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High temperatures

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Structural Studies Of Crsi2 At High Pressures And Temperatures, Weldu Gabrimicael, Ravhi S. Kumar, Andrew Cornelius Aug 2008

Structural Studies Of Crsi2 At High Pressures And Temperatures, Weldu Gabrimicael, Ravhi S. Kumar, Andrew Cornelius

Undergraduate Research Opportunities Program (UROP)

It is of extreme importance to develop new potential energy sources to reduce dependence on fossil fuels. As a result of this, the study of thermoelectric materials, capable of changing heat into electrical energy, has become a field of great interest regarding fundamental properties. To help better understand these materials, facilities for the measurement of relevant properties at high pressure have been developed, but lack the ability to characterize the materials at high temperature and pressure. Therefore, this project has the goal of developing a heater arrangement to be used in conjunction with the high pressure capabilities already developed to …


The Search For Ferroelectric Domain Structures In Carbohydrate Glasses Using Atomic Force Microscopy, Louis S. Prahl, David P. Shelton Aug 2008

The Search For Ferroelectric Domain Structures In Carbohydrate Glasses Using Atomic Force Microscopy, Louis S. Prahl, David P. Shelton

Undergraduate Research Opportunities Program (UROP)

D-glucose was studied as a possible candidate for ferroelectric domain imaging using an Atomic Force Microscope (AFM). The large dipole moment of carbohydrates is such that they may show localized ferroelectric domain formation in liquid phase. Samples were heated at their melting point on glass slides and then left to cool to room temperature in a desiccator. Differential Thermal Analysis (DTA) was used to test the effectiveness of this method, and it was found that the oven preparation created samples with 41% crystallinity, where both a glass transition and sharp melting peak were observed. DTA was again used to find …