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Technological University Dublin

Masters

1999

Articles 1 - 2 of 2

Full-Text Articles in Chemistry

The Development And Validation Of A Methodology For The Analysis Of Polyaromatic Hydrocarbons In Air Particulates (Indoor And Outdoor), Kathryn O'Malley Jan 1999

The Development And Validation Of A Methodology For The Analysis Of Polyaromatic Hydrocarbons In Air Particulates (Indoor And Outdoor), Kathryn O'Malley

Masters

PAH form a large class of ubiquitous pollutants mainly of anthropogenic origin. Several PAH found in air particulates have been identified as carcinogens and mutagens. Sixteen of these PAH have been listed by the USEPA as priority pollutants. This research is concerned with the development and optimisation of a method for the analysis of these sixteen PAH in air particulates. Soxhlet and ultrasonic extraction procedures were investigated to optimise the recoveries from spiked glass fibre filters with a standard 1ppm mixture of the 16PAH. Standard mixtures of the 16 PAH were analysed by HPLC with fluorescence detection with approx. linearity …


Studies On The Amylolytic Breakdown Of Damaged Starch In Cereal And Non-Cereal Flours, Karen Bailey Jan 1999

Studies On The Amylolytic Breakdown Of Damaged Starch In Cereal And Non-Cereal Flours, Karen Bailey

Masters

The term starch damage refers to a number of changes to the starch granule structure, which are detectable by different analytical techniques. Damaged starch is the substrate for amylases, which in turn provides carbohydrates that are used in the production of certain foods and food ingredients; as a result, therefore, determination of levels in flours is a procedure carried out routinely by many manufacturers of starch based products. Enzymatic assay methods emulate the susceptibility of damaged starch granules to enzymatic attack. The first aim of this study was to evaluate enzymatic methods(1,2) to determine damaged starch in wheat flours and …