Mechanical Engineering Commons^™

Nd-Fe-B Nanoparticles Through Surfactant Assisted Mechanical Milling And Alloy Design, Jordann M. Bornhoft

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Surfactant-assisted mechanical milling has been used to produce discrete nanoparticles of both Nd-Fe-B and Sm-Co amenable for bottom-up production of nanostructured or nanocomposite permanent magnets. However, in Nd-Fe-B the comminution of the material proceeds by transgranular fracture, which influences both the morphology of the nanoparticles and the magnetic properties. This paper utilizes alloy design to alter the fracture behavior from transgranular fracture to intergranular fracture. Nd-rich Nd₂Fe₁₄B alloys were produced by melt spinning in an overquenched state. The melt spun ribbons were annealed at 700°C and 800°C to ensure complete crystallization and to form different grain …

Kolsky Bar Experiment For High-Rate Large Deformations Of Polycarbonate, Jason Gerald Vogeler

Department of Engineering Mechanics: Dissertations, Theses, and Student Research

Polycarbonate (PC) is a tough, transparent engineering thermoplastic. Its impact strength and ability undergo large plastic deformations without shatter make PC an ideal protective material for impact-resilient eyewear, aircraft windows and transparent armor. A good understanding of the response of this material to large deformations at high strain rates is critical for its utilization in these applications. To this end, a striker-less Kolsky bar device is employed in this work for the needed material characterization. The apparatus allow impulsive torsion and/or compression loadings with pulse durations sufficiently long for the plastic flow behavior to develop fully. Three new testing techniques …

Ultrasonic Propagation And Scattering In Pearlitic Steel, Hualong Du

Department of Engineering Mechanics: Dissertations, Theses, and Student Research

Diffuse ultrasonic backscatter measurements have been especially useful for extracting microstructural information and for improving flaw detection in materials. In this dissertation, this approach is applied to inspection of railroad wheels. To improve the wear resistance, the tread surfaces of railroad wheels are usually quenched with water to increase the hardness. The pearlite phase of iron, characterized by alternating ferrite and cementite phases, is created by the quenching and the lamellar spacing within grains increases progressively from the quenched tread surface to deeper locations due to the non-uniform cooling rate. The quench depth is an important parameter governing the wheel …

Structural & Magnetic Characterization Study Of Hfco7 Alloy With Substitutions Of Si, Ti, Fe, Mn & B, Jacob A. Lewis

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Magnetic materials are a critical component of the modern technological society. The market of high-energy product hard magnets is dominated by the rare-earth element containing neodymium-iron-boron (NdFeB) magnets. As a result of worldwide demand coupled with trade restrictions on rare-earth minerals, new magnet compositions are explored to reduce pressure on the already strained market. The hafnium-cobalt alloy system has shown promise as a candidate for filling the gap in saturation magnetization between rare-earth containing alloys and those made with abundant elements. This study explores the magnetic effects of silicon, titanium, iron, manganese and boron substitutions in the hafnium-cobalt-7 (1:7 atomic …

Experimental Study On The Effect Of Air Flow On Soap Bubble Formation, John M. Davidson

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Soap bubbles are a common interfacial fluid dynamics phenomenon having applications such as buoyant hollow spherical fillers and flow visualization of large scale airflows. In contrast to the dynamics of liquid drops in gas and gas bubbles in liquid, the dynamics of soap bubbles has not been well documented, possibly because soap bubbles have gas-liquid-gas interfaces. Having the thin-liquid-film interface seems to alter the characteristics of the bubble/drop creation process. Thus, the main objective of this study is to experimentally examine how airflow develops and interacts with the soap liquid film as the film stretches and finally collapses to pinch-off. …

Effects Of Time Varying Background Noise Conditions On Human Perception And Performance, Andrew H. Hathaway

Durham School of Architectural Engineering and Construction: Dissertations, Thesis, and Student Research

This thesis was designed to study the effects of changing noise conditions on human perception and performance. In two phases, participants were exposed to a number of noise conditions and their performance on an arithmetic task involving short-term memory was monitored and their subjective perception of noise conditions was collected via questionnaires.

