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2009

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Full-Text Articles in Physical Sciences and Mathematics

Improved Synthesis Of Pincer Ligand Precursor, And Synthesis And Structural Characterization Of Terphenyl Scaffolded S–C–S Palladium Pincer Complex., Paul Schroder, Thomas Spilker, Wilson Luu, James Updegraff, Man Lung Kwan, Paul Challen, John Protasiewicz May 2013

Improved Synthesis Of Pincer Ligand Precursor, And Synthesis And Structural Characterization Of Terphenyl Scaffolded S–C–S Palladium Pincer Complex., Paul Schroder, Thomas Spilker, Wilson Luu, James Updegraff, Man Lung Kwan, Paul Challen, John Protasiewicz

Man Lung Desmond Kwan

An easier and more expedient synthesis of 2,6-(BrCH2C6H4)2-4-I-C6H3 (2) is reported. This material allowed easy synthesis of the new pincer ligand precursor 2,6-(4-CH3C6H4SCH2C6H4)2-4-I-C6H3 (3) in 87% yield. Compound 3 reacts with Pd2(dba)3 to give the new palladium pincer complex 4. Compound 4 has been fully characterized, including structural characterization by single crystal X-ray diffraction methods. The results of the crystallographic work on 4 reveal a twisted type pincer complex not unlike related terphenyl pincer complexes.

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The European Court Of Human Rights Ruling Against Britain's Policy Of Keeping Fingerprints & Dna Samples Of Criminal Suspects, K. Michael, Clive Harfield Feb 2013

The European Court Of Human Rights Ruling Against Britain's Policy Of Keeping Fingerprints & Dna Samples Of Criminal Suspects, K. Michael, Clive Harfield

Clive Harfield

In England and Wales, the Police and Criminal Evidence Act 1984 (the PACE) contained powers for the taking of fingerprints, and samples in the form of deoxyribonucleic acid (DNA). In 2001, Section 64(1A) of the PACE was substituted with Section 82 of the Criminal Justice and Police Act. The change to legislation meant that a suspect of a crime would have their fingerprints and samples permanently stored on the police national computer (PNC) even after having been acquitted. This paper critically analyses the circumstances of the landmark case of S. AND MARPER V. THE UNITED KINGDOM in two different contexts …

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Improved Synthesis Of Pincer Ligand Precursor, And Synthesis And Structural Characterization Of Terphenyl Scaffolded S–C–S Palladium Pincer Complex., Paul Schroder, Thomas Spilker, Wilson Luu, James Updegraff, Man Lung Kwan, Paul Challen, John Protasiewicz Nov 2009

Improved Synthesis Of Pincer Ligand Precursor, And Synthesis And Structural Characterization Of Terphenyl Scaffolded S–C–S Palladium Pincer Complex., Paul Schroder, Thomas Spilker, Wilson Luu, James Updegraff, Man Lung Kwan, Paul Challen, John Protasiewicz

Paul R. Challen

An easier and more expedient synthesis of 2,6-(BrCH2C6H4)2-4-I-C6H3 (2) is reported. This material allowed easy synthesis of the new pincer ligand precursor 2,6-(4-CH3C6H4SCH2C6H4)2-4-I-C6H3 (3) in 87% yield. Compound 3 reacts with Pd2(dba)3 to give the new palladium pincer complex 4. Compound 4 has been fully characterized, including structural characterization by single crystal X-ray diffraction methods. The results of the crystallographic work on 4 reveal a twisted type pincer complex not unlike related terphenyl pincer complexes.

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Polarimetry Studies For The Npdgamma Experiment At The Sns, Jonny Dadras Nov 2009

Polarimetry Studies For The Npdgamma Experiment At The Sns, Jonny Dadras

Jonny Dadras

The NPDGamma collaboration aims to measure a parity-violating directional gamma-ray asymmetry from the capture of polarized cold neutrons on protons. The asymmetry, predicted to be on the order of 50 ppb, is a result of the weak interaction between mesons and nucleons during the neutron capture reaction. The experiment is designed to make a statistics limited measurement of the asymmetry at the level of about 20%. The experiment will be carried out at the Fundamental neutron Physics Beamline (FnPB) at the Spallation Neutron Source (SNS). The neutron beam is polarized by a super-mirror polarizer. A 9.5 G magnetic field guides …

