Nanoscience and Nanotechnology Commons^™

Microparticle Propulsion For In Vivo Navigation, Louis Rogowski

Mechanical Engineering Research Theses and Dissertations

Microscale propulsion impacts a diverse array of fields, with simplistic microrobots allowing for novel innovations in microscale surgery and drug delivery. Propulsion at the microscale is constrained by physics, with time-reversal and geometric symmetries limiting available propulsion mechanisms. However, certain fluid environments and surface coatings allow for the propulsion of microparticles through externally applied magnetic fields. Presented here is a detailed analysis of microparticles propelling using spontaneous symmetry breaking, flagella surface coatings, and multi-modal actuation mechanisms. Spontaneous symmetry breaking in nonlinearly viscoelastic fluids is presented for the first time in literature, with two equal and opposite propulsion states existing along …

Interface Engineering Of Materials For Energy And Biological Applications, Ardalan Chaichi

LSU Doctoral Dissertations

Interface interactions are generally classified into solid-liquid, solid-gas, solid-vacuum, liquid-gas, light-matter and electron-matter categories. Surface morphological studies as well as surface chemical reactions can be studied in various types of complex systems thanks to technological advances in materials characterization methods. By employing interface engineering in different applications, it is possible to control electrical, chemical, mechanical, optical and biological properties of materials. Accordingly, we have applied interface engineering in three different areas of energy materials, biomaterials and surface imaging. As a result, firstly, we have introduced a high intensity light flash-based method on engineered substrates for delamination of reduced graphene oxide …

The Varied Thermal Response Of Magnetic Iron-Oxide Nanoparticles During Induction Heating In Liquid And Solid-Liquid Phase Change Mediums, Joshua Tompkins

Graduate Theses and Dissertations

This study investigates the induction heating response of uncapped iron oxide nanoparticles sonically dispersed as a nanofluid and mechanically distributed in solid phase change materials. The nanoparticles examined have a mean diameter of 14.42 nm and are magnetically heated in an alternating magnetic field at an amplitude of 72.6 kA/m at frequencies of 217, 303, and 397 kHz. Nanoparticle characterization was undertaken through transition electron microscopy, x-ray diffraction, and dynamic light scattering when in suspension. Carrier fluids were characterized through viscosity, heat capacity, and density measurements which were used in the calorimetric calculation of the specific absorption rate (SAR) of …

Sustainable Drug Release From Polycaprolactone Coated Chitin‑Lignin Gel Fibrous Scaffolds, Turdimuhammad Abdullah, Kalamegam Gauthaman, Azadeh Mostafavi, Ahmed Alshahrie, Numan Salah, Pierfrancesco Morganti, Angelo Chianese, Ali Tamayol, Adnan Memic

Department of Mechanical and Materials Engineering: Faculty Publications

Non-healing wounds have placed an enormous stress on both patients and healthcare systems worldwide. Severe complications induced by these wounds can lead to limb amputation or even death and urgently require more effective treatments. Electrospun scaffolds have great potential for improving wound healing treatments by providing controlled drug delivery. Previously, we developed fibrous scaffolds from complex carbohydrate polymers [i.e. chitin-lignin (CL) gels]. However, their application was limited by solubility and undesirable burst drug release. Here, a coaxial electrospinning is applied to encapsulate the CL gels with polycaprolactone (PCL). Presence of a PCL shell layer thus provides longer shelf-life for the …

Modulating Mechanical Properties Of Polymer Composites Via Colloidal Particle Reinforcement, Yusheng Guo

LSU Master's Theses

Additive manufacturing allows the rapid process of complex objects with excellent design flexibility. However, the products often exhibit poor mechanical properties when pure polymer is applied as printable material. In this work, we demonstrate that printability of polymer can be dramatically improved when particle filler is added to form reinforced polymer composites. Furthermore, the interaction between filler and polymer matrix leads to the enhancement in mechanical properties of the printed product. The material reinforcement induced by addition of fillers enables the wide application of polymer composites to print structures with unique features. In the printing of silica-reinforced pNIPAM composite, we …

