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David Sellmyer Publications

TEM

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Full-Text Articles in Physics

A Tem Study Of Fe3+X Co3-XTi2 (X = 0, 1, 2, 3) Intermetallic Alloys, Xingzhong Li, Anandakumar Sarella, B. Balasubramanian, Shah R. Valloppilly Oct 2022

A Tem Study Of Fe3+X Co3-XTi2 (X = 0, 1, 2, 3) Intermetallic Alloys, Xingzhong Li, Anandakumar Sarella, B. Balasubramanian, Shah R. Valloppilly

David Sellmyer Publications

A TEM study has been carried out on crystal structures in the rare-earth-free intermetallic alloys, Fe3+xCo3-xTi2 (x = 0, 1, 2, 3). These alloys have been demonstrated to have potentially high magnetic anisotropy. In these alloys, the main intermetallic compound was recently reported as a new hexagonal phase with a space group of P-6 m2. The present study reveals that the main compound belongs to Laves C14 variant surrounded by α-Fe type crystal as secondary phase in the Fe3+xCo3-xTi2 (x = 0, 1, 2, 3) alloys, in agreement with the …


Orthorhombic Zr2Co11 Phase Revisited, Xingzhong Li, Wenyong Zhang, David J. Sellmyer, X Zhao, M C. Nguyen, C Z. Wang, K M. Ho Jan 2014

Orthorhombic Zr2Co11 Phase Revisited, Xingzhong Li, Wenyong Zhang, David J. Sellmyer, X Zhao, M C. Nguyen, C Z. Wang, K M. Ho

David Sellmyer Publications

The structure of the orthorhombic Zr2Co11 phase was revisited in the present work. Selected-area electron diffraction (SAED) and high-resolution electron microscopy (HREM) techniques were used to investigate the structure. They show the orthorhombic Zr2Co11 phase has a 1-D incommensurate modulated structure. The structure can be approximately described as a B-centered orthorhombic lattice. The lattice parameters of the orthorhombic Zr2Co11 phase have been determined by a tilt series of SAED patterns. A hexagonal network with a modulation wave has been observed in the HREM image and the hexagonal motif is considered as …


Pore Structure, Barrier Layer Topography And Matrix Alumina Structure Of Porous Anodic Alumina Film, Yucheng Sui, B.Z. Cui, L. Martinez, R. Perez, David J. Sellmyer Apr 2002

Pore Structure, Barrier Layer Topography And Matrix Alumina Structure Of Porous Anodic Alumina Film, Yucheng Sui, B.Z. Cui, L. Martinez, R. Perez, David J. Sellmyer

David Sellmyer Publications

Different anodic voltages and methods were adopted to produce porous anodic alumina films (PAAF) in an aqueous solution of oxalic acid. Carbon tube growth by chemical vapor deposition (CVD) in the films was used to copy the internal pore structure and was recorded by transmission electron microscopy (TEM) photos. Atomic force microscope (AFM) was employed to obtain the topography of the barrier layer of the corresponding films. When the anodic voltage was 40 V and the two-step method adopted, the barrier layer of the film had domains with highly ordered hexagonal cell distribution, and the corresponding pores were straight. When …