In the first phase, participants were tested while being subjected to RC-29(H) and RC-47(RV) conditions created by broadband noise fluctuating on different time intervals, resembling the changing noise conditions potentially found in modern HVAC systems. These intervals varied from two minutes to ten minutes. Results show a significant …

Near-Infrared Surface-Enhanced Fluorescence Using Silver Nanoparticles In Solution, Michael D. Furtaw

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Fluorescence spectroscopy is a widely used detection technology in many research and clinical assays. Further improvement to assay sensitivity may enable earlier diagnosis of disease, novel biomarker discovery, and ultimately, improved outcomes of clinical care along with reduction in costs. Near-infrared, surface-enhanced fluorescence (NIR-SEF) is a promising approach to improve assay sensitivity via simultaneous increase in signal with a reduction in background. This dissertation describes research conducted with the overall goal to determine the extent to which fluorescence in solution may be enhanced by altering specific variables involved in the formation of plasmonactive nanostructures of dye-labeled protein and silver nanoparticles …

Ergonomichandle And Articulating Laparoscopictool, M. Susan Hallbeck, Dmitry Oleynikov, Kathryn Done, Tim Judkins, Allison Dimartino, Jonathan Morse, Lawton N. Verner

Department of Mechanical and Materials Engineering: Faculty Publications

The present invention relates to a laparoscopic apparatus. The apparatus includes a handle having a body portion, a top surface, opposite bottom surface, a proximal and distal end. The top surface of the base is contoured to compliment the natural curve of the palm. The apparatus further includes a shaft projecting from the distal end of the handle. The shaft has a proximal and distal end. A control sphere is located on the handle. The control sphere can be moved by one or more of a user's fingers to indicate direction. An end effector is located at the distal end …

Scalar Differential Equation For Slowly-Varying Thickness-Shear Modes In At-Cut Quartz Resonators With Surface Impedance For Acoustic Wave Sensor Application, Huijing He, Jiashi Yang, John A. Kosinski

Department of Mechanical and Materials Engineering: Faculty Publications

For time-harmonic motions, we generalize a 2-D scalar differential equation derived previously by Tiersten for slowly-varying thickness-shear vibrations of AT-cut quartz resonators. The purpose of the generalization is to include the effects of surface acoustic impedance from, e.g., mass layers or fluids for sensor applications. In addition to the variation of fields along the plate thickness, which is considered in the usual 1-D acoustic wave sensor models, the equation obtained also describes in-plane variations of the fields, and therefore can be used to study the vibrations of finite plate sensors with edge effects. The equation is compared with the theory …

A New Angle On Microscopic Suspension Feeders Near Boundaries, Rachel E. Pepper, Marcus Roper, Sangjin Ryu, Nobuyoshi Matsumoto, Moeto Nagai, Howard A. Stone

Department of Mechanical and Materials Engineering: Faculty Publications

Microscopic sessile suspension feeders are a critical component in aquatic ecosystems, acting as an intermediate trophic stage between bacteria and higher eukaryotic taxa. Because they live attached to boundaries, it has long been thought that recirculation of the feeding currents produced by sessile suspension feeders inhibits their ability to access fresh fluid. However, previous models for the feeding flows of these organisms assume that they feed by pushing fluid perpendicular to surfaces they live upon, whereas we observe that sessile suspension feeders often feed at an angle to these boundaries. Using experiments and calculations, we show that living suspension feeders …

Flow-Induced Crystallization Of Isotactic Polypropylene And Random Polyethylene-Polypropylene Copolymers, Frederic Aubin

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Flow-induced crystallization (FIC) has been investigated for decades but the effect of molecular characteristics that hinder crystallization—such as the presence of random comonomers— on FIC remains scarcely explored. Flow greatly enhances crystallization kinetics and can induce the formation of highly oriented morphologies that affect final properties (i.e. stiffness, permeability, thermal conductivity, elastic modulus, etc.). Therefore, understanding FIC remains particularly important for developing predictive models to allow optimization of processing techniques involving flows.

Polypropylene represents ~ 40% of the global polyolefin production. The addition of ethylene comonomer allows their use as engineering plastics because of their particular toughness and flexibility. This …

The Mechanics Of Intracranial Loading During Blast And Blunt Impacts – Experimental And Numerical Studies, Veera Selvan Kuppuswamy

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Head injuries in an explosion occur as a result of a sudden pressure changes (e.g. shock-blast) in the atmosphere (primary injury), high velocity impacts of debris (secondary injury) and people being thrown against the solid objects (tertiary injury) in the field. In this thesis, experimental and numerical approaches are used to delineate the intracranial loading mechanics of both primary (blast) and tertiary injuries (blunt).

