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Articles 1 - 30 of 97
Full-Text Articles in Physics
Enabling Rapid Chemical Analysis Of Plutonium Alloys Via Machine Learning-Enhanced Atomic Spectroscopy Techniques, Ashwin P. Rao
Enabling Rapid Chemical Analysis Of Plutonium Alloys Via Machine Learning-Enhanced Atomic Spectroscopy Techniques, Ashwin P. Rao
Theses and Dissertations
Analytical atomic spectroscopy methods have the potential to provide solutions for rapid, high fidelity chemical analysis of plutonium alloys. Implementing these methods with advanced analytical techniques can help reduce the chemical analysis time needed for plutonium pit production, directly enabling the 80 pit-per-year by 2030 manufacturing goal outlined in the 2018 Nuclear Posture Review. Two commercial, handheld elemental analyzers were validated for potential in situ analysis of Pu. A handheld XRF device was able to detect gallium in a Pu surrogate matrix with a detection limit of 0.002 wt% and a mean error of 8%. A handheld LIBS device was …
Characterization Of Environmental Conditioning Of Lithium Hydride Using Spectroscopy And Machine Learning, Ryan E. Pinson
Characterization Of Environmental Conditioning Of Lithium Hydride Using Spectroscopy And Machine Learning, Ryan E. Pinson
Theses and Dissertations
Lithium compounds such as lithium hydride (LiH) and anhydrous lithium hydroxide (LiOH) have various applications in industry but are highly reactive when exposed to moisture and CO2. These reactions create new molecular forms, including compounds such as lithium oxide (Li2O), lithium hydroxide monohydrate (LiOH ·H2O), and lithium carbonate (Li2CO3). These new compounds degrade the effectiveness in applications using these compounds. The negative effects induced by new lithium compounds creates a need for the ability to characterize the in-growth of such compounds. To study these in-growths, this work will present environmental …
Development Of A Magnetic Confinement Attachment For Enhanced Signal In Handheld Laser Induced Breakdown Spectroscopy Soil Analysis, Alfred C. Anderson
Development Of A Magnetic Confinement Attachment For Enhanced Signal In Handheld Laser Induced Breakdown Spectroscopy Soil Analysis, Alfred C. Anderson
Theses and Dissertations
Field techniques for characterizing low levels of heavy elements of less than 100 parts per million in soils tend to be unreliable because of the relatively weak signal of these elements and the large, variable background inherent to analyzing soils with minimal sample preparation. To enhance the detection and analysis capability of a handheld laser-induced breakdown spectroscopy (LIBS) instrument, this work investigates the effects of a unique magnetic confinement apparatus on signal intensities, focusing on five iron lines as well as those from actinides in 11 soil samples. The proposed magnetic confinement apparatus achieved over 0.8 T but did not …
Neutron Energy Tuning Assemblies For Nuclear Weapon Environment Applications At The National Ignition Facility, Nicholas J. Quartemont
Neutron Energy Tuning Assemblies For Nuclear Weapon Environment Applications At The National Ignition Facility, Nicholas J. Quartemont
Theses and Dissertations
An energy tuning assembly was developed to spectrally shape the National Ignition Facility deuterium-tritium fusion neutron source to a notional thermonuclear and prompt fission neutron spectrum to fulfill neutron source capability gaps. The experimental neutron environment was characterized with activation dosimetry, neutronics and covariance models, and unfolded to determine the as-fielded neutron spectrum. The first energy tuning assembly was demonstrated to create synthetic spectrally accurate post-detonation fission products, enhancing U.S. technical nuclear forensics capabilities. ATHENA, a second-generation energy tuning assembly, was also optimized to meet similar objectives, but the new platform neutron fluence efficiency was increased by a factor of …
Correlated Positron-Electron Orbital (Cpeo): A Novel Method That Models Positron-Electron Correlation In Virtual Ps At The Mean-Field Level, Kevin E. Blaine
Correlated Positron-Electron Orbital (Cpeo): A Novel Method That Models Positron-Electron Correlation In Virtual Ps At The Mean-Field Level, Kevin E. Blaine
Theses and Dissertations
The Correlated Positronic-Electronic Orbital (CPEO) method was developed and implemented to capture correlation effects at between the positron and electron in the modeling of systems that involve a bound positron. Methods that effectively model these systems require many hundred basis functions and use a mean field approach as the beginning step. CPEO builds an orbital for virtual Positronium (Ps) that contains a positron in a bound state along with an accompanying electron to the larger system. Assigning the virtual Ps orbital allows for the two particle variational optimization in conjunction with the other particles that compose the whole system. This …
