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Full-Text Articles in Mechanical Engineering

A Bubble-Powered Micro-Rotor: Conception, Manufacturing, Assembly And Characterization, Jonathan Kao, Xiaolin Wang, John Warren, Jie Xu, Daniel Attinger Dec 2007

A Bubble-Powered Micro-Rotor: Conception, Manufacturing, Assembly And Characterization, Jonathan Kao, Xiaolin Wang, John Warren, Jie Xu, Daniel Attinger

Daniel Attinger

A steady fluid flow, called microstreaming, can be generated in the vicinity of a micro-bubble excited by ultrasound. In this paper, we use this phenomenon to assemble and power a microfabricated rotor at rotation speeds as high as 625 rpm. The extractible power is estimated to be of the order of a few femtowatts. A first series of experiments with uncontrolled rotor shapes is presented, demonstrating the possibility of this novel actuation scheme. A second series of experiments with 65 µm rotors micromanufactured in SU-8 resin is then presented. Variables controlling the rotation speed and rotor stability are investigated, such …


A Practical Guideline For Establishing Non-Return Valve Specification And Performance Criteria, Eric W. Dawkins Dec 2007

A Practical Guideline For Establishing Non-Return Valve Specification And Performance Criteria, Eric W. Dawkins

Masters Theses

The non-return valve has been a standard piece of equipment in the injection molding industry since the reciprocating screw was developed. Most molders understand the role of the non-return valve in the molding process. But few understand the functional problems of the non-return valve. Because of this, the non-return valve has been considered a nuisance item for injection molders.

Wear of the non-return valve is another problem that molders are faced with. The factors contributing toward wear are not entirely understood. Material, temperatures, hours and machine size, etc., all effect the life of a valve. Consequently, most worn valves are …


Designing And Manufacturing Microelectronic Packages For High-Power Light-Emitting Diodes, Brian Wright, Jianbiao Pan, Richard Savage Nov 2007

Designing And Manufacturing Microelectronic Packages For High-Power Light-Emitting Diodes, Brian Wright, Jianbiao Pan, Richard Savage

Industrial and Manufacturing Engineering

A new microelectronic package was designed for a high-power light-emitting diode (LED). The objective was to build a package that enables the LED to operate with currents as high as 2 Amps. An innovative thin-film interface has been developed to electrically connect the cathode of the LED die to a 22AWG Cu wire. This thin-film interface is wirebondable and solderable, and consists of three layers: Au, Ni93/V7, and Si. Four 1 mil Au wirebonds, supporting 2A of maximum current, connect the Au thin-film to the LED die cathode. Sn96Ag4 solder is used for connecting the Ni93/V7 thin-film to the 22AWG …


In-House Development Of Scheduling Decision Support Systems: Case Study For Scheduling Semiconductor Device Test Operations, Tali Freed, K. H. Doerr, T. Chang Nov 2007

In-House Development Of Scheduling Decision Support Systems: Case Study For Scheduling Semiconductor Device Test Operations, Tali Freed, K. H. Doerr, T. Chang

Industrial and Manufacturing Engineering

Most manufacturing processes can benefit from an automated scheduling system. However;: the design of a fast, computerised scheduling system that achieves high-quality results and requires minimal resources is a difficult undertaking. Efficient .. scheduling of a semiconductor device test facility requires an information system that provides good schedules quickly. Semiconductor device testing-is the last stage of the long semiconductor manufacturing process, and therefore. is subjected to customer service pressures. The cost of an off-the-shelf computerised scheduling system may he prohibitive for many companies. In addition, many companies are taken aback by other characteristics of off-the-shelf scheduling systems, such as code …


Fabrication Of Functionally Graded 3a/5a Zeolites By Electrophoretic Deposition, X. Wang, E. A. Olevsky, E. Bruce, M. B. Stern, D. T. Hayhurst Nov 2007

Fabrication Of Functionally Graded 3a/5a Zeolites By Electrophoretic Deposition, X. Wang, E. A. Olevsky, E. Bruce, M. B. Stern, D. T. Hayhurst

Industrial and Manufacturing Engineering

Functionally graded zeolites of molecular sieve type 3A and 5A are deposited by electrophoretic deposition (EPD) from acetone suspension with 8% volume concentration of n-butylamine as particle charging agent. The EPD characteristics of both 3A and 5A suspensions are studied. Functionally graded zeolite 3A/5A deposits are obtained at 200 V DC. Energy dispersive X-ray dispersion (EDX) analysis results confirm the graded structure. The deposited zeolites are also analysed by scanning electron microscopy (SEM). The factors influencing the deposition process are discussed.