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Measurements Of Electron Density, Temperature And Photoionization Cross Sections Of The Excited States Of Neon In A Discharge Plasma, Shaukat Mahmood, Nek Shaikh, M. Kalyar, Naveed Piracha, M. Baig Oct 2009

Measurements Of Electron Density, Temperature And Photoionization Cross Sections Of The Excited States Of Neon In A Discharge Plasma, Shaukat Mahmood, Nek Shaikh, M. Kalyar, Naveed Piracha, M. Baig

Naveed K. Piracha

In the present work emission and absorption spectroscopy have been used to determine the plasma parameters of neon in a hollow cathode discharge lamp. The excitation temperature is determined using the intensity ratio method and Boltzmann’s plot method whereas the electron density is determined from the Stark broadening of the spectral lines. The behavior of the optogalvanic signal as a function of laser energy has been studied for three transitions from the 2p53s [1/2]2 metastable state following ΔJ=ΔK=0, ±1 dipole selection rules. The saturation technique has been used to measure the photoionization cross section from three intermediate states 2p53p′ [1/2]1, …

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One Million Downloads For Uow’S Research Online, Kate Mcilwain, Michael Organ, K. Michael, M. Michael Oct 2009

One Million Downloads For Uow’S Research Online, Kate Mcilwain, Michael Organ, K. Michael, M. Michael

Michael Organ

No abstract provided.

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Zincast-1: A Photochemically Active Chelator For Zn2+, Shawn Burdette, Celina Gwizdala, Daniel Kennedy Oct 2009

Zincast-1: A Photochemically Active Chelator For Zn2+, Shawn Burdette, Celina Gwizdala, Daniel Kennedy

Shawn C. Burdette

Two strategies were applied to the synthesis of ZinCast-1, a nitrobenzhydrol-based caged complex that upon photolysis exhibits a nearly 400-fold difference in binding for Zn2+.

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An Aztec 1.1mm Survey Of The Goods-N Field – Ii. Multiwavelength Identifications And Redshift Distribution, Thushara Perera, Edward Chapin, Alexandra Pope, Douglas Scott, Itziar Aretxaga, Jason Austermann, Ranga-Ram Chary, Kristen Coppin, Mark Halpern, David Hughes, James Lowenthal, Glenn Morrison, Kimberly Scott, Grant Wilson, Min Yun Sep 2009

An Aztec 1.1mm Survey Of The Goods-N Field – Ii. Multiwavelength Identifications And Redshift Distribution, Thushara Perera, Edward Chapin, Alexandra Pope, Douglas Scott, Itziar Aretxaga, Jason Austermann, Ranga-Ram Chary, Kristen Coppin, Mark Halpern, David Hughes, James Lowenthal, Glenn Morrison, Kimberly Scott, Grant Wilson, Min Yun

Thushara A. Perera

No abstract provided.

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Copula Density Estimation By Total Variation Penalized Likelihood, Leming Qu, Yi Qian, Hui Xie Sep 2009

Copula Density Estimation By Total Variation Penalized Likelihood, Leming Qu, Yi Qian, Hui Xie

Leming Qu

Copulas are full measures of dependence among random variables. They are increasingly popular among academics and practitioners in financial econometrics for modeling comovements between markets, risk factors, and other relevant variables. A copula's hidden dependence structure that couples a joint distribution with its marginals makes a parametric copula non-trivial. An approach to bivariate copula density estimation is introduced that is based on a penalized likelihood with a total variation penalty term. Adaptive choice of the amount of regularization is based on approximate Bayesian Information Criterion (BIC) type scores. Performance are evaluated through the Monte Carlo simulation.

