Mechanical Engineering Commons^™

Characterization And Improvement Of Powder Properties Through Plasma Spheroidization For Use In The Laser Powder Bed Fusion Process, M. Hossein Sehhat

Doctoral Dissertations

"This research was conducted to characterize the powder properties using different characterization techniques to enhance the powder behavior in the Laser Powder Bed Fusion (LPBF) process. One of the shortcomings of LPBF process is the high cost of gas-atomized powder feedstock. To overcome this downside, the cheaper water-atomized powder was characterized and used in LPBF process, and its performance was compared with those of gas-atomized powder. Also, the plasma spheroidization process was used to improve the powder characteristics; if the spheroidized powder could function as well as the virgin powder, plasma spheroidization process could be applied to the used powders …

Fabricating Tinicu Ternary Shape Memory Alloy By Directed Energy Deposition Via Elemental Metal Powders, Yitao Chen, Xinchang Zhang, Mohammad Masud Parvez, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In this paper, a TiNiCu shape memory alloy single-wall structure was fabricated by the directed energy deposition technique with a mixture of elemental Ti, Ni, and Cu powders following the atomic percentage of Ti50Ni45Cu5 to fully utilize the material flexibility of the additive manufacturing process to develop ternary shape memory alloys. The chemical composition, phase, and material properties at multiple locations along the build direction were studied, using scanning electron microscopy, energy-dispersive X-ray spectroscopy, X-ray diffraction, Vickers hardness test-ing, tensile testing, and differential scanning calorimetry. The location-dependent compositions of martensitic TiNi and austenitic TiNi phases, mechanical properties, and functional properties …

Absorption Of Nitrogen During Pulsed Wave L-Pbf Of 17-4 Ph Steel, Ben Brown, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In the fabrication of 17-4 PH by laser powder bed fusion (L-PBF) the well-documented occurrence of large amounts of retained austenite can be attributed to an elevated concentration of nitrogen present in the material. While the effects of continuous wave (CW) laser processing on in-situ nitrogen absorption characteristics have been evaluated, power modulated pulsed wave (PW) laser processing effects have not. In this study the effects of PW L-PBF processing of 17-4 PH on nitrogen absorption, phase composition, and mechanical performance are explored using commercially available PW L-PBF equipment and compared to samples produced by CW L-PBF. PW L-PBF samples …

Development Of In-Situ Radiometric Inspection Methods For Quality Assurance In Laser Powder Bed Fusion, Cody S. Lough

Doctoral Dissertations

“Laser Powder Bed Fusion (LPBF) metal Additive Manufacturing (AM) fabricates 3D metal parts layer-by-layer. The process enables production of geometrically complex parts that are difficult to inspect with traditional methods. The LPBF parts experience significant geometry driven thermal variations during manufacturing. This creates microstructure and mechanical property inhomogeneities and can stochastically cause defects. Mission critical applications require part qualification by measuring the defects non-destructively. The layer-to-layer nature of LPBF permits non-intrusive measurement of radiometric signals for a part’s entire volume. These measurements provide thermal features that correlate with the local part health. This research establishes Optical Emission Spectroscopy (OES) and …

Sources Of Quality Uncertainty In Laser Powder Bed Fusion Metal Additive Manufacturing, Zachary Young

Doctoral Dissertations

"Powder based additive manufacturing (AM) exhibits tremendous uncertainties, where variations in build quality is present despite utilizing similar build processing parameters. First, this work reports the features and formation mechanisms of five unique types of spatter during the LPBF process by in-situ high-speed, high-energy x-ray imaging. The unique physical characteristics of spatter are determined. The effect of laser scan speed and laser power on spatter formation, ejection, and mitigation are determined. Second, this work addresses the uncertainty challenge by identifying the sources of uncertainty in SLM by in-situ characterization due to variations from the additive manufacturing processing parameters needed for …

Numerical And Experimental Study Of Mechanical Properties For Laser Metal Deposition (Lmd) Process Part, Lan Li

Doctoral Dissertations

"Laser Metal Deposition (LMD), also called as, Laser Engineered Net Shaping (LENS), Directed Energy Deposition (DED), is a typical Additive Manufacturing (AM) technology, is used for advanced free-form fabrication. It creates parts by directly melting materials and depositing them on the workpiece layer by layer. In this process, the metal powder or fiber is melted within the melting pool by laser beam or electron beam and quickly solidifies to the deposited layer. LMD technology shows great advantages over traditional manufacturing on complex structure fabrication, including high building rates, easy material replacement and reduced material waste. These merits make the wide …

Hydrokinetic Turbine Composite Blades And Sandwich Structures: Damage Evaluation And Numerical Simulation, Mokhtar Fal