The Benefits Of Automatic Data Collection In The Fresh Produce Supply Chain, Ryan Charles Panos, Tali Freed Sep 2007

The Benefits Of Automatic Data Collection In The Fresh Produce Supply Chain, Ryan Charles Panos, Tali Freed

Industrial and Manufacturing Engineering

The potential for RFID based systems to improve the safety and efficiency of a supply chain with rapidly decaying products and strict health standards is creating pressure to adopt RFID in several agricultural industries. A handful of fresh produce industry leaders currently participate in mandated pilot projects, while the industry as a whole is still intimidated by the perceived cost of RFID. Therefore in this study we attempt to validate the correlation between performance and automated data collection, paving the way to economic justification of investment in data collection technologies, such as barcode and RFID.

The majority of product in …


Experimental Investigation Of Effect Of Environment Temperature On Freeze-Form Extrusion Fabrication, Xiyue Zhao, Michael S. Mason, Tieshu Huang, Ming-Chuan Leu, Robert G. Landers, Greg Hilmas, Samuel J. Easley, Michael W. Hayes Aug 2007

Experimental Investigation Of Effect Of Environment Temperature On Freeze-Form Extrusion Fabrication, Xiyue Zhao, Michael S. Mason, Tieshu Huang, Ming-Chuan Leu, Robert G. Landers, Greg Hilmas, Samuel J. Easley, Michael W. Hayes

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Freeze-form Extrusion Fabrication (FEF) is an additive manufacturing technique that extrudes ceramic loaded aqueous pastes layer by layer below the paste freezing temperature for component fabrication. A computer controlled 3-D gantry system has been developed for the FEF process. The system includes a temperature control subsystem that allows for fabrication of components below the paste freezing temperature. The low temperature environment allows for larger component fabrication. Comparisons in terms of layer thickness, self-sustaining ability, and system response were performed between 0⁰C and -20⁰C for alumina sample fabrications. The minimum deposition angles without use of support material have been determined for …


Modeling And Validation Of Temperature And Concentration For Rapid Freeze Prototyping, Frances D. Bryant, Ming-Chuan Leu Aug 2007

Modeling And Validation Of Temperature And Concentration For Rapid Freeze Prototyping, Frances D. Bryant, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Rapid Freeze Prototyping is a solid freeform fabrication process that uses water as the main build material in a cold environment to create three-dimensional parts. A eutectic sugar-water solution (C6H12O6 – H2O) has been used as a sacrificial material in order to create complex 3D parts with features such as overhangs. A study of the interaction of the build and support materials is presented in this paper. The temperature of both materials during deposition and subsequent cooling is modeled using a semi-empirical model and a theoretical model. A concentration model is used to …


Thermocouple Embedding For The Production Of A Substrate For Rapid Manufacturing, Rana Gunaratnam, Todd E. Sparks, Frank W. Liou Aug 2007

Thermocouple Embedding For The Production Of A Substrate For Rapid Manufacturing, Rana Gunaratnam, Todd E. Sparks, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

This paper reports the results of a set of experiments testing methods to embed thermocouples during laser deposition. Various operating settings and shielding materials are explored. Temperature readings of the embedded thermocouples are compared with surface temperature readings taken by a non-contact digital pyrometer during the deposition process. Also, possibilities of using this information for system control are discussed.


Variable Powder Flow Rate Control In Laser Metal Deposition Processes, Lie Tang, Jianzhong Ruan, Robert G. Landers, Frank W. Liou Aug 2007

Variable Powder Flow Rate Control In Laser Metal Deposition Processes, Lie Tang, Jianzhong Ruan, Robert G. Landers, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

This paper proposes a novel technique, called Variable Powder Flow Rate Control (VPFRC), for the regulation of powder flow rate in laser metal deposition processes. The idea of VPFRC is to adjust the powder flow rate to maintain a uniform powder deposition per unit length even when disturbances occur (e.g., the motion system accelerates and decelerates). Dynamic models of the powder delivery system motor and the powder transport system (i.e., five-meter pipe, powder dispenser, and cladding head) are first constructed. A general tracking controller is then designed to track variable powder flow rate references. Since the powder flow rate at …