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Impedance Differences Found With N-Alkanethiol Monolayers Prepared By Contact Printing And Solution Adsorption, Leslie Adamczyk, Mark Anderson Aug 2009

Impedance Differences Found With N-Alkanethiol Monolayers Prepared By Contact Printing And Solution Adsorption, Leslie Adamczyk, Mark Anderson

Mark R. Anderson

Self-assembled monolayers (SAMs) of n-octadecanethiol, n-dodecanethiol and n-pentanethiol formed by contact printing and solution adsorption are characterized by electrochemical impedance spectroscopy (EIS). Impedance measurements show that monolayers prepared by contact printing are on the order of 5 times less resistive to charge transfer and have greater defect density than monolayers prepared by solution adsorption. Modeling of the average defect size and density show that the size of monolayer defects stays relatively constant independent of the monolayer preparation conditions; however, the density of defects decreases with increasing concentration for the contact printed monolayers. The impedance data also show that monolayers prepared …

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Correction To “The Theory Of Quaternion Orthogonal Designs”, Tadeusz Wysocki, Beata Wysocki, Sarah Spence Adams Jul 2009

Correction To “The Theory Of Quaternion Orthogonal Designs”, Tadeusz Wysocki, Beata Wysocki, Sarah Spence Adams

Sarah Spence Adams

Seberry et al. claimed that even though the dual-polarized transmission channel cannot be considered as described by means of a single quaternionic gain, the maximum-likelihood (ML) decoding rule can be decoupled for orthogonal space–time-polarization block codes (OSTPBCs) derived from quaternion orthogonal designs (QODs) [1, Sec. IV]. Regretfully, a correction is necessary, and we will show that decoupled decoding using the method presented therein is only optimal for codes derived from certain QODs, not from arbitrary QODs as previously suggested.

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The Spectroelectrochemical, Magnetic, And Structural Characterization Of Reduced Hexaazatriphenylenehexacarbonitrile, Hat(Cn)6., Joseph Gallegos, Anthony Francis, Nathan Ockwig, Paul Rasmussen, Raphael Raptis, Paul Challen, Issouf Ouedraogo Jul 2009

The Spectroelectrochemical, Magnetic, And Structural Characterization Of Reduced Hexaazatriphenylenehexacarbonitrile, Hat(Cn)6., Joseph Gallegos, Anthony Francis, Nathan Ockwig, Paul Rasmussen, Raphael Raptis, Paul Challen, Issouf Ouedraogo

Paul R. Challen

The cyanoazacarbon, hexaazatriphenylenehexacarbonitrile, or HAT(CN)6, is readily reduced and the spectroelectrochemical properties associated with the multiple reductions are described. The singly reduced radical monoanion forms stable salts and we report the crystal structure and magnetic properties for the tetrabutylammonium salt. [Tetra-n-butylammonium] [HAT(CN)6] behaves ferromagnetically below 3K and follows Curie Law behavior at higher temperatures after correction for Pauli-type susceptibility. The room temperature conductivity of the powdered salt is 3.8×10−8S/cm. The crystal structure shows closely bound pairs of radical anions with slip-stacking of these pairs to form a staircase, features that elucidate the observed properties. Thin films of HAT(CN)6 were found …

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Wavelet Deconvolution In A Periodic Setting Using Cross-Validation, Leming Qu, Partha Routh, Kyungduk Ko Jul 2009

Wavelet Deconvolution In A Periodic Setting Using Cross-Validation, Leming Qu, Partha Routh, Kyungduk Ko

Kyungduk Ko

The wavelet deconvolution method WaveD using band-limited wavelets offers both theoretical and computational advantages over traditional compactly supported wavelets. The translation-invariant WaveD with a fast algorithm improves further. The twofold cross-validation method for choosing the threshold parameter and the finest resolution level in WaveD is introduced. The algorithm’s performance is compared with the fixed constant tuning and the default tuning in WaveD.

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Bayesian Wavelet-Based Methods For The Detection Of Multiple Changes Of The Long Memory Parameter, Kyungduk Ko Jul 2009

Bayesian Wavelet-Based Methods For The Detection Of Multiple Changes Of The Long Memory Parameter, Kyungduk Ko

Kyungduk Ko

Long memory processes are widely used in many scientific fields, such as economics, physics, and engineering. Change point detection problems have received considerable attention in the literature because of their wide range of possible applications. Here we describe a wavelet-based Bayesian procedure for the estimation and location of multiple change points in the long memory parameter of Gaussian autoregressive fractionally integrated moving average models (ARFIMA(p, d, q)), with unknown autoregressive and moving average parameters. Our methodology allows the number of change points to be unknown. The reversible jump Markov chain Monte Carlo algorithm is used for posterior inference. The method …

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Geochemical Partitioning Of Copper, Lead And Zinc In Benthic, Estuarine Sediment Profiles, Edward Burton, Ian Phillips, Darryl Hawker Jul 2009