Data Driven Investigation Into The Off-Axis Brdf To Develop An Algorithm To Classify Anisotropicity, Anne W. Werkley
Data Driven Investigation Into The Off-Axis Brdf To Develop An Algorithm To Classify Anisotropicity, Anne W. Werkley
Theses and Dissertations
The Bi-directional Reflectance Distribution Function (BRDF) is used to describe reflectances of materials by calculating the ratio of the reflected radiance to the incident irradiance. While it was found that isotropic BRDF microfacet models maintained symmetry about ɸs = π, such symmetry was not maintained about the θs = θi axis, except for close to the specular peak. This led to development of a novel data-driven metric for how isotropic a BRDF measurement is. Research efforts centered around developing an algorithm that could determine material anisotropy without having to fit to models. The algorithm developed here successfully …
Lithium Compound Characterization Via Laser Induced Breakdown Spectroscopy And Raman Spectroscopy, James T. Stofel
Lithium Compound Characterization Via Laser Induced Breakdown Spectroscopy And Raman Spectroscopy, James T. Stofel
Theses and Dissertations
Industries such as lithium-ion battery producers and the nuclear industry community seek to produce and store lithium in pure chemical forms. However, these lithium compounds are reactive with the atmosphere and quickly degrade into less desirable forms. Therefore, industry desires a fast and effective quality control approach to quantify the ingrowth of these secondary lithium chemical forms. This research presents a novel approach using Laser-Induced Breakdown Spectroscopy (LIBS) and Raman spectroscopy in tandem to enhance lithium compound characterization beyond what is achieved by either technique alone. The resulting spectral data are aggregated using data fusion and analyzed using chemometrics for …
Error Reduction For The Determination Of Transverse Moduli Of Single-Strand Carbon Fibers Via Atomic Force Microscopy, Joshua D. Frey
Error Reduction For The Determination Of Transverse Moduli Of Single-Strand Carbon Fibers Via Atomic Force Microscopy, Joshua D. Frey
Theses and Dissertations
The transverse modulus of single strand carbon fibers is measured using PeakForce Atomic Force Microscopy - Quantitative Nanomechanical Measurement to less than 5 percent error for 11 types of carbon fiber with longitudinal moduli between 924-231 GPA, including export-controlled fibers. Statistical methods are employed to improve the quality of data to exclude outliers within an measurement and within the sample set. A positive linear correlation between the longitudinal and transverse modulus with an R2=0.76 is found. Pitch-based fibers exhibit lower measurement error than PAN-based fibers, while PAN fibers exhibited no apparent modulus correlation when the Pitch fibers are …
Computational Electromagnetic Modeling Of Metasurface Optical Devices With Defect Study, Carlos D. Diaz
Computational Electromagnetic Modeling Of Metasurface Optical Devices With Defect Study, Carlos D. Diaz
Theses and Dissertations
One of the first fabricated metasurface optical devices, the in-plane V-antenna lenses, were plagued by a fundamental transmission limit (<25 >). Two distinct sets of Out-of-Plane phase elements were designed with improved transmission (~60 ). These were fabricated as beamsteerers and characterized in terms of their Bidirectional Transmittance Distribution Function measured as a function of scatter angle. Experimental data from the beamsteerers was analyzed via simulations using a finite element method (FEM). The measurements showed the designed beamsteering, but also a strong zero-order diffraction not present in the simulations, which motivated this study to understand what was causing these differences. …
Ab Initio Spectroscopy Of Natural And Artificial Fire Contaminants For V/W Band Frequency Signal Absorbance, Matthew B. Husk
Ab Initio Spectroscopy Of Natural And Artificial Fire Contaminants For V/W Band Frequency Signal Absorbance, Matthew B. Husk
Theses and Dissertations
