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Full-Text Articles in Mechanical Engineering
Structural Investigations On Nanocrystalline Ni-W Alloy Films By Transmission Electron Microscopy
Structural Investigations On Nanocrystalline Ni-W Alloy Films By Transmission Electron Microscopy
A.S. Md Abdul Haseeb
Electrodeposited Ni-W alloys have been investigated in the as-deposited state by transmission electron microscopy in order to investigate the microstructural features in dependence of the tungsten content. Within the tungsten content range from 7 at.% up to 12 at.%, the microstructure is nanocrystalline characterized by a bimodal grain size distribution, consisting out of 20 to 200 nm sized grains and also larger grains with several 100 nm characteristic dimension. No clear trend in microstructure formation is visible with W content or deposition conditions in the investigated W content range. Only solid solution phase characteristics were observed. The lattice constant is …
Thermal Stability Of Electrodeposited Liga Ni-W Alloys For High Temperature Mems Applications
Thermal Stability Of Electrodeposited Liga Ni-W Alloys For High Temperature Mems Applications
A.S. Md Abdul Haseeb
For thermally stable LIGA materials for high temperature MEMS applications LIGA Ni-W layers and micro testing samples with different compositions (15 and 5 at% W) were electrodeposited. In order to investigate the thermal stability the Ni-W layers were annealed at different temperatures (300-700°C) and for different durations (1, 4, 16 h). Their microstructure and micro-hardness were than analysed after annealing and compared with those of as-deposited states. The observed microstructures show, in comparison to pure LIGA nickel, a small grain growth and a relatively stable structure up to 700°C. The micro-hardness values of the LIGA Ni-W layers are higher than …
Xrd, Xps And Sims Investigations On Electrodeposited Nickel-Phosphorous Alloy Coatings
Xrd, Xps And Sims Investigations On Electrodeposited Nickel-Phosphorous Alloy Coatings
A.S. Md Abdul Haseeb
Structural and chemical investigations on electrodeposited nickel-phosphorous alloy coatings by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and secondary ion mass spectroscopy (SIMS) are described. Electrodeposition of nickel-phosphorous coatings has been carried out galvanostatically in a hypophosphite bath at two different current densities, namely 20 and 80 mA cm -2. XRD has shown a broad peak indicating an amorphous structure in both cases. XPS shows the presence of Ni 2P compound. XPS also reveals the amount of phosphorous in both coatings to be around 10.20 wt.%. SIMS has shown that the coating deposited at lower current density (20 mA cm …