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Mechanical Engineering Commons

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Interfaces (materials)

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Full-Text Articles in Mechanical Engineering

Stability Of Molybdenum Nanoparticles In Sn-3.8ag-0.7cu Solder During Multiple Reflow And Their Influence On Interfacial Intermetallic Compounds Feb 2012

Stability Of Molybdenum Nanoparticles In Sn-3.8ag-0.7cu Solder During Multiple Reflow And Their Influence On Interfacial Intermetallic Compounds

A.S. Md Abdul Haseeb

This work investigates the effects of molybdenum nanoparticles on the growth of interfacial intermetallic compound between Sn-3.8Ag-0.7Cu solder and copper substrate during multiple reflow. Molybdenum nanoparticles were mixed with Sn-3.8Ag-0.7Cu solder paste by manual mixing. Solder samples were reflowed on a copper substrate in a 250 °C reflow oven up to six times. The molybdenum content of the bulk solder was determined by inductive coupled plasma-optical emission spectrometry. It is found that upon the addition of molybdenum nanoparticles to Sn-3.8Ag-0.7Cu solder, the interfacial intermetallic compound thickness and scallop diameter decreases under all reflow conditions. Molybdenum nanoparticles do not appear to …


Xrd, Xps And Sims Investigations On Electrodeposited Nickel-Phosphorous Alloy Coatings Jan 1996

Xrd, Xps And Sims Investigations On Electrodeposited Nickel-Phosphorous Alloy Coatings

A.S. Md Abdul Haseeb

Structural and chemical investigations on electrodeposited nickel-phosphorous alloy coatings by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and secondary ion mass spectroscopy (SIMS) are described. Electrodeposition of nickel-phosphorous coatings has been carried out galvanostatically in a hypophosphite bath at two different current densities, namely 20 and 80 mA cm -2. XRD has shown a broad peak indicating an amorphous structure in both cases. XPS shows the presence of Ni 2P compound. XPS also reveals the amount of phosphorous in both coatings to be around 10.20 wt.%. SIMS has shown that the coating deposited at lower current density (20 mA cm …