The blast induced head injuries are simulated using a fluid-filled cylinder. This simplified model represents the head-brain complex and the model is subjected to a blast with the Friedlander waveform type of loading. We measured the …

Propagation Of Thermo-Mechanical Waves In Deforming Nonlinear Viscoelastic Bodies, Lili Zhang

Department of Engineering Mechanics: Dissertations, Theses, and Student Research

This work studies the propagation of thermo-mechanical disturbances in bodies made of viscoelastic materials that might already be loaded such that they are undergoing large inhomogeneous time varying deformations. In the process of this study we develop the general equations governing the thermo-mechanical motion of such disturbances and ones for internally constrained systems, provide the general structure of the solution, match the solution to existing results for the special case of time harmonic plane waves in elastic bodies and in viscoelastic bodies under constant homogenous loading, and consider some special applications.

The results of this work should have applications in …

Relaxation Of Shear-Induced Precursors In Isotactic Polypropylene And Random Propylene-Ethylene Copolymers, Benjamin Schammé

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Flow induced crystallization (FIC) has a large impact on kinetics and morphology of semicrystalline polymers, and can therefore drastically change final properties such as dimensional and thermal stability, modulus and strength. Processing of polymers usually involves flow, so it is important to understand the mechanism of FIC. It is known that oriented precursors formed during flow are the key to FIC but they are not yet well understood. In this study, flow induced precursors are investigated by examining their relaxation, and the effect of comonomer is probed.

Using a commercial isotactic polypropylene and random propylene-ethylene copolymers, a fiber pull-out technique …

Measurement And Description Of Dynamics Required For In Vivo Surgical Robotics Via Kinematic Methods, Jacob G. Greenburg

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

With the goal of improved recovery times and reduced trauma to the patient there has been a substantial shift in the medical community’s demand for minimally invasive surgical (MIS) techniques. With the standardization of MIS becoming more commonplace in the medical field there are still many improvements that are desired. Traditional, manual methods of these surgeries require multiple incisions on the abdomen for the tools and instruments to be inserted. The more recent demand has been to localize the incisions into what is being referred to as a Laparoendoscopic Single-Site (LESS) surgery. Furthermore, the manual instruments that are commonly used …

Interface Properties Of Bio-Based Composites Of Polylactic Acid And Bamboo Fibers, Quentin Viel

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Environmental impact plays an ever-increasing role in the industrial production of materials, and because of its importance, the scientific community is examining a wide variety of new materials that are more environmentally friendly. Bioplastics are characterized by the fact that the usual petrochemical resins (polypropylene, polyethylene etc.) are replaced by bio-sourced resins and the reinforcements (glass fibers, carbon fibers etc.) are replaced by natural fibers (bamboo, flax, cotton, etc.). Polylactic acid (PLA) is a biodegradable polymer that is increasingly used in biomedical applications and in packaging. Additionally, bamboo is a promising source of fibers that could be used as reinforcement. …

Development Of A Controllable Polymer System Using Interpenetrating Networks, Emilie Bobo

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

My research partners and I have studied the possibility of building a material system with controllable properties using two interpenetrating polymer networks (IPNs). This study is part of a project to build a rapid prototyping system that allows for the printing of objects with predefined spatial distribution of properties, with the goal that property distributions are controlled though interactions at the molecular level.

One can change the properties of an IPN by adjusting the ratio of interpenetrating networks present in a given cured mixture. This is similar to how one obtains different shades of the color green by gradually changing …

Investigation Of Sound Transmission Through An Open Window Into A Room, Caleb F. Sieck

Durham School of Architectural Engineering and Construction: Dissertations, Thesis, and Student Research

In recent decades, noise levels in cities and the associated annoyance and health consequences have become regular topics of discussion. As a result, the assessment of environmental noise transmitting into buildings has received much attention. Current models of sound transmission through open windows have either neglected their thickness or the presence of a room behind on one side. The objectives of the present work were to (1) develop an accurate analytical model of sound transmission through an open window of finite thickness into a room, (2) verify the analytical model using a finite element model and experimental measurements, and (3) …

Design Of A Compliant Underactuated Robotic Finger With Coordinated Stiffness, Etienne Dessauw