Optimal Control Of Active Nematics, Michael M. Norton, Piyush Grover, Michael F. Hagan, Seth Fraden

Department of Mechanical and Materials Engineering: Faculty Publications

In this work we present the first systematic framework to sculpt active nematic systems, using optimal control theory and a hydrodynamic model of active nematics. We demonstrate the use of two different control fields, (i) applied vorticity and (ii) activity strength, to shape the dynamics of an extensile active nematic that is confined to a disk. In the absence of control inputs, the system exhibits two attractors, clockwise and counterclockwise circulating states characterized by two co-rotating topological þ1 2 defects. We specifically seek spatiotemporal inputs that switch the system from one attractor to the other; we also examine phase-shifting perturbations. …

Microfluidic Systems With Embedded Cell Culture Chambers For High Throughput Biological Assays, Arian Jaberi, Amir Monemian Esfahani, Fariba Aghabaglou, Jae Sung Park, Sidy Ndao, Ali Tamayol, Ruiguo Yang

Department of Mechanical and Materials Engineering: Faculty Publications

The ability to generate chemical and mechanical gradients on chips is important both for creating biomimetic designs or enabling high-throughput assays. However, there is still a significant knowledge gap in the generation of mechanical and chemical gradients in a single device. In this study, we developed gradient-generating microfluidic circuits with integrated microchambers to allow cell culture and to introduce chemical and mechanical gradients to cultured cells. A chemical gradient is generated across the microchambers, exposing cells to a uniform concentration of drugs. The embedded microchamber also produces a mechanical gradient in the form of varied shear stresses induced upon cells …

Study On The Chemical And Mechanical Stability Of Polymer Nanofluidic Biosensors, Dae Won Kim

LSU Master's Theses

Polymer nanofluidic devices have great potential to replace silicon (Si) and glass-based nanofluidic devices in biomedical applications due to their advantages such as low material and fabrication cost, various physicochemical properties, well-developed surface modification protocol, and low electrical noises for electrical measurements. In nanofluidic sensing applications, single molecules such as DNA are introduced into the fabricated nanochannel or nanopore, measuring their physicochemical properties optically or electrically. The properties of materials for nanofluidic devices have a significant role in the performance of the devices, such as DNA translocation and device stability.

Among several nanoscale fluidic physics, surface charge density is a …

Comparison Of Plantar Pressure Profile Of Young Adults During Training On Elliptical Devices And Overground Walking: A Pilot Study, Guilherme Manna Cesar, Thad W. Buster, Judith M. Burnfield

Department of Mechanical and Materials Engineering: Faculty Publications

Background: Elliptical training may offer advantages over other cardiorespiratory exercises for those requiring podiatric care, since its constant double-limb support diminishes recurring high-impact plantar forces while allowing exercise in a functional, upright posture. Unknown is the impact of distinct elliptical models, that can alter user’s body mechanics, on potential variations in plantar pressure patterns.

Purpose: To compare plantar pressure variables while exercising on four ellipticals and walking.

Methods: For this cross-sectional pilot study, plantar pressure data were recorded from ten young adults while exercising on four ellipticals (True, Octane, Life Fitness, SportsArt) and walking overground. One-way repeated measures ANOVA identified …

Magnetically Induced Carrier Distribution In A Composite Rod Of Piezoelectric Semiconductors And Piezomagnetics, Guolin Wang, Jinxi Liu, Wenjie Feng, Jiashi Yang

Department of Mechanical and Materials Engineering: Faculty Publications

In this work, we study the behavior of a composite rod consisting of a piezoelectric semiconductor layer and two piezomagnetic layers under an applied axial magnetic field. Based on the phenomenological theories of piezoelectric semiconductors and piezomagnetics, a one-dimensional model is developed from which an analytical solution is obtained. The explicit expressions of the coupled fields and the numerical results show that an axially applied magnetic field produces extensional deformation through piezomagnetic coupling, the extension then produces polarization through piezoelectric coupling, and the polarization then causes the redistribution of mobile charges. Thus, the composite rod exhibits a coupling between the …