The rotation and vibration spectral properties including frequencies and intensities for highly concentrated molecules present in wildland and artificial fires have been studied. These properties were used to determine absorption and its effect in a link budget analysis. Absorption in link budget analyses is commonly accounted for via line-by-line methodology aided by HITRAN documented intensities. Limited, if any, customization of spectral properties is available with HITRAN and other spectral databases. Ab initio calculations with different atomic basis sets were employed to obtain structures, dipole moments, rotational-vibrational frequencies and intensities, as well as various coupling parameters. Anharmonic corrections to the vibrational …
Physics-Constrained Hyperspectral Data Exploitation Across Diverse Atmospheric Scenarios, Nicholas M. Westing
Physics-Constrained Hyperspectral Data Exploitation Across Diverse Atmospheric Scenarios, Nicholas M. Westing
Theses and Dissertations
Hyperspectral target detection promises new operational advantages, with increasing instrument spectral resolution and robust material discrimination. Resolving surface materials requires a fast and accurate accounting of atmospheric effects to increase detection accuracy while minimizing false alarms. This dissertation investigates deep learning methods constrained by the processes governing radiative transfer to efficiently perform atmospheric compensation on data collected by long-wave infrared (LWIR) hyperspectral sensors. These compensation methods depend on generative modeling techniques and permutation invariant neural network architectures to predict LWIR spectral radiometric quantities. The compensation algorithms developed in this work were examined from the perspective of target detection performance using …
Low-Information Radiation Imaging Using Rotating Scatter Mask Systems And Neural Network Algorithms, Robert J. Olesen
Low-Information Radiation Imaging Using Rotating Scatter Mask Systems And Neural Network Algorithms, Robert J. Olesen
Theses and Dissertations
While recent studies have demonstrated the directional capabilities of the single-detector rotating scatter mask (RSM) system for discrete, dual-particle environments, there has been little progress towards adapting it as a true imaging device. In this research, two algorithms were developed and tested using an RSM mask design previously optimized for directional detection and simulated 137Cs signals from a variety of source distributions. The first, maximum-likelihood expectation-maximization (ML-EM), was shown to generate noisy images, with relatively low accuracy (145% average relative error) and signal-to-noise ratio (0.27) for most source distributions simulated. The second, a novel regenerative neural network (ReGeNN), performed exceptionally …
Rapid Analysis Of Plutonium Surrogate Material Via Hand-Held Laser-Induced Breakdown Spectroscopy, Ashwin P. Rao
Rapid Analysis Of Plutonium Surrogate Material Via Hand-Held Laser-Induced Breakdown Spectroscopy, Ashwin P. Rao
Theses and Dissertations
This work investigated the capability of a portable LIBS device to detect and quantify dopants in plutonium surrogate alloys, specifically gallium, which is a common stabilizer used in plutonium alloys. The SciAps Z500-ER was utilized to collect spectral data from cerium-gallium alloys of varying gallium concentrations. Calibration models were built to process spectra from the Ce-Ga alloys and calculate gallium concentration from spectral emission intensities. Univariate and multivariate analysis techniques were used to determine limits of detection of different emission line ratios. Spatial mapping measurements were conducted to determine the device's ability to detect variations in gallium concentration on the …
Measurement Of The 160Gd(P,N)160Tb Excitation Function From 4 18 Mev, Using A Stacked Foil Technique, Ryan K. Chapman
Measurement Of The 160Gd(P,N)160Tb Excitation Function From 4 18 Mev, Using A Stacked Foil Technique, Ryan K. Chapman
Theses and Dissertations
A stack of thin Gd, Ti, and Cu foils were irradiated with an 18 MeV proton beam at Lawrence-Berkeley National Laboratory's 88-Inch Cyclotron to investigate the 160Gd(p,n)160Tb nuclear reaction for nuclear forensics applications. This experiment will improve knowledge of 160Tb production rates, allowing 160Tb to be efficiently created in a foil stack consisting of other proton induced isotopes for forensics applications. A set of 15 measured cross sections between 4-18 MeV for 160Gd(p,n)160Tb were obtained using a stacked foil technique. The foil stack consisted of one stainless steel, one iron, fifteen gadolinium, …
Comparison Of The Accuracy Of Rayleigh-Rice Polarization Factors To Improve Microfacet Brdf Models, Rachel L. Wolfgang
Comparison Of The Accuracy Of Rayleigh-Rice Polarization Factors To Improve Microfacet Brdf Models, Rachel L. Wolfgang
Theses and Dissertations