Modeling And Simulation Of A Laser Deposition Process, Frank W. Liou, Zhiqiang Fan, Heng Pan, Kevin P. Slattery, Mary Kinsella, Joseph William Newkirk, Hsin-Nan Chou Aug 2007

Modeling And Simulation Of A Laser Deposition Process, Frank W. Liou, Zhiqiang Fan, Heng Pan, Kevin P. Slattery, Mary Kinsella, Joseph William Newkirk, Hsin-Nan Chou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

A laser deposition process involves the supply of metallic powders into a laser-heated spot where the powder is melted and forms a melt puddle which quickly solidifies into a bead. In order to design an effective system, the laser beam, the powder beam, and their interactions need to be fully understood. In this paper, the laser-material interaction within the melt pool is reported using a multi-scale model: A macroscopic model to model mass, heat, and momentum transfer. Experiments were also conducted to validate the simulation model.


Aqueous-Based Extrusion Fabrication Of Ceramics On Demand, Michael S. Mason, Tieshu Huang, Robert G. Landers, Ming-Chuan Leu, Greg Hilmas, Michael W. Hayes Aug 2007

Aqueous-Based Extrusion Fabrication Of Ceramics On Demand, Michael S. Mason, Tieshu Huang, Robert G. Landers, Ming-Chuan Leu, Greg Hilmas, Michael W. Hayes

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Aqueous-Based Extrusion Fabrication is an additive manufacturing technique that extrudes ceramic slurries of high solids loading layer by layer for part fabrication. The material reservoir in a previously developed system has been modified to allow for starting and stopping of extrusion process on demand. Design pros and cons are examined and a comparison between two material reservoir designs is made. Tests were conducted to determine the optimal deposition parameters for starting and stopping of the extrudate on demand. The collected test data is used to create a process model that describes the relationship between ram velocity and material extrusion rate. …


Design Of Embedded Resistance Heating Element Using Rapid Manufacturing Process, Ravi Philip, Todd E. Sparks, Frank W. Liou Aug 2007

Design Of Embedded Resistance Heating Element Using Rapid Manufacturing Process, Ravi Philip, Todd E. Sparks, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

This paper discusses the design of heating element suitable for embedding in a rapid manufacturing process. A specific pattern is built using the laser deposition Process available at the University of Missouri--Rolla. A resistance heating element which is then cast into place using a castable refractory material, which acts as an electrical insulator. An application of this technology is for preheating the substrate before direct metal deposition.


Laser Deposition Cladding On-Line Inspection Using 3-D Scanner, Yu Yang, Todd E. Sparks, Jianzhong Ruan, Lan Ren, Frank W. Liou Aug 2007

Laser Deposition Cladding On-Line Inspection Using 3-D Scanner, Yu Yang, Todd E. Sparks, Jianzhong Ruan, Lan Ren, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Laser deposition directly deposits metal cladding to fabricate and repair components. In order to finish the fabrication or repair, 3-D shape of the deposition needs to be inspected, and thus it can be determined if it has sufficient cladding to fabricate a part after deposition process. In the present hybrid system in the Laser Aided Manufacturing Lab (LAMP) at the University of Missouri - Rolla, a CMM system is used to do the inspection. A CMM requires point-by-point contact, which is time consuming and difficult to plan for an irregular deposition geometry. Also, the CMM is a separate device, which …


Numerical Simulation Of The Evolution Of Solidification Microstructure In Laser Deposition, Zhiqiang Fan, Todd E. Sparks, Frank W. Liou, Anand Jambunathan, Yaxin Bao, Jianzhong Ruan, Joseph William Newkirk Aug 2007

Numerical Simulation Of The Evolution Of Solidification Microstructure In Laser Deposition, Zhiqiang Fan, Todd E. Sparks, Frank W. Liou, Anand Jambunathan, Yaxin Bao, Jianzhong Ruan, Joseph William Newkirk