Geochemical Partitioning Of Copper, Lead And Zinc In Benthic, Estuarine Sediment Profiles, Edward Burton, Ian Phillips, Darryl Hawker

Associate Professor Edward D Burton

Received for publication May 11, 2004. The geochemical partitioning of copper (Cu), lead (Pb), and zinc (Zn) was examined in benthic sediment profiles (0- to 20-cm depth interval) composed of relatively coarse (65–90% sand-sized particles), noncohesive, suboxic material (Eh +120 to +260 mV). Total Cu, Pb, and Zn concentrations ranged from 8.3 to 194, 16.3 to 74.8, and 30.1 to 220 mg/kg, respectively, and were related to vertical trends in sediment texture. The observed distribution coefficients describing solid–solution partitioning were in the range of 100 to 1000 L/kg. The geochemical partitioning of solid-phase Cu, Pb, and Zn between six operationally …

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Reactive Sulphide Relationships With Trace Metal Extractability In Sediments From Southern Moreton Bay, Australia, Edward Burton, Ian Phillips, Darryl Hawker Jul 2009

Reactive Sulphide Relationships With Trace Metal Extractability In Sediments From Southern Moreton Bay, Australia, Edward Burton, Ian Phillips, Darryl Hawker

Associate Professor Edward D Burton

No abstract provided.

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Distribution And Enrichment Of Trace Metals In Benthic, Estuarine Sediments: Southport Broadwater, Australia, Edward Burton, Ian Phillips, Darryl Hawker Jul 2009

Distribution And Enrichment Of Trace Metals In Benthic, Estuarine Sediments: Southport Broadwater, Australia, Edward Burton, Ian Phillips, Darryl Hawker

Associate Professor Edward D Burton

The distribution and enrichment of selected trace metals (Cd, Cr, Cu, Ni, Pb, Sn, Zn) in benthic sediments of the Southport Broadwater, a semi-enclosed coastal body of water adjacent to the Gold Coast city, south-eastern Queensland, Australia, was studied with the objective of assessing the extent and degree of sediment contamination. Sediment samples from the 0–10 cm and 10–20 cm depth intervals of 32 sites within the Southport Broadwater and surrounding residential canals were analysed for particle size distribution, pH, organic C and ‘near-total’ major (Al, Ca, Fe, Mn) and trace (Cd, Cr, Cu, Ni, Pb, Sn, Zn) metal contents. …

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Nutrient Leaching In Undisturbed Cores Of An Acidic Sandy Podosol Following Simultaneous Potassium Chloride And Di-Ammonium Phosphate Application, Ian Phillips, Edward Burton Jul 2009

Nutrient Leaching In Undisturbed Cores Of An Acidic Sandy Podosol Following Simultaneous Potassium Chloride And Di-Ammonium Phosphate Application, Ian Phillips, Edward Burton

Associate Professor Edward D Burton

In south-east Queensland, Australia, extensive areas of sandy soils (Podosols) with shallow (<1>m) watertables are used for exotic pine tree production. Despite concerns that surface-applied fertilisers (di-ammonium phosphate (DAP) and potassium chloride (KCl)) may be contributing to a decline in local groundwater quality, published information on nutrient leaching in these Podosols is scarce. Large (0.3 m i.d. · 0.85 m long) undisturbed soil cores were intermittently leached with deionised water following a single surface application of KCl in combination with DAP. Potassium was applied at rates (equivalent on a surface area basis) of 0 (K0), 50 (K50), 100 (K100) …

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Copper Behaviour In A Podosol. Ii: Sorption Reversibility, Geochemical Partitioning And Column Leaching, Edward Burton, Ian Phillips, Darryl Hawker, Dane Lamb Jul 2009

Copper Behaviour In A Podosol. Ii: Sorption Reversibility, Geochemical Partitioning And Column Leaching, Edward Burton, Ian Phillips, Darryl Hawker, Dane Lamb