Microfacet BRDF models assume that a surface has many small microfacets making up the roughness of the surface. Despite their computational simplicity in applications in remote sensing and scene generation, microfacet models lack the physical accuracy of wave optics models. In a previous work, Butler proposed to replace the Fresnel reflectance term of microfacet models with the Rayleigh-Rice polarization factor, Q, to create a more accurate model. This work examines the novel model that combines microfacet and wave optics terms for its accuracy in the pp and ss polarized cases individually. The model is fitted to the polarized data in …
The Design Of A Continuous Wave Molecular Nitrogen Stimulated Raman Laser In The Visible Spectrum, Timothy J. Bate
The Design Of A Continuous Wave Molecular Nitrogen Stimulated Raman Laser In The Visible Spectrum, Timothy J. Bate
Theses and Dissertations
Hollow-core photonic crystal fibers (HCPCFs) shows promise as a hybrid laser with higher nonlinear process limits and small beam size over long gain lengths. This work focuses on the design of a CW molecular nitrogen (N2) stimulated Raman laser. N2 offers Raman gains scaling up to 900 amg, scaling higher than H2. The cavity experiment showed the need to include Rayleigh scattering in the high pressure required for N2 Raman lasing. Even at relatively low pressure ssuch as 1,500 psi, high conversion percentages should be found if the fiber length is chosen based on …
Development Of A Model For 11C Production Via The 14N(P,Α) Reaction Using A Ge Pettrace Cyclotron, Amy C. Hall
Development Of A Model For 11C Production Via The 14N(P,Α) Reaction Using A Ge Pettrace Cyclotron, Amy C. Hall
Theses and Dissertations
The GE PETtrace 800 Series cyclotron at the Missouri University Research Reactor (MURR) facility is used extensively for medical and research radioisotope production. However, no model exists of its radioisotope production performance, and the energy, full intensity, and spatial profile of the cyclotron proton beam has never been measured. To improve production planning for research and medical isotopes, a MCNP6 model of the isotope production process was developed to maximize efficiency in target design and better understand irradiation conditions. Since the cyclotron beam energy and profile has a significant impact on the types of reactions that take place and the …
Luminescence In Lithium Borates, Brant T. Kananen
Luminescence In Lithium Borates, Brant T. Kananen
Theses and Dissertations
Spectrometry methods are used to identify and characterize point defects in single crystals of lithium tetraborate (Li2B4O7) and lithium triborate (LiB3O5) doped with silver or copper, and explore the role of these point defects in luminescence. New defects are identified in Ag-doped including: lithium vacancy substitutional-silver-ion defect-pairs (hole trap); isolated lithium vacancies (hole trap); isolated oxygen vacancies (electron trap); interstitial-silver-ion substitutional-silver-ion defect pairs (electron trap); isolated interstitial silver ions (electron trap); and interstitial-silver-ion lithium-vacancy defect pairs (electron trap). Defect models are proposed, and adjustments made to defect models known defects. …
Three-Dimensional Imaging Of Cold Atoms In A Magneto-Optical Trap With A Light Field Microscope, Gordon E. Lott
Three-Dimensional Imaging Of Cold Atoms In A Magneto-Optical Trap With A Light Field Microscope, Gordon E. Lott
Theses and Dissertations
Imaging of trapped atoms in three dimensions utilizing a light field microscope is demonstrated in this work. Such a system is of interest in the development of atom interferometer accelerometers in dynamic systems where strictly defined focal planes may be impractical. A light field microscope was constructed utilizing a Lytro® Development Kit micro-lens array and sensor. It was used to image fluorescing rubidium atoms in a magneto-optical trap. The three-dimensional (3D) volume of the atoms is reconstructed using a modeled point spread function (PSF), taking into consideration the low magnification (1.25) of the system which changed typical assumptions in the …
Special Features Of The Air-To-Space Neutron Transport Problem, Whitman T. Dailey
Special Features Of The Air-To-Space Neutron Transport Problem, Whitman T. Dailey
Theses and Dissertations
Special features of the air-to-space neutron transport problem are identified, characterized, and quantified to provide information on features that should be included in Monte Carlo simulations to obtain accurate predictions. Currently available codes and tools for Monte Carlo neutron transport calculations do not provide an adequate (in accuracy nor precision nor efficiency) framework for practical transport calculations in the context of the air-to-space neutron transport problem. A new Fortran code, High Altitude Transport to Space for Neutrons (HATS-n), is developed and tested to perform high fidelity Monte Carlo neutron transport calculations for this class of problems. Special features of the …