Mechanical and Aerospace Engineering Faculty Research & Creative Works

A predictive model is developed to simulate the evolution of the solidification microstructure during the laser deposition process. The microstructure model is coupled with a comprehensive macroscopic thermodynamic model. This model simulates dendritic grain structures and morphological evolution in solidification. Based on the cellular automata approach, this microstructure model takes into account the heterogeneous nucleation both within the melt pool and at the substrate/melt interface, the growth kinetics, and preferential growth directions of dendrites. Both diffusion and convection effects are included. This model enables prediction and visualization of grain structures during and after the deposition process. This model is applied …


Comparing The Feasibility Of Cutting Thin-Walled Sections From Five Commonly Used Metals Utilizing Wire Electric Discharge Machining, Richard C. Stephenson Jul 2007

Comparing The Feasibility Of Cutting Thin-Walled Sections From Five Commonly Used Metals Utilizing Wire Electric Discharge Machining, Richard C. Stephenson

Theses and Dissertations

Wire Electric Discharge Machining (wire-EDM) is a non-traditional machining process. Controlled electric sparks are successively used to vaporize part of a workpiece along a programmed path in order to machine a desired part. Because there is no tool that comes in direct contact with the workpiece, it is possible to machine thin, delicate parts. This thesis was designed to observe and analyze the differences in cutting capabilities for a conventional wire-EDM machine when cutting thin-walled sections from five commonly used metals utilizing a variation of roughing and finishing passes. The five metals that were used in this study are: Aluminum …


Friction Stir Welding Of High-Strength Automotive Steel, Eric Michael Olsen Jul 2007

Friction Stir Welding Of High-Strength Automotive Steel, Eric Michael Olsen

Theses and Dissertations

The following thesis is a study on the ability to create acceptable welds in thin-plate, ultra-high-strength steels (UHSS) by way of friction stir welding (FSW). Steels are welded together to create tailor-welded blanks (TWB) for use in the automotive industry. Dual Phase (DP) 590, 780, and 980 steel as well as Transformation-Induced Plasticity (TRIP) 590 steel with thicknesses ranging from 1.2 mm to 1.8 mm were welded using friction stir welding under a variety of processing conditions, including experiments with dissimilar thicknesses. Samples were tested under tensile loads for initial determination if an acceptable weld had been created. Acceptable welds …


Fabrication Of Net-Shape Functionally Graded Composites By Electrophoretic Deposition And Sintering: Modeling And Experimentation, E.A. Olevsky, X. Wang, A. Maximenko, M.A. Meyers Jun 2007

Fabrication Of Net-Shape Functionally Graded Composites By Electrophoretic Deposition And Sintering: Modeling And Experimentation, E.A. Olevsky, X. Wang, A. Maximenko, M.A. Meyers

Industrial and Manufacturing Engineering

It is shown that electrophoretic deposition (EPD) sintering is a technological sequence that is capable of producing net-shape bulk functionally graded materials (FGM). By controlling the shape of the deposition electrode, components of complex shapes can be obtained. To enable sintering net-shape capabilities, a novel optimization algorithm and procedure for the fabrication of net-shape functionally graded composites by EPD and sintering has been developed. The initial shape of the green specimen produced by EPD is designed in such a way that the required final shape is achieved after sintering-imposed distortions. The optimization is based on a special innovative iteration procedure …


Modeling Of The Size Effects On The Behavior Of Metals In Microscale Deformation Processes, Gap-Yong Kim, Jun Ni, Muammer Koc Jun 2007

Modeling Of The Size Effects On The Behavior Of Metals In Microscale Deformation Processes, Gap-Yong Kim, Jun Ni, Muammer Koc

Gap-Yong Kim

For the accurate analysis and design of microforming process, proper modeling of material behavior at the micro/mesoscale is necessary by considering the size effects. Two size effects are known to exist in metallic materials. One is the “grain size” effect, and the other is the “feature/specimen size” effect. This study investigated the feature/specimen size effect and introduced a scaling model which combined both feature/specimen and grain size effects. Predicted size effects were compared with three separate experiments obtained from previous research: a simple compression with a round specimen, a simple tension with a round specimen, and a simple tension in …


Investigation Of The Lead-Free Solder Joint Shear Performance, James Webster, Jianbiao Pan, Brian J. Toleno Apr 2007

Investigation Of The Lead-Free Solder Joint Shear Performance, James Webster, Jianbiao Pan, Brian J. Toleno