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

The concept of underactuation has been previously developed in the robotic field for grasping applications. For these anthropomorphic grippers, the minimization of the number of input signals, or in other words underactuation, is the most expected characteristic. This method has become very popular in recent decades. Indeed, by minimizing the number of input signals, it minimizes the complexity of the system’s control and at the same time avoids increased weight and cost. The inconvenience of such a technique is that the design of this type of system remains a difficult task if the behavior of the underactuated set of joints …

Developing And Characterizing A Rapid Prototyping Stereo-Lithography Machine To Produce Interpenetrating Polymer Network Systems, Lena R. Butterfield

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Rapid prototyping and interpenetrating network systems (IPNs) ideas and technologies were studied in order to develop a rapid prototyping machine capable of producing IPNs. This work was done as collaboration between the University of Nebraska-Lincoln and the University of Rouen, France, and is part of a project of controlling material property distribution by means of gradient IPN production within a rapid prototyping machine.

A standard stereo-lithography rapid prototyping (RP) machine was built and then modified for the purpose of producing an IPN system composed of an acrylic component, bisphenol A propoxylate diacrylate (BPA-PDA) and an epoxy component, 3,4 epoxycyclohexyl-methyl 3,4 …

Rating Low Levels Of Ambient Noise In Performing Arts Facilities, Lily M. Wang, Brent A. Kraay

Durham School of Architectural Engineering and Construction: Faculty Publications

Previous studies have indicated that common indoor noise rating metrics, such as Noise Criteria NC and Room Criteria RC, do not best correlate to human perceptions of annoyance and distraction in typical office environments. Based on investigations conducted at the University of Nebraska using noise levels between 30 – 60 dBA, the author has proposed that an effective indoor noise rating method should begin with a rating of level (either dBA or sones), then an assessment of spectral quality, tones, and fluctuations. How well would such a system work at very low levels of ambient noise, though, as found in …

Quantifying The Just Noticeable Difference Of Reverberation Time With Band-Limited Noise Centered Around 1000 Hz Using A Transformed Up-Down Adaptive Method, Matthew G. Blevins, Adam T. Buck, Zhao Peng, Lily M. Wang

Durham School of Architectural Engineering and Construction: Faculty Publications

This study seeks to quantify the just noticeable difference (JND) of reverberation time (RT) using band-limited noise. ISO 3382-1 lists the JND of reverberation metrics at 5% based on work by Seraphim (1958). However, others have found the JND of RT to be higher from 6% to 39%. Many of these studies utilized band-limited stimuli, e.g. speech, music motifs and bandlimited noise. A previous study by the authors conducted on 30 subjects using white noise demonstrated a JND of RT at 22%. To further verify these results and investigate potential upward frequency masking, the present study was conducted following the …

Effects Of Background Noise Alternating Between Two Levels At Varying Time Intervals On Human Perception And Performance, Andrew Hathaway, Lily M. Wang

Durham School of Architectural Engineering and Construction: Faculty Publications

This research experiment aims to better quantify human perception and performance under increased background noise levels of varying intervals. Twenty-seven participants were tested over five 30 minute sessions where they were subjected to RC-29(H) and RC-47(RV) conditions created by broadband noise fluctuating on different time intervals. These intervals varied from two minutes to ten minutes, simulating the conditions of a noisy HVAC system turning on and off. The performance results of an arithmetic test dealing with short-term memory and a subjective questionnaire will be presented and compared to a similar test using broadband noise bursts and correlated to noise metrics …

Effects Of Reverberation And Noise On Speech Comprehension By Native And Non-Native English-Speaking Listeners, Zhao Peng, Lily M. Wang, Siu Kit Lau, Adam M. Steinbach

Durham School of Architectural Engineering and Construction: Faculty Publications

Previous studies have demonstrated the negative impact of adverse signal-to-noise-ratios on non-native English-speaking listeners' performance on speech recognition using recall tasks, as well as implied that comprehension skills were more impaired than recognition skills under reverberation and noise. The authors have themselves previously conducted a pilot study on three native and three non-native Englishspeaking listeners to examine the effects of reverberation and noise using speech comprehension tasks. Those results suggested that speech comprehension performance is worse under longer reverberation times (RT), and that a longer RT is more detrimental to speech comprehension by non-native listeners than native listeners. This paper …

Thickness-Shear And Thickness-Twist Vibrations Of Circular At-Cut Quartz Resonators, Huijing He, Jiashi Yang, Qing Jiang

Department of Mechanical and Materials Engineering: Faculty Publications

Exact solutions for free vibration frequencies and modes are obtained for thickness-shear and thickness-twist vibrations of unelectroded circular AT-cut quartz plates governed by the two-dimensional scalar differential equation derived by Tiersten and Smythe. Comparisons are made with experimental results and the widely-used perturbation solution by Tiersten and Smythe under the assumption of weak in-plane anisotropy. Our solution is found to be much closer to the experimental results than the perturbation solution . For the frequency of the fundamental thickness- shear mode, the error of the perturbation method is 0.4549%, significant in resonator applications.

