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Old Dominion University

Virginia Journal of Science

2022

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Using Ftir-Atr And Chemometric Methods To Detect Sucrose Adulteration In Commercial Honey Samples, Dylan T. Roberts, Kevin Kittredge Oct 2022

Using Ftir-Atr And Chemometric Methods To Detect Sucrose Adulteration In Commercial Honey Samples, Dylan T. Roberts, Kevin Kittredge

Virginia Journal of Science

Fourier transform infrared spectroscopy-attenuated total reflectance (FTIR–ATR) was used to analyze pure and adulterated honey samples. The FTIR spectra was analyzed using principal component analysis (PCA) and partial least squares (PLS) regression analysis to determine if these methods could differentiate between pure, commercial, and sucrose-adulterated honey samples. PCA showed a clear distinction between pure and adulterated honey samples. Commercial honey samples showed clustering around the unadulterated samples. PLS regression analysis correctly identified 81.8% of the standards and samples used in the PCA analysis. The five commercial samples were tested and shown to have a concentration of less than 3% adulterant, …