Open Access. Powered by Scholars. Published by Universities.®

Physics Commons

Open Access. Powered by Scholars. Published by Universities.®

Articles 1 - 4 of 4

Full-Text Articles in Physics

Nanoscale Manipulation Of Pristine And Functionalized Freestanding Graphene Using Scanning Tunneling Microscopy, Matthew Ackerman Aug 2014

Nanoscale Manipulation Of Pristine And Functionalized Freestanding Graphene Using Scanning Tunneling Microscopy, Matthew Ackerman

Graduate Theses and Dissertations

Over the past ten years the 2D material graphene has attracted an enourmous amount of attention from researchers from across diciplines and all over the world. Many of its outstanding electronic properties are present only when it is not interacting with a substrate but is instead freestanding. In this work I demonstrate that pristine and functionalized freestanding graphene can be imaged using a scanning tunneling microscope (STM) and that imaging a flexible 2D surface is fundamentally different from imaging a bulk material due to the attraction between the STM tip and the sample. This attraction can be used to manipulate …


Spin And Orbital Moments And Magnetic Order In Fe3o4 Nanoparticle Assemblies, Yanping Cai Mar 2014

Spin And Orbital Moments And Magnetic Order In Fe3o4 Nanoparticle Assemblies, Yanping Cai

Theses and Dissertations

Fe3O4 magnetic nanoparticles of 5 to 11 nm in size were prepared by organic methods. Particle size was analyzed by both X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM) techniques. Zero Field Cooling (ZFC) / Field Cooling (FC) and magnetization loop measurements were recorded by VSM, and they confirmed superparamagnetic behavior in the sample. The blocking temperature is found to be in the range of 30 K ~ 170 K. It has a dependence on the particle size. ZFC / FC curves also indicate the presence of magnetic coupling between particles. X-ray Magnetic Circular Dichroism (XMCD) measurements of these nanoparticles …


Quantitative Scanning Transmission Electron Microscopy Of Thick Samples And Of Gold And Silver Nanoparticles On Polymeric Surfaces, Aniruddha Dutta Jan 2014

Quantitative Scanning Transmission Electron Microscopy Of Thick Samples And Of Gold And Silver Nanoparticles On Polymeric Surfaces, Aniruddha Dutta

Electronic Theses and Dissertations

Transmission Electron Microscopy (TEM) is a reliable tool for chemical and structural studies of nanostructured systems. The shape, size and volumes of nanoparticles on surfaces play an important role in surface chemistry. As nanostructured surfaces become increasingly important for catalysis, protective coatings, optical properties, detection of specific molecules, and many other applications, different techniques of TEM can be used to characterize the properties of nanoparticles on surfaces to provide a path for predictability and control of these systems. This dissertation aims to provide fundamental understanding of the surface chemistry of Electroless Metallization onto Polymeric Surfaces (EMPS) through characterization with TEM. …


Inverted Linear Halbach Array For Separation Of Magnetic Nanoparticles, Chetan Poudel Jan 2014

Inverted Linear Halbach Array For Separation Of Magnetic Nanoparticles, Chetan Poudel

Honors Papers

Magnetic nanoparticles have unique physical and chemical properties, making them appealing candidates for biomedical applications. These applications depend critically on size and magnetic uniformity of the nanoparticles. Unfortunately, very few purification methods exist to sort nanoparticles based on their magnetic properties. Here, we describe an unusual approach to this problem through our construction of a device containing a linear array of permanent magnets in a Halbach configuration, where successive magnet blocks have their magnetization orientation at right angles. The array provides a large region of relatively low magnetic field, yet high magnetic field gradient where sorting of nanoparticles based on …