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Zeolite Linde Type L As Micro-Solid Phase Extraction Sorbent For The High Performance Liquid Chromatography Determination Of Ochratoxin A In Coffee And Cereal, Eng-Poh Ng Dr. Jan 2012

Zeolite Linde Type L As Micro-Solid Phase Extraction Sorbent For The High Performance Liquid Chromatography Determination Of Ochratoxin A In Coffee And Cereal, Eng-Poh Ng Dr.

Eng-Poh Ng

Zeolite Linde Type L (LTL) crystals with different length, diameter and particle size (nanosized LTL, rod LTL, cylinder LTL and needle LTL) were synthesized, characterized and were used as sorbent in the micro-solid phase extraction of ochratoxin A (OTA) before the high performance liquid chromatography detection. Under the optimized conditions, the detection limits of OTA for coffee and cereal were 0.09 ng g−1 and 0.03 ng g−1, respectively, while the quantification limits were 0.28 ng g−1 and 0.08 ng g−1, respectively. The recoveries of OTA of coffee and cereal spiked at 0.5, 10 and 25 ng g−1 ranged from 91.7 …


Capturing Ultrasmall Emt Zeolite From Template-Free Systems, Eng-Poh Ng Dr. Jan 2012

Capturing Ultrasmall Emt Zeolite From Template-Free Systems, Eng-Poh Ng Dr.

Eng-Poh Ng

No abstract provided.