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Preparation, Spectroscopy, Antimicrobial Assay, And X-Ray Structure Of Dimethyl Bis-(4-Methylpiperidine Dithiocarbamato-S,S`)-Tin(Iv), Zia-Ur Rehman, Saira Shahzadi, Saqib Ali, Guo-Xin Jin
Preparation, Spectroscopy, Antimicrobial Assay, And X-Ray Structure Of Dimethyl Bis-(4-Methylpiperidine Dithiocarbamato-S,S`)-Tin(Iv), Zia-Ur Rehman, Saira Shahzadi, Saqib Ali, Guo-Xin Jin
Turkish Journal of Chemistry
Dimethyl bis(4-methylpiperidine dithiocarbamato-S,S')-tin(IV) was synthesized and characterized by elemental analysis, IR and mass spectrometry, multinuclear NMR (^1H- and ^{13}C-NMR), and X-ray single crystal analysis. IR data showed that the ligand acts as a bidentate in the solid state. X-ray data showed the unsymmetrical nature of the ligand towards coordination to tin. It crystallized in the monoclinic P2_1/n space group. Its geometry is distorted octahedral. Antimicrobial activity data shows that the complex exhibits significantly more activity than the free ligand.