Lstm-Based Anomaly Detection For Non-Linear Dynamical System, Yue Tan, Chungjing Hu, Kuan Zhang, Kan Zeng, Ethan A. Davis, Jae Sung Park

Department of Mechanical and Materials Engineering: Faculty Publications

Anomaly detection for non-linear dynamical system plays an important role in ensuring the system stability. However, it is usually complex and has to be solved by large-scale simulation which requires extensive computing resources. In this paper, we propose a novel anomaly detection scheme in non-linear dynamical system based on Long Short-Term Memory (LSTM) to capture complex temporal changes of the time sequence and make multi-step predictions. Specifically, we first present the framework of LSTM-based anomaly detection in non-linear dynamical system, including data preprocessing, multi-step prediction and anomaly detection. According to the prediction requirement, two types of training modes are explored …

Quantifying Wicking In Functionlized Surfaces, Maureen Winter, Ryan Regan, Alfred Tsubaki, Craig Zuhlke, Dennis Alexander, George Gogos

UCARE Research Products

Wicking remains the enigmatic key factor in many research areas. From boiling in power plants, to anti-icing on plane wings, to medical instruments, to heat pipes, efficiency and safety depend on how quickly a surface becomes wet. Yet wicking remains difficult to quantify and define as a property of the surface. This experiment strives to measure the wicking property by examining the rate that a liquid can be pulled out of a container. A superhydrophilic surface is placed in contact with the liquid at the bottom of a tube so that the volume flow rate across the surface can be …

A Wirelessly Controlled Smart Bandage With 3d-Printed Miniaturized Needle Arrays, Hossein Derakhshandeh, Fariba Aghabaglou, Alec Mccarthy, Azadeh Mostafavi, Chris Wiseman, Zack Bonick, Ian Ghanavati, Seth Harris, Craig Kreikemeier-Bower, Seyed Masoud Moosavi Basri, Jordan Rosenbohm, Ruiguo Yang, Pooria Mostafalu, Dennis Orgill, Ali Tamayol

Department of Mechanical and Materials Engineering: Faculty Publications

PUBLIC ACCESS

Cycle-To-Cycle Flow Variations In A Square Duct With A Symmetrically Oscillating Constriction, Erica Sherman, Lori M. Lambert, Bethany White, Michael H. Krane, Timothy Wei

Department of Mechanical and Materials Engineering: Faculty Publications

Spatially and temporally resolved Digital Particle Image Velocimetry (DPIV) measurements are presented of flow complexities in a nominally two-dimensional, symmetric, duct with an oscillating constriction. The motivation for this research lies in advancing the state-of-the-art in applying integral control volume analysis to modeling unsteady internal flows. The specific target is acoustic modeling of human phonation. The integral mass and momentum equations are directly coupled to the acoustic equations and provide quantitative insight into acoustic source strengths in addition to the dynamics of the fluid-structure interactions in the glottis. In this study, a square cross-section duct was constructed with symmetric, computer …

Multiscale Modeling Of Carbon Fibers/Graphene Nanoplatelets/Epoxy Hybrid Composites For Aerospace Applications, Hashim Al Mahmud

Dissertations, Master's Theses and Master's Reports

Significant research effort has been dedicated for decades to improve the mechanical properties of aerospace polymer-based composite materials. Lightweight epoxy-based composite materials have increasingly replaced the comparatively heavy and expensive metal alloys used in aeronautical and aerospace structural components. In particular, carbon fibers (CF)/graphene nanoplatelets (GNP)/epoxy hybrid composites can be used for this purpose owing to their high specific stiffness and strength. Therefore, this work has been completed to design, predict, and optimize the effective mechanical properties of CF/GNP/epoxy composite materials at different length scales using a multiscale modeling approach. The work-flow of modeling involves a first step of using …