Industrial and Manufacturing Engineering

Reflow profile has significant impact on solder joint performance because it influences wetting and microstructure of the solder joint. The purpose of this study is to investigate the effects of reflow profile and thermal shock on the shear performance of eutectic SnPb (SnPb) and Sn3.0Ag0.5Cu (SAC305) solder joints. Test boards were assembled with four different sized surface mount chip resistors (1206, 0805, 0603 and 0402). Nine reflow profiles for SAC 305 and nine reflow profiles for SnPb were developed with three levels of peak temperature (12ºC, 22ºC, and 32ºC above solder liquidus temperature, or 230ºC, 240ºC, and 250ºC for SAC …


"Minimizing Injuries Resulting From Patient Handling In Nursing Home Staff" - A Hazard Control Plan, Vikas Singh Apr 2007

"Minimizing Injuries Resulting From Patient Handling In Nursing Home Staff" - A Hazard Control Plan, Vikas Singh

Vikas Singh

A concise hazard control plan for "Minimizing Injuries Resulting from Patient Handling In Nursing Home Staff".


An Experimental Investigation On Semi-Solid Forming Of Micro/Meso-Scale Features, Gap-Yong Kim, Jun Ni, Rhett Mayor, Heesool Kim Apr 2007

An Experimental Investigation On Semi-Solid Forming Of Micro/Meso-Scale Features, Gap-Yong Kim, Jun Ni, Rhett Mayor, Heesool Kim

Gap-Yong Kim

The potentials of semi-solid forming technology have generated much interest regarding its application in micromanufacturing. This study investigates the feasibility of using semi-solid forming technology to produce parts with micro/meso features. An experimental setup has been developed to study the effects of die/punch temperature, initial solid fraction, punch speed, and workpiece shape on the semi-solid forming process. A part has been produced for a microreactor application and has been analyzed with an optical measurement system for feature formation. The results indicated complex interaction among the process parameters and the material flow, which affected the final pin formation. The punch temperature …


Modeling Of The Semi-Solid Material Behavior And Analysis Of Micro-/Mesoscale Feature Forming, Gap-Yong Kim, Muammer Koc, Rhet Mayor, Jun Ni Apr 2007

Modeling Of The Semi-Solid Material Behavior And Analysis Of Micro-/Mesoscale Feature Forming, Gap-Yong Kim, Muammer Koc, Rhet Mayor, Jun Ni

Gap-Yong Kim

One of the major challenges in simulation of semi-solid forming is characterizing the complex behavior of a material that consists of both solid and liquid phases. In this study, a material model for an A356 alloy in a semi-solid state has been developed for high solid fractions (>0.6) and implemented into a finite element simulation tool to investigate the micro-/mesoscale feature formation during the forming process. Compared to previous stress models, which are limited to expressing the stress dependency on only the strain rate and the temperature (or the solid fraction), the proposed stress model adds the capability of …


Objective Test Methods For Waveguide Audio Synthesis, Steven Gregory Wood Mar 2007

Objective Test Methods For Waveguide Audio Synthesis, Steven Gregory Wood

Theses and Dissertations

Acoustic Physical Modeling has emerged as a newer musical synthesis technique. The most common form of physical modeling synthesis in both industry and academia is digital waveguide synthesis. Commercially available for the past thirteen years, the top synthesizer manufacturers have chosen to include physical modeling synthesis in their top of the line models. In the area of audio quality testing, the most common tests have traditionally been group listening tests. While these tests are subjective and can be expensive and time-consuming, the results are validated by the groups' proper quality standards. Research has been conducted to evaluate objective testing procedures …


An Evaluation Of American Companies That Outsource Manufacturing To China: Decision-Making And Performance, Michael Kenyon Favreau Mar 2007

An Evaluation Of American Companies That Outsource Manufacturing To China: Decision-Making And Performance, Michael Kenyon Favreau

Theses and Dissertations

The topic of outsourcing ranks at the top of business issues for a wide variety of companies (Wery, 2004; Ezrati, 2004). The majority of American companies believe that offshore-related matters rank as the most strategic decisions that management is expected to make in the next 12 months (Wery, 2004). “Outsourcing in China can help many companies save money, but it can be very frustrating if not done right" (Ting, 2004). The perceived benefits of outsourcing production to China are tremendously enticing, but a lack of understanding of the total costs involved lures many companies into outsourcing when it is not …


