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Physical Sciences and Mathematics Commons

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Physics

Utah State University

Scanning electron microscopy

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Full-Text Articles in Physical Sciences and Mathematics

The Density Factor In The Synthesis Of Carbon Nanotube Forest By Injection Chemical Vapor Deposition, Robert W. Call, C. Read, C Mart, T. C. Shen Jan 2012

The Density Factor In The Synthesis Of Carbon Nanotube Forest By Injection Chemical Vapor Deposition, Robert W. Call, C. Read, C Mart, T. C. Shen

Graduate Student Publications

Beneath the seeming straight-forwardness of growing carbon nanotube(CNT) forests by the injection chemical vapor deposition(CVD) method, control of the forest morphology on various substrates is yet to be achieved. Using ferrocene dissolved in xylene as the precursor, we demonstrate that the concentration of ferrocene and the injection rate of the precursor dictate the CNT density of these forests. However, CNT density will also be affected by the substrates and the growth temperature which determine the diffusion of the catalyst adatoms. The CNT growth rate is controlled by the temperature and chemical composition of the gases in the CVD reactor. We …


A Loading Device For Fracture Testing Of Compact Tension Specimens In The Scanning Electron Microscope, Jügen Rödel, James F. Kelly, Mark R. Stoudt, Stephen J. Bennison Oct 1990

A Loading Device For Fracture Testing Of Compact Tension Specimens In The Scanning Electron Microscope, Jügen Rödel, James F. Kelly, Mark R. Stoudt, Stephen J. Bennison

Scanning Microscopy

A loading device for performing fracture experiments on compact tension specimens in the SEM has been designed. Its key elements are a piezoelectric translator for applying controlled displacements to the loading points on the specimen and a load cell to measure applied loads. The effective transmission of displacement from the piezoelectric driver to the specimen was found to be the major mechanical design problem. The peripheral equipment includes a function generator and a high voltage amplifier that drives the piezoelectric translator as well as a video overlay and standard video equipment to record the image continuously during the course of …