Nanothermomechanical And And Or Logic Gates, Ahmed Hamed, Sidy Ndao

Department of Mechanical and Materials Engineering: Faculty Publications

Today’s electronics cannot perform in harsh environments (e.g., elevated temperatures and ionizing radiation environments) found in many engineering applications. Based on the coupling between near-field thermal radiation and MEMS thermal actuation, we presented the design and modeling of NanoThermoMechanical AND, OR, and NOT logic gates as an alternative, and showed their ability to be combined into a full thermal adder to perform complex operations. in this work, we introduce the fabrication and characterization of the first ever documented Thermal AND and OR logic gates. Theresults show thermal logic operations can be achieved successfully through demonstrated and easy-to- manufacture nanothermoMechanical logic …

Variations In Plantar Pressure Variables Across Elliptical Trainers In Older Adults, Judith M. Burnfield, Guilherme Manna Cesar, Thad W. Buster

Department of Mechanical and Materials Engineering: Faculty Publications

Background: Ellipticals are used to address walking and cardiorespiratory training goals of older adults, some of whom are at risk for foot injuries. Variations in joint kinematics and muscle demands when using different ellipticals could lead to plantar pressure differences. This study explored plantar pressure variables during gait and use of four ellipticals.

Methods: Plantar pressures were recorded while 10 adults [68.1 (4.5) years] walked and used the True, Octane, Life Fitness, and SportsArt ellipticals. Repeated-measures ANOVAs (5 × 1) identified forefoot and heel differences across conditions.

Findings: Maximum forefoot forces and peak pressures were significantly lower than walking for …

Challenges In Path Planning Of High Energy Density Beams For Additive Manufacturing, Karunakaran K. P, Seema Negi, Arun Nambolan, Yogesh Patil, Milan Pandya, Sajan Kapil, Dmitriy Trushnikov, Michael P. Sealy, Alain Bernard

Department of Mechanical and Materials Engineering: Faculty Publications

As there are no cutting forces in High Energy Density (HED) beams like lasers and Electron Beam (EB), their speeds are limited only by their positioning systems. On the other hand, as the entire matrix of the 3D printed part has to be addressed by the thin beam in multiple passes in multiple layers, they have to travel several kilometers in tiny motions. Therefore, the acceleration of the motion system becomes the limiting factor than velocity or precision. The authors have proposed an area-filling strategy for EB to fill the layer with optimal squares to exploit analog and hardware computing. …

3d Printing Of Multilayered Scaffolds For Rotator Cuff Tendon Regeneration, Xiping Jiang, Shaohua Wu, Mitchell Kuss, Yunfan Kong, Wen Shi, Philipp N. Streubel, Tieshi Li, Bin Duan

Department of Mechanical and Materials Engineering: Faculty Publications

Repairing massive rotator cuff tendon defects remains a challenge due to the high retear rate after surgical intervention. 3D printing has emerged as a promising technique that enables the fabrication of engineered tissues with heterogeneous structures and mechanical properties, as well as controllable microenvironments for tendon regeneration. In this study, we developed a new strategy for rotator cuff tendon repair by combining a 3D printed scaffold of polylactic-co-glycolic acid (PLGA) with cell-laden collagen-fibrin hydrogels. We designed and fabricated two types of scaffolds: one featuring a separate layer-by-layer structure and another with a tri-layered structure as a whole. Uniaxial tensile tests …

Imparities Of Shear Avalanches Dynamic Evolution In A Metallic Glass, Yin Du, Qing Zhou, Qian Jia, Yidi Shi, Haifeng Wang, Jian Wang

Department of Mechanical and Materials Engineering: Faculty Publications

The imparities of shear avalanches dynamic evolution under nanoindentation originating from the soft regions and the stiff matrix were explored in a metallic glass by statistical and dynamic analysis. Upon the continuous indentation process, the dynamic state of the stiff matrix exhibits a transition from a chaotic behavior to a self-organized critical (SOC) behavior, whereas the soft regions are domi-nated by the SOC behavior throughout the indentation process. The mechanism was clarified by the evolution of the cut-off size of shear avalanches. These findings might advance our fundamental understanding of inhomogeneous deformation on microscale.