Coupling Nuclear Induced Phonon Propagation With Conversion Electron Mössbauer Spectroscopy, Michael J. Parker
Coupling Nuclear Induced Phonon Propagation With Conversion Electron Mössbauer Spectroscopy, Michael J. Parker
Theses and Dissertations
Mössbauer spectroscopy is a very sensitive measurement technique (10-8 eV) which prompted motivation for the experiment described in this thesis. Namely, can a sensitive detection system be developed to detect nuclear recoils on the order of 10 to 100 of eVs? The hypothesis that this thesis tests is: Nuclear induced phonon bursts caused by Rutherford scattered alphas, decayed from 241Am, in a type-310 stainless steel material can couple with 7.3 keV conversion electron Mössbauer events at the other end of the material which will have a statistically significant effect on a Mössbauer spectrum. The phonon bursts produced by …
An Experimental Evaluation Of Image Quality For Various Scenarios In A Chromotomographic System With A Spinning Prism, Kyle J. Dufaud
An Experimental Evaluation Of Image Quality For Various Scenarios In A Chromotomographic System With A Spinning Prism, Kyle J. Dufaud
Theses and Dissertations
A lab and eld based hyperspectral chromotomographic imager has been developed at the Air Force Institute of Technology. It is a prototype used to study the requirements for a space-based system. The imager uses a high speed visible band camera behind a direct-vision prism to image both spatial dimensions and the spectral dimension at the same time. Capturing all 3 simultaneously allows for the hyperspectral imaging of transient events. The prism multiplexes the spectral and spatial information, so tomographic reconstruction algorithms must be used to separate hyperspectral channels. Experiments were conducted to compare reconstructed image quality as a function of …
Distributed Spacing Stochastic Feature Selection And Its Application To Textile Classification, Jeffrey D. Clark
Distributed Spacing Stochastic Feature Selection And Its Application To Textile Classification, Jeffrey D. Clark
Theses and Dissertations
Many situations require the need to quickly and accurately locate dismounted individuals in a variety of environments. In conjunction with other dismount detection techniques, being able to detect and classify clothing (textiles) provides a more comprehensive and complete dismount characterization capability. Because textile classification depends on distinguishing between different material types, hyperspectral data, which consists of several hundred spectral channels sampled from a continuous electromagnetic spectrum, is used as a data source. However, a hyperspectral image generates vast amounts of information and can be computationally intractable to analyze. A primary means to reduce the computational complexity is to use feature …
Context Aided Tracking With Adaptive Hyperspectral Imagery, Andrew C. Rice
Context Aided Tracking With Adaptive Hyperspectral Imagery, Andrew C. Rice
Theses and Dissertations
A methodology for the context-aided tracking of ground vehicles in remote airborne imagery is developed in which a background model is inferred from hyperspectral imagery. The materials comprising the background of a scene are remotely identified and lead to this model. Two model formation processes are developed: a manual method, and method that exploits an emerging adaptive, multiple-object-spectrometer instrument. A semi-automated background modeling approach is shown to arrive at a reasonable background model with minimal operator intervention. A novel, adaptive, and autonomous approach uses a new type of adaptive hyperspectral sensor, and converges to a 66% correct background model in …
Cathodoluminescence Of Irradiated Hafnium Dioxide, Emily A. Purcell
Cathodoluminescence Of Irradiated Hafnium Dioxide, Emily A. Purcell
Theses and Dissertations
The purpose of this research is to understand the effect of radiation on HfO2 thin films, and to compare the quality of HfO2 thin films produced by both atomic layer deposition (ALD) and pulsed laser deposition (PLD); PLD samples had varying substrate temperatures during deposition (300°C, 500°C, and 750°C). The entirety of this research was conducted using cathodoluminescence (CL) as the examination method. The excitation source was a Kimball Physics EMG-12 electron gun. The photomultiplier tube contained a gallium arsenide photocathode. Measurements were made with beam energies ranging from 1 to 10 keV and beam currents ranging from …