Experimental Assessment Of The Impact Of Asymptomatic Gas Emboli On The Vessel Wall, Linxia Gu, Eric L. Cutler

Department of Mechanical and Materials Engineering: Faculty Publications

Quantitative evaluation of shear stress in the vessel wall due to the presence of asymptomatic gas emboli is lacking. The goal of this work was to assess the impact of chronic asymptomatic gas emboli on the risk of atherosclerosis through a custom-built cardiovascular flow simulator. Gas bubbles were created by forced air from a syringe pump. The influences of embolism injection rate, pulse rate, and time-averaged flow rate on the wall mean shear stress were investigated at resting and elevated heart rate conditions. The recorded pressure and volumetric flow rate from 24 experimental settings with four repetitions each were used …

Zone Of Intrusion For Permanent 9.1-Degree Single Slope Concrete Barriers, Cale J. Stolle

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Three WDOT 9.1-degree single-slope concrete barriers, with top heights of 36 in. (914 mm), 42 in. (1,067 mm), and 56 in. (1,422 mm) (Standard 14B32), were analyzed for Zone of Intrusion (ZOI)’ and working width using nonlinear finite element analysis (FEA). Tire-barrier friction, vehicle-barrier friction, barrier stiffness, mesh size, tire deflation, and suspension component failures were all found to have effects on simulation results. The zone of intrusion and working width were evaluated for each barrier under varying tire deflation and suspension failure conditions and determined to have a maximum value of 12.2 in. (310 mm) for the front fender …

Design Of Experimental Methods To Test The Performance Of Pads And Helmets Under Blast Loading Conditions, Kurtis Palu

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Improvised explosive devices (IEDs) have become a primary weapon in conflicts against US and allied forces. Improvements in body armor and medicine have increased the survivability of such events. These factors have caused an increase in traumatic brain injury (TBI) and mild traumatic brain injury (mTBI) induced by primary blast waves. Injury mechanisms caused from primary blast waves are not clearly understood or defined. How primary blast waves interact with materials or between narrow gaps found between helmet pads is not known. Two novel test fixtures were developed to provide a basic understanding of these two issues.

The first fixture …

High-Resolution Correlation Spectroscopy Of 13c Spins Near A Nitrogen-Vacancy Centre In Diamond, Abdelghani Laraoui, Florian Dolde, Christian Burk, Friedemann Reinhard, Jorg Wrachtrup, Carlos A. Meriles

Department of Mechanical and Materials Engineering: Faculty Publications

Spin complexes comprising the nitrogen-vacancy centre and neighbouring spins are being considered as a building block for a new generation of spintronic and quantum information processing devices. As assembling identical spin clusters is difficult, new strategies are being developed to determine individual node structures with the highest precision. Here we use a pulse protocol to monitor the time evolution of the 13C ensemble in the vicinity of a nitrogenvacancy centre. We observe long-lived time correlations in the nuclear spin dynamics, limited by nitrogen-vacancy spin–lattice relaxation. We use the host 14N spin as a quantum register and demonstrate that hyperfine-shifted resonances …

Thickness-Shear Vibration Of A Rectangular Quartz Plate With Partial Electrodes, Huijing He, Jiashi Yang, John A. Kosinski, Ji Wang

Department of Mechanical and Materials Engineering: Faculty Publications

We study free vibration of a thickness-shear mode crystal resonator of AT-cut quartz. The resonator is a rectangular plate partially and symmetrically electroded at the center with rectangular electrodes. A single-mode, three-dimensional equation governing the thickness-shear displacement is used. A Fourier series solution is obtained. Numerical results calculated from the series show that there exist trapped thickness-shear modes whose vibration is mainly under the electrodes and decays rapidly outside the electrodes. The effects of the electrode size and thickness on the trapped modes are examined.