IMPACT STATEMENT The shear avalanches dynamic …

Foundry Sand Source Reduction Options: Life Cycle Assessment Evaluation, Samuel Ghormley, Robert Williams, Bruce Dvorak

Department of Mechanical and Materials Engineering: Faculty Publications

Foundries represent a significant part of the world’s economy and are a large consumer of energy and producer of solid waste. Sand-handling processes can use 5–10% of a foundry’s total energy. The goal of this research was to explore source reduction and waste minimization at a foundry, using both economic and Life Cycle Assessment (LCA) techniques to compare three secondary sand-reclamation options. LCA software modeled all sand processes at a mid-sized ferrous foundry in the USA. The LCA showed all secondary reclamation technologies, while more energy intensive at the foundry, lowered life cycle environmental impacts, including GHG emissions, ecotoxicity, and …

Fluid Mechanics Education Using Japanese Anime: Examples From “Castle In The Sky” By Hayao Miyazaki, Sangjin Ryu, Haipeng Zhang, Markeya S. Peteranetz, Tareq Daher

Department of Mechanical and Materials Engineering: Faculty Publications

Current K-12 and undergraduate student have grown up with constant exposure to visual popular culture (e.g., movies, TV programs, graphic novels, etc.). Because youth find pop culture references in the classroom to be engaging, many science and engineering instructors have shown that examples found in visual pop culture can be used to teach science and engineering concepts.1,2 One recent study on the efficay os using pop ulture for instruction found that high school studetns learning from graphic-novel styles comics acquired deeper understanding of complex subject matter and reported higher engagement with the instructional materials as compared to students learning from …

Rotating-Liquid-Based Hydrogel Bead Generator, Haipeng Zhang, Sangjin Ryu

Department of Mechanical and Materials Engineering: Faculty Publications

Hydrogel beads are widely used in various applications, but producing such beads often requires complicated devices. Instead, we propose an easy-to-adopt, cost effective, open source hydrogel bead generator. This generator consists of two modules. The first module rotates two immiscible liquids in rigid body motion: mineral oil as the continuous phase (CP) liquid on top, and a hydrogel cross-linking (CL) liquid at bottom. The second module injects a hydrogel pre-polymer solution as the dispersed phase (DP) liquid into the rotating CP liquid. As the DP liquid flows out of a syringe needle, its drops are pinched off by the shear …

Leidenfrost Droplet Microfluidics, Sidy Ndao, George Gogos, Dennis Alexander, Troy Anderson, Craig Zuhlke

Department of Mechanical and Materials Engineering: Faculty Publications

Systems and methods are described for propelling a liquid droplet in a Leidenforst state. A microfluidic device embodiment includes, but is not limited to, a solid structure having a patterned surface, the patterned surface including at least a first patterned region having a first Leidenfrost temperature with respect to a fluid, the first patterned region adjacent to the second patterned region, the first patterned region defining a path over which a droplet of the fluid is configured to travel in a Leidenfrost state.

Colocalized Sensing And Intelligent Computing In Micro-Sensors, Mohammad H. Hasan, Ali Al-Ramini, Eihab Abdel-Rahman, Roozbeh Jafari, Fadi Alsaleem

Department of Mechanical and Materials Engineering: Faculty Publications

This work presents an approach to delay-based reservoir computing (RC) at the sensor level without input modulation. It employs a time-multiplexed bias to maintain transience while utilizing either an electrical signal or an environmental signal (such as acceleration) as an unmodulated input signal. The proposed approach enables RC carried out by sufficiently nonlinear sensory elements, as we demonstrate using a single electrostatically actuated microelectromechanical system (MEMS) device. The MEMS sensor can perform colocalized sensing and computing with fewer electronics than traditional RC elements at the RC input (such as analog- to-digital and digital-to-analog converters). The performance of the MEMS RC …

Roboticdeviceswithonboard Control And Related Systems And Devices, Shane Michael Farritor, Erik Mumm, Philip Chu, Nishant Kumar, Jason Dumpert, Yutaka Tsutano

Department of Mechanical and Materials Engineering: Faculty Publications

The embodiments disclosed herein relate to various medical device components, including components that can be incorporated into robotic and/or in vivo medical devices. Certain embodiments include various modular medical devices for in vivo medical procedures.