Positron Annihilation Ratio Spectroscopy (Psars) Applied To Positronium Formation Studies, Robert C. Slaughter
Positron Annihilation Ratio Spectroscopy (Psars) Applied To Positronium Formation Studies, Robert C. Slaughter
Theses and Dissertations
A Positron Annihilation of Radiation Spectrometer (PsARS) was developed and characterized. PsARS spectroscopy as well as digital Positron Annihilation Lifetime Spectroscopy (PALS) was applied to measure positronium formation on gold nanoparticles deposited through an evaporative method onto a thin capillary tube. This gold coated capillary tube was designed to be used for positronium lifetime studies in local electric field experiments. High local electric fields can polarize a positron-electron pair, which may result in an extended lifetime of the positron. These fields may be created through the interaction of an external electric field with silver nanoparticles deposited onto the surface of …
Passive Ranging Using Infra-Red Atmospheric Attenuation, Douglas J. Macdonald
Passive Ranging Using Infra-Red Atmospheric Attenuation, Douglas J. Macdonald
Theses and Dissertations
Methods of estimating range to an emissive target based on the depth of an atmospheric absorption band are demonstrated. The present work uses measurements of the CO2 absorption band centered at 2.0 µm where signal-to-background ratios are maximum for many applications. Model results, based on high-resolution transmission molecular absorption (HITRAN) database cross sections, are used to predict range accuracy at ranges of up to 50 km and are compared with short range (<5km) experimental results. The spectra of 23 high explosive events were used to validate the model. Using the assumption of a blackbody spectrum, extracted ranges consistently underestimated the true range by approximately 13%. By incorporating the stoichiometry of the fireball from previous research and using particulate contribution as a parameter, the error for the range estimates could be reduced to 3%.
Scene Change Artifacts In Fourier Transform Spectroscopy Of Temporally Changing Sources, Anthony M. Young
Scene Change Artifacts In Fourier Transform Spectroscopy Of Temporally Changing Sources, Anthony M. Young
Theses and Dissertations
Improved understanding of midwave infrared (1-5 micron) spectral emissions from detonation fireballs is needed to develop phenomenological models for battle space optical forensics. The ability to measure radiance over a wide band pass at arbitrary resolutions make Fourier-transform spectrometers (FTS) an attractive tool. However, interferometer based spectroscopic measurements can be corrupted when the observed intensity changes during data acquisition. While small, random fluctuations in scene intensity translate into noise, systematic variations introduce scene-change artifacts (SCAs) into Fourier-transformed spectrum.
Hard Collisions In Rubidium Using Sub-Doppler Spectroscopy, Douglas E. Thornton
Hard Collisions In Rubidium Using Sub-Doppler Spectroscopy, Douglas E. Thornton
Theses and Dissertations
To better understand the laser kinetics of an alkali gain medium, hard collisions, or velocity-changing collisions, has been studied and a velocity-changing collisional rate has been calculated. Previous works have studied these collisions, but no rate has been calculated. Using the precise tool of sub-Doppler spectroscopy, atomic hard collisions can be observed. The collected spectra are fitted with two different line shapes to demonstrate the accuracy of this method. From the fits, the number of hard collisions can be extracted. The time scale of the hard collisions in rubidium is interpolated by varying the chopping frequency of the pump beam, …
Midwave Infrared Imaging Fourier Transform Spectrometry Of Combustion Plumes, Kenneth C. Bradley
Midwave Infrared Imaging Fourier Transform Spectrometry Of Combustion Plumes, Kenneth C. Bradley
Theses and Dissertations
A midwave infrared (MWIR) imaging Fourier transform spectrometer (IFTS) was used to successfully capture and analyze hyperspectral imagery of combustion plumes. Jet engine exhaust data from a small turbojet engine burning diesel fuel at a flow rate of 300 cm3/min was collected at 1 cm−1 resolution from a side-plume vantage point on a 200x64 pixel window at a range of 11.2 meters. Spectral features of water, CO, and CO2 were present, and showed spatial variability within the plume structure. An array of thermocouple probes was positioned within the plume to aid in temperature analysis. A single-temperature …