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Utah State University

Scanning electron microscopy

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Full-Text Articles in Physical Sciences and Mathematics

The Density Factor In The Synthesis Of Carbon Nanotube Forest By Injection Chemical Vapor Deposition, Robert W. Call, C. Read, C Mart, T. C. Shen Jan 2012

The Density Factor In The Synthesis Of Carbon Nanotube Forest By Injection Chemical Vapor Deposition, Robert W. Call, C. Read, C Mart, T. C. Shen

Graduate Student Publications

Beneath the seeming straight-forwardness of growing carbon nanotube(CNT) forests by the injection chemical vapor deposition(CVD) method, control of the forest morphology on various substrates is yet to be achieved. Using ferrocene dissolved in xylene as the precursor, we demonstrate that the concentration of ferrocene and the injection rate of the precursor dictate the CNT density of these forests. However, CNT density will also be affected by the substrates and the growth temperature which determine the diffusion of the catalyst adatoms. The CNT growth rate is controlled by the temperature and chemical composition of the gases in the CVD reactor. We …


Scanning Electron Microscopic Analysis Of Rock Varnish Chemistry For Cation-Ratio Dating: An Examination Of Electron Beam Penetration Depths, Steven L. Reneau, Roland C. Hagan, Charles D. Harrington, Robert Raymond Jr. Jan 1991

Scanning Electron Microscopic Analysis Of Rock Varnish Chemistry For Cation-Ratio Dating: An Examination Of Electron Beam Penetration Depths, Steven L. Reneau, Roland C. Hagan, Charles D. Harrington, Robert Raymond Jr.

Scanning Microscopy

Rock varnish is a microns-thick manganese- and iron-rich coating that forms on exposed rock surfaces in arid and semi-arid environments, and empirical correlations of the varnish cation ratio (K+Ca):Ti with age have been used to estimate ages of geomorphic surfaces. One method of obtaining varnish chemistry for cation-ratio dating involves scanning electron microscope (SEM) energy dispersive x-ray (EDX) analysis of natural varnish surfaces. The chemical analyses of rock varnish with SEM/EDX utilize a sequence of accelerating voltages to vary penetration depths into the sample. Using elemental x-ray maps of natural varnish surfaces obtained by SEM/EDX analysis, penetration into the substrate …


Barium Concentration In Rock Varnish: Implications For Calibrated Rock Varnish Dating Curves, C. D. Harrington, D. J. Krier, R. Raymond Jr., S. L. Reneau Jan 1991

Barium Concentration In Rock Varnish: Implications For Calibrated Rock Varnish Dating Curves, C. D. Harrington, D. J. Krier, R. Raymond Jr., S. L. Reneau

Scanning Microscopy

Cation-ratio dating of rock varnish is a recently developed technique for obtaining surface exposure ages of a wide variety of geomorphic surfaces. As originally proposed, the technique utilizes a ratio among minor cations [(K+Ca)/Ti] in rock varnish. Although this varnish cation ratio is related to the Ti concentration, it can also be affected by the presence of Ba that may be partially included in the analyzed concentration of Ti. Barium is a minor constituent found in virtually all rock varnishes sampled from the Lake Mead area, Las Vegas Valley, and the Crater Flat region of southern Nevada. Barium is heterogeneously …


A Loading Device For Fracture Testing Of Compact Tension Specimens In The Scanning Electron Microscope, Jügen Rödel, James F. Kelly, Mark R. Stoudt, Stephen J. Bennison Oct 1990

A Loading Device For Fracture Testing Of Compact Tension Specimens In The Scanning Electron Microscope, Jügen Rödel, James F. Kelly, Mark R. Stoudt, Stephen J. Bennison

Scanning Microscopy

A loading device for performing fracture experiments on compact tension specimens in the SEM has been designed. Its key elements are a piezoelectric translator for applying controlled displacements to the loading points on the specimen and a load cell to measure applied loads. The effective transmission of displacement from the piezoelectric driver to the specimen was found to be the major mechanical design problem. The peripheral equipment includes a function generator and a high voltage amplifier that drives the piezoelectric translator as well as a video overlay and standard video equipment to record the image continuously during the course of …