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1997

Faculty Publications

EPR

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System For Electron Paramagnetic Resonance Measurements At High Pressure And Low Temperature, Ke Huang, Daniel L. Decker, H. Mark Nelson, J. Dean Barnett Oct 1997

System For Electron Paramagnetic Resonance Measurements At High Pressure And Low Temperature, Ke Huang, Daniel L. Decker, H. Mark Nelson, J. Dean Barnett

Faculty Publications

Major improvements have been made on the sensitive high pressure electron paramagnetic resonance (EPR) system developed previously in 1978 at this laboratory. These changes allow low temperature measurements and provide a more stable signal. The high pressure EPR cell is placed inside a vacuum chamber to provide thermal isolation, so that the system may be cooled by a closed cycle refrigerator to temperatures between 45 and 60 K, depending on the energy input to the modulation coil. The combination of high pressure and low temperature greatly expands the thermodynamic range over which EPR measurements can be made. An improved and …