Associate Professor Edward D Burton

The sorption–desorption and leaching behaviour of Cu in a Podosol from south-east Queensland, Australia, was examined. Copper sorption was described by a linear distribution coefficient at low sorption levels (KDCa→0) of 481 L/kg and a sorption capacity (CS,Max) of 382 mg/kg. Selective removal of soil organic matter reduced these values by approximately 95%, indicating that Cu was sorbed predominantly to soil organic matter. The KDCa→0 and CS,Max values from Cu desorption experiments were 934 L/kg and 516 mg/kg, respectively, which indicates that sorption was not fully reversible. This irreversibility was related to …

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Copper Behaviour In A Podosol. I: Ph-Dependent Sorption-Desorption, Sorption Isotherm Analysis And Aqueous Speciation Modelling, Edward Burton, Ian Phillips, Darryl Hawker, Dane Lamb Jul 2009

Copper Behaviour In A Podosol. I: Ph-Dependent Sorption-Desorption, Sorption Isotherm Analysis And Aqueous Speciation Modelling, Edward Burton, Ian Phillips, Darryl Hawker, Dane Lamb

Associate Professor Edward D Burton

The effects of pH and Cu loading on the solid/solution partitioning of Cu in a Podosol from south-east Queensland, Australia was examined. Sorption–desorption of Cu exhibited maximum linear distribution coefficients (KD) at approximately pH 5. Observed decrease in KD values at pH >5 was attributed to increased solubility of native dissolved organic carbon (DOC) at higher pH and subsequent formation of non-sorbing Cu–DOC complexes. Speciation modelling with the MINTEQA2 code indicated that >90% of aqueous Cu was present as Cu–DOC complexes at pH >5.5. The effect of Cu loading was examined with sorption isotherm analysis at pH …

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Ligand-Dependent Effects On The Conformational Equilibrium Of The Na+,K+-Atpase As Monitored By Voltage Clamp Fluorometry, Robert Dempski, Stefan Geys, Ernst Bamberg Jun 2009

Ligand-Dependent Effects On The Conformational Equilibrium Of The Na+,K+-Atpase As Monitored By Voltage Clamp Fluorometry, Robert Dempski, Stefan Geys, Ernst Bamberg

Robert E. Dempski

Voltage clamp fluorometry was used to monitor conformational changes associated with electrogenic partial reactions of the Na(+),K(+)-ATPase after changes in the concentration of internal sodium (Na(+)(i)) or external potassium (K(+)(o)). To probe the effects of the Na(+)(i) concentration on the Na(+) branch of the Na(+),K(+)-ATPase, oocytes were depleted of Na(+)(i) and then loaded with external sodium (Na(+)(o)) using the amiloride-sensitive epithelial sodium channel. The K(+) branch of the Na(+),K(+)-ATPase was studied by exposing the oocytes to different K(+)(o) concentrations in the presence and absence of Na(+)(o) to obtain additional information on the apparent affinity for K(+)(o). Our results demonstrate that …

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The Study Of The 1s4–2pj Optogalvanic Transients In A Neon Discharge Plasma, Naveed Piracha, R. Feaver, T. Gilani, Rizwan Ahmed, R. Ali, M. Baig Jun 2009

The Study Of The 1s4–2pj Optogalvanic Transients In A Neon Discharge Plasma, Naveed Piracha, R. Feaver, T. Gilani, Rizwan Ahmed, R. Ali, M. Baig

Naveed K. Piracha

Time dependent optogalvanic signals induced by the 1s4→2pj laser excitations have been studied in neon DC plasma. The decay rates related to all the four 1si levels have been derived by fitting the waveforms with a mathematical rate equation model. The temporal signatures of three transitions namely 638.3, 650.7 and 724.5nm related to the 2p7, 2p8 and 2p10 upper levels, respectively, have been found to be different from the rest of the transitions. We relate these effects to the population redistribution of decaying channels and to the processes responsible for the optogalvanic effect.