Doctoral Dissertations

“Composite materials are gaining interest due to their high strength to weight ratio. This study deals with both experimental and numerical approaches to cover the aspects of the failure of composite materials in hydrokinetic turbine applications. In Part I, the location and magnitude of failure in the horizontal axis water turbine carbon fiber-reinforced polymer (CFRP) composite blades with different laminate stacking sequences were investigated. Two lay-up orientations were adopted for this work ([0⁰]₄ and [0⁰/90⁰]_2s). A finite element analysis model was generated to examine the stresses along the blade. Five angles were introduced to study the effect …

Performance Evaluation Of Alsi10mg Fabricated By A Selective Laser Melting Process, David Michael Murphy

Masters Theses

“Selective laser melting is becoming a widely used additive manufacturing technique that melts metal powder in a layer by layer process in order to build a desired part or geometry. Like many additive processes, selective laser melting allows for fabrication of parts with complex geometries. In order to fabricate a fully dense part there are a number of variables to take into account including: powder characteristics, laser parameters, and environmental parameters. Each of these variables can affect the microstructure and thus the mechanical performance of an additively manufactured part. In this work, the aluminum alloy AlSi10Mg was investigated. AlSi10Mg is …

Influence Of Input Energy On Mechanical Properties Of Laser Powder Bed Fused Aisi 304l Stainless Steel, Tan Pan

Masters Theses

“Powder Bed Fusion process with selective laser melting technique is popularly adopted in additive manufacturing area on account of its layer by layer manufacturing fashion capable of fabricating components with complex internal and external geometries and structures. However, the process-property map is unique and vital for different materials and AM configurations used for fabrication. The process parameter is identified as a significant factor that heavily influences the properties and performances of the printed materials.

Current work aimed to extend the existing knowledge on Laser Powder Bed Fusion fabricated AISI 304L by accessing the influence of varying energy input on the …

Additive Manufacturing Of Customized Lithium-Ion Batteries: Process Fundamentals And Applications, Xiaowei Yu

Doctoral Dissertations

“In the pasting decades, considerable efforts have been spent in developing the next-generation lithium-ion batteries (LIBs), from advanced active materials to new manufacturing methods. The development of additive manufacturing (AM) has brought new opportunities to LIBs. In this work, two AM methods are introduced for fabricating electrodes of LIBs. The first method is aerosol printing, which is a solvent-based wet additive method. Whereas the second method is a solvent-free, dry printing method. The commonly used materials for current collectors and active materials (including cathodes and anodes) of LIBs are aerosol printed and the electrochemical functionalities of the printed materials are …

A Framework For A Successful Additive Repair System, Todd E. Sparks

Doctoral Dissertations

“The goal of this research is to generate a revolutionary improvement to the usability and usefulness of additive repair technology by integrating a set of tools into a seamless work flow. Insufficient automation in the current repair process is a huge hurdle in achieving cost-effective, reliable repairs. Many opportunities have been missed due to inconsistency, quality issues and lack of robustness and flexibility. The present work addresses deficiencies in preparatory steps such as 2D and 3D geometry processing, parameter estimation, and path planning as well as on-machine execution of the path plan. The bulk of the effort is focused on …

A Displacement Controlled Fatigue Test Method For Additively Manufactured Materials, Mohammad Masud Parvez, Yitao Chen, Sreekar Karnati, Connor Coward, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

A novel adaptive displacement-controlled test setup was developed for fatigue testing on mini specimens. In property characterization of additive manufacturing materials, mini specimens are preferred due to the specimen preparation, and manufacturing cost but mini specimens demonstrate higher fatigue strength than standard specimens due to the lower probability of material defects resulting in fatigue. In this study, a dual gauge section Krouse type mini specimen was designed to conduct fatigue tests on additively manufactured materials. The large surface area of the specimen with a constant stress distribution and increased control volume as the gauge section may capture all different types …

A Framework For Process Inspection Of Metal Additive Manufacturing, Chih-Kun Cheng, Frank W. Liou, Yi-Chien Cheng, Sheng-Chih Shen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

In this paper, we propose a process inspection framework for metal additive manufacturing (AM) processes. AM, also known as 3D printing, is the process of joining materials to make objects on the basis of 3D model data and is envisioned to play a strategic role in maintaining economic and scientific dominance. Different from conventional manufacturing methods, the AM process is a point-by-point and layer-by-layer manufacturing. Thus, there are many opportunities to generate a process error that can cause quality issues in an AM part. A systematic AM process inspection is needed to yield acceptable performance of the part. The critical …

Additive Manufacturing Of Metal Functionally Graded Materials: A Review, Yitao Chen, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Functionally graded materials (FGMs) have attracted a lot of research interest due to their gradual variation in material properties that result from the non-homogeneous composition or structure. Metal FGMs have been widely researched in recent years, and additive manufacturing has become one of the most important approaches to fabricate metal FGMs. The aim of this paper is to review the research progress in metal FGMs by additive manufacturing. It will first introduce the unique properties and the advantages of FGMs. Then, typical recent findings in research and development of two major types of metal additive manufacturing methods, namely laser metal …

