properties of the Sn-SnOiC composite were also investigated. The Sn-SnOiC composite as an electrode material has both higher reversible capacity (887 mAh· g-I). and …


Ultrabroadband Optical Parametric Chirped Pulse Amplifier System For Single-Cycle Waveform Synthesis, Shu-Wei Huang, Giovanni Cirmi, Jeffrey Moses, Kyung-Han Hong, Andrew Benedick, Li-Jin Chen, Enbang Li, Benjamin J. Eggleton, Giulio Cerullo, Franz X. Kartner Jan 2010

Ultrabroadband Optical Parametric Chirped Pulse Amplifier System For Single-Cycle Waveform Synthesis, Shu-Wei Huang, Giovanni Cirmi, Jeffrey Moses, Kyung-Han Hong, Andrew Benedick, Li-Jin Chen, Enbang Li, Benjamin J. Eggleton, Giulio Cerullo, Franz X. Kartner

Faculty of Engineering and Information Sciences - Papers: Part A

We demonstrate synchronized few-cycle 800-nm and 2-μm pulse trains seeded from a single Ti:sapphire oscillator, able to generate scalable, high-energy pulses lasting less than a single electric-field cycle. Such pulses are attractive for high-field physics.


Low Temperature Synthesis Of Al-Aln Composites From A Nanostructure Made By Controlled Magneto-Ball Milling Of Al In Ammonia, Andrzej Calka, J I. Nikolov, G H. J Wantenaar Jan 1994

Low Temperature Synthesis Of Al-Aln Composites From A Nanostructure Made By Controlled Magneto-Ball Milling Of Al In Ammonia, Andrzej Calka, J I. Nikolov, G H. J Wantenaar

Faculty of Engineering and Information Sciences - Papers: Part A

The formation of an AlN compound in ball milled Al powder in ammonia was studied. In this work a magneto‐ball milling device with controlled ball movement was used. The end milling product was an Al based nanostructure. This product can be transformed into an AlN‐Al nanocomposite upon heating below the melting point of Al. It was found that the level of unreacted Al is dependent on milling time. The maximum amount of AlN was 88.28 wt %. The structure of as‐milled and annealed samples was investigated using x‐ray diffractometry and transmission electron microscopy. Differential thermal analysis was performed on as‐milled …