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Numerical Studies Of A Nonlinear Heat Equation With Square Root Reaction Term, Ron Buckmire, Karl Mcmurtry, Ronald Mickens Apr 2009

Numerical Studies Of A Nonlinear Heat Equation With Square Root Reaction Term, Ron Buckmire, Karl Mcmurtry, Ronald Mickens

Ron Buckmire

Interest in calculating numerical solutions of a highly nonlinear parabolic partial differential equation with fractional power diffusion and dissipative terms motivated our investigation of a heat equation having a square root nonlinear reaction term. The original equation occurs in the study of plasma behavior in fusion physics. We begin by examining the numerical behavior of the ordinary differential equation obtained by dropping the diffusion term. The results from this simpler case are then used to construct nonstandard finite difference schemes for the partial differential equation. A variety of numerical results are obtained and analyzed, along with a comparison to the …

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Simulation Of Ultrashort Laser Pulse Propagation And Plasma Generation In Nonlinear Media. Dissertation, Jeremy Gulley Apr 2009

Simulation Of Ultrashort Laser Pulse Propagation And Plasma Generation In Nonlinear Media. Dissertation, Jeremy Gulley

Jeremy R. Gulley

In this dissertation, a modified nonlinear Schrödinger equation is derived, which describes the propagation of ultrashort laser pulses through nonlinear materials in which plasma generation and laser-induced damage can occur. Differences between this model and models currently used in the literature are investigated and analyzed by numerical simulations. Ultrafast laser-induced material modification is investigated using this method by simulating the propagation of fully 3+1D (3 spatial plus 1 time dimension) laser pulses, which are numerically constructed from experimentally measured beam profiles and pulse shape data. The latest of these investigations reveals that standard rate-equation models for the free-electron plasma generation …

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Mountain Building Across A Lithospheric Boundary During Arc Construction: The Cretaceous Peninsular Ranges Batholith In The Sierra San Pedro Martir Of Baja California, Mexico, K Schmidt, S Paterson, Ann Blythe, C Kopf Apr 2009

Mountain Building Across A Lithospheric Boundary During Arc Construction: The Cretaceous Peninsular Ranges Batholith In The Sierra San Pedro Martir Of Baja California, Mexico, K Schmidt, S Paterson, Ann Blythe, C Kopf

Ann Blythe

The Jura-Cretaceous Peninsular Ranges batholith (PRB) of Southern and Baja California contains a remarkable example of variation in crustal composition and structure across a batholith-parallel lithospheric-scale discontinuity. This lithospheric boundary between western oceanic-floored and eastern continental-floored crust influenced contractional deformation, arc magmatism, and differential exhumation of western and eastern zones in the batholith during its evolution. In the Sierra San Pedro Martir of Baja California, Mexico, a ca. 20 km wide, doubly vergent fan structure occurs across the PRB basement transition that consists of inward-dipping mylonite thrust sheets on the sides of the fan that gradually transition to a steeply-dipping …

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Homologation Of Α-Amino Acids To Β-Amino Acids Via A Modified Arndt-Eistert Synthesis, Brian Brennan, James Carolan, '10 Apr 2009

Homologation Of Α-Amino Acids To Β-Amino Acids Via A Modified Arndt-Eistert Synthesis, Brian Brennan, James Carolan, '10

Brian B. Brennan

No abstract provided.

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Utilizing Phage Display To Identify Novel Peptides That Bind To Sickle Cell Hemoglobin, Brian Brennan, Chris Betzle, '10 Apr 2009

Utilizing Phage Display To Identify Novel Peptides That Bind To Sickle Cell Hemoglobin, Brian Brennan, Chris Betzle, '10

Brian B. Brennan

No abstract provided.

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The Development Of A Novel Therapeutic For The Treatment Of Sickle Cell Disease, Brian Brennan, Steven Sturlis, '10 Apr 2009

The Development Of A Novel Therapeutic For The Treatment Of Sickle Cell Disease, Brian Brennan, Steven Sturlis, '10

Brian B. Brennan

No abstract provided.

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Novel Therapeutics In The Treatment Of Sickle Cell Disease: Expression And Purification Of Hemoglobin And Sickle Cell Hemoglobin, Brian Brennan, Susan Zhong, '11 Apr 2009

Novel Therapeutics In The Treatment Of Sickle Cell Disease: Expression And Purification Of Hemoglobin And Sickle Cell Hemoglobin, Brian Brennan, Susan Zhong, '11

Brian B. Brennan

No abstract provided.

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Utilizing Phage Display To Identify Novel Peptides That Bind To Sickle Cell Hemoglobin, Brian Brennan, Chris Betzle, '10 Apr 2009

Utilizing Phage Display To Identify Novel Peptides That Bind To Sickle Cell Hemoglobin, Brian Brennan, Chris Betzle, '10

Brian B. Brennan

No abstract provided.

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