Lifetime Testing Of Wire-Grid Polarizers With Selected Over-Coatings, Steven J. Malone Mar 2007

Lifetime Testing Of Wire-Grid Polarizers With Selected Over-Coatings, Steven J. Malone

Theses and Dissertations

Wire-grid polarizers (WGPs) offer superior extinction, durability, angle of incidence, and heat resistance when compared to traditional organic polarizers. WGPs are found in applications such as high lumen lighting, laser devices, high lumen digital cinema projectors, LED packaging, and other integrated optical applications and are driving the need for over-coatings. Over-coating a WGP has been found to increase lifetime and durability. This research provides lifetime data on coated and uncoated WGPs. WGPs over-coated with 100nm of SiO2, 300nm of MgF2, and with no over-coating were heated to temperatures of 450 ºC, 500 ºC, and 550 ºC and timed until they …


A Qualitative Study Of Selected Quality Knowledge And Practices In Guangdong Province, China, Tyler R. Thomas Mar 2007

A Qualitative Study Of Selected Quality Knowledge And Practices In Guangdong Province, China, Tyler R. Thomas

Theses and Dissertations

The manufacturing industry has become very competitive in today's global market environment. Many US companies are faced with the choice of keeping their manufacturing domestic or looking to low cost off-shore countries to take advantage of the labor costs differences. To gain an understanding of the state of manufacturing in China, a major focus in the manufacturing world today, this thesis was undertaken. This thesis presents the findings of research conducted in Guangdong Province, China in June - July, 2005. This research addressed customer focus, leadership and general manufacturing and quality knowledge and practices of small, medium and large sized …


Spot Friction Welding Of Ultra High-Strength Automotive Sheet Steel, Jack H. Sederstrom Mar 2007

Spot Friction Welding Of Ultra High-Strength Automotive Sheet Steel, Jack H. Sederstrom

Theses and Dissertations

Spot friction welding (SFW) was performed on ultra high strength steel (UHSS) steel sheet commonly used in automobile manufacturing. Alloys studied included DP780, DP780EG, DP980, and DF140T sheet steel of varying thickness from 1.2 mm to 1.4 mm. Welding was accomplished using a PCBN standard tool. Weld strengths were then compared to a proposed AWS standard. Initial hardness readings were taken in cross sectioned samples. Grain structure in a SFW is presented. Resistance spot welds were created in three steels. This study focuses on the strength of SFW joints as compared to traditional resistance spot welding (RSW) in welding like …


Control And Ultrasonic Actuation Of A Gas–Liquid Interface In A Microfluidic Chip, Jie Xu, Daniel Attinger Mar 2007

Control And Ultrasonic Actuation Of A Gas–Liquid Interface In A Microfluidic Chip, Jie Xu, Daniel Attinger

Daniel Attinger

This paper describes the design and manufacturing of a microfluidic chip, allowing for the actuation of a gas–liquid interface and of the neighboring fluid. The first way to control the interface motion is to apply a pressure difference across it. In this case, the efficiency of three different micro-geometries at anchoring the interface is compared. Also, the critical pressures needed to move the interface are measured and compared to a theoretical result. The second way to control the interface motion is by ultrasonic excitation. When the excitation is weak, the interface exhibits traveling waves, which follow a dispersion equation. At …


Synthesis Of Gold Micro- And Nano-Wires By Infiltration And Thermolysis, E.A. Olevsky, X. Wang, E. Bruce, M.B. Stern, S. Wildhack, F. Aldinger Feb 2007

Synthesis Of Gold Micro- And Nano-Wires By Infiltration And Thermolysis, E.A. Olevsky, X. Wang, E. Bruce, M.B. Stern, S. Wildhack, F. Aldinger

Industrial and Manufacturing Engineering

An approach for synthesizing micro- and nano-sized gold wires by infiltration and thermolysis is investigated. A porous ZrO2 ceramic preform with aligned pores obtained by unidirectional freezing and freeze-drying is employed as an infiltration template. The sintered porous ZrO2 preform is then infiltrated by a brushing gold solution. The thermolysis is conducted at 600 °C in air. Micro- and nano-sized gold wires are developed within the walls of the pores after thermolysis. The diameter of the gold wires ranges from several hundred nanometers to several microns.