Low- And High-Drag Intermittencies In Turbulent Channel Flows, Rishav Agrawal, Henry C.-H. Ng, Ethan A. Davis, Jae Sung Park, Michael D. Graham, David J.C. Dennis, Robert J. Poole

Department of Mechanical and Materials Engineering: Faculty Publications

Recent direct numerical simulations (DNS) and experiments in turbulent channel flow have found intermittent low- and high-drag events in Newtonian fluid flows, at Reτ = uτh/ν between 70 and 100, where uτ, h and ν are the friction velocity, channel half-height and kinematic viscosity, respectively. These intervals of low-drag and high-drag have been termed “hibernating” and “hyperactive”, respectively, and in this paper, a further investigation of these intermittent events is conducted using experimental and numerical techniques. For experiments, simultaneous measurements of wall shear stress and velocity are carried out in a channel flow facility using hot-film anemometry (HFA) and laser …

Role Of Interfacial Transition Zones In The Fracture Of Cu/V Nanolamellar Multilayers, Siyuan Wei, Shijian Zheng, Lifeng Zhang, Yue Liu, Jian Wang, Xianping Wang, Jiangwei Wang

Department of Mechanical and Materials Engineering: Faculty Publications

Plastic deformation and fracture behavior of Cu/V nanoscale metallic multilayers (NMMs) were systematically investigated through in situ transmission electron microscopy testing. Two different types of interfaces: sharp interfaces and interfacial transition zones (ITZs), formed in the as-fabricated Cu/V NMMs. Upon deformation, sharp interfaces and ITZs exert distinct influences on the fracture behavior of Cu/V NMMs. Sharp interfaces can impede the crack propagation by deflecting the crack propagation and blunting the crack tip, while the ITZs can induce microcracks and facilitate the fracture process. These findings shed light on the important roles of interface structures in the deformation of a broad …

An Overview Of Additive Manufacturing Technologies—A Review To Technical Synthesis In Numerical Study Of Selective Laser Melting, Abbas Razavykia, Eugenio Brusa, Cristiana Delprete, Reza Yavari

Department of Mechanical and Materials Engineering: Faculty Publications

Additive Manufacturing (AM) processes enable their deployment in broad applications from aerospace to art, design, and architecture. Part quality and performance are the main concerns during AM processes execution that the achievement of adequate characteristics can be guaranteed, considering a wide range of influencing factors, such as process parameters, material, environment, measurement, and operators training. Investigating the effects of not only the influential AM processes variables but also their interactions and coupled impacts are essential to process optimization which requires huge efforts to be made. Therefore, numerical simulation can be an effective tool that facilities the evaluation of the AM …

Characteristic Boundaries Associated With Three-Dimensional Twins In Hexagonal Metals, Shujuan Wang, Mingyu Gong, Rodney J. Mccabe, Laurent Capolungo, Jian Wang, Carlos N. Tomé

Department of Mechanical and Materials Engineering: Faculty Publications

Twinning is a critically important deformation mode in hexagonal close-packed metals. Twins are three-dimensional (3D) domains, whose growth is mediated by the motion of facets bounding the 3D twin domains and influences work hardening in metals. An understanding of twin transformations therefore necessitates that the atomic-scale structure and intrinsic mobilities of facets be known and characterized. The present work addresses the former point by systematically characterizing the boundary structures of 3D { ̄1012} twins in magnesium using high-resolution transmission electron microscopy (HRTEM). Eight characteristic facets associated with twin boundaries are reported, five of which have never been experimentally observed before. …