The Influence Of Build Parameters On The Compressive Properties Of Selective Laser Melted 304l Stainless Steel, Okanmisope Fashanu, Mario F. Buchely, R. Hussein, S. Anandan, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, H. Misak, M. A. Walker

Materials Science and Engineering Faculty Research & Creative Works

Process parameters used during Selective Laser Melting (SLM) process have significant effects on the mechanical properties of the manufactured parts. In this study, the influence of two build parameters (build orientation and hatch angle) on the compressive properties of 304L stainless steel was evaluated. SLM 304L samples were manufactured using three hatch angles, 0°, 67°,105° and two orientations, z-direction and x-direction, and tested using a compression frame according to ASTM E9-09. Bulk density was measured according to ASTM C373-17 before compression. Properties evaluated were the bulk density, yield strength, strength at 15% plastic-strain and strength at 30% plastic-strain. Results showed …

Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Lattice structures fabricated by Additive Manufacturing (AM) processes are promising for many applications, such as lightweight structures and energy absorbers. However, predicting and controlling of their mechanical behaviors is challenging due to the complexity of modeling and the uncertainties exist in the manufacturing process. In this paper, we explore the possibilities enabled by controlling the local densities. A set of lattice structures with different density gradients are designed using an implicit isosurface equation, and they are manufactured by Selective Laser Melting (SLM) process with 304L stainless steel. Finite element analysis and compression test are used to evaluate their mechanical properties. …

Development And Management Of Advanced Batteries Via Additive Manufacturing And Modeling, Jie Li

Doctoral Dissertations

"The applications of Li-ion batteries require higher energy and power densities, improved safety, and sophisticated battery management systems. To satisfy these demands, as battery performances depend on the network of constituent materials, it is necessary to optimize the electrode structure. Simultaneously, the states of the battery have to be accurately estimated and controlled to maintain a durable condition of the battery system. For those purposes, this research focused on the innovation of 3D electrode via additive manufacturing, and the development of fast and accurate physical based models to predict the battery status for control purposes. Paper I proposed a novel …

Designed Extrudate For Ceramic Additive Manufacturing, Devin Mcmillen

Masters Theses

"The objective of this thesis work was to design ceramic paste systems that assist in achieving a high theoretical density ( > 95%) after deposition by a novel additive manufacturing process, i.e. Ceramic On-Demand Extrusion (CODE). The work is encompassed in five main sections: Sections 1 and 2 provide an introduction and literature review of relevant topics for the following sections of experimentation. Section 3 provides an analysis of a reaction chemistry to identify three discrete materials that could be combined via CODE and result in zirconium diboride (ZrB₂) post-sintering. Section 4 describes the development of a high solids …

Laser-Aided Additive Manufacturing Of Glass, John Michael Hostetler

Masters Theses

“This thesis presents various approaches for the laser-aided additive manufacturing of glass. First, a technique is investigated to create free-form, low to zero coefficient of thermal expansion structures out of silica-gel. A CO₂ laser was coupled through a gantry system and focused onto a binder-free silica-gel powder bed (15-40 μm particles). Prior to writing each layer, powder is dispensed by sifting it onto the build platform as opposed to a conventional wiper system, avoiding contacting and potentially damaging sensitive parts. After deposition, the parts are annealed in a furnace to increase their strength. The influence of various process parameters …

Fabrication And Characterization Of Advanced Materials Using Laser Metal Deposition From Elemental Powder Mixture, Xueyang Chen

Doctoral Dissertations

"Over the past decades of years, a great deal of money has been spent to machine large and complex parts from high-performance metals (i.e., titanium components for aerospace applications), so users attempt to circumvent the high cost of materials. Laser metal deposition (LMD) is an additive manufacturing technique capable of fabricating complicated structures with superior properties. This dissertation aims to improve the applications of LMD technique for manufacturing metallic components by using various elemental powder mixture according to the following three categories of research topics. The first research topic is to investigate and develop a cost-effective possibility by using elemental …

Laser Foil Printing And Surface Polishing Processes, Chen Chen

Doctoral Dissertations

"A foil-based additive manufacturing technology for fabricating metal parts, called Laser Foil Printing (LFP), was proposed and developed in this dissertation. The manufacturing sub-processes comprising the LFP technology were comprehensively studied, which include the laser spot welding of foil, laser raster-scan welding of foil, laser cutting of foil, and laser polishing processes. The fabricated free-form parts were demonstrated and own better mechanical properties (micro hardness and tensile strength) than the raw material, because of the rapid-cooling process of laser welding. The full and strong bond between layers was formed by the laser welding process, with no micro-cracks or pores observed. …

Research On Additive Manufacturing Of Metallic Glass Alloy, Yiyu Shen

Doctoral Dissertations

"The required rapid cooling has limited the dimension of the Bulk Metallic glasses (BMGs) produced by traditional method, and hence has seriously limited their applications, despite their remarkable mechanical properties. In this present project, a detailed study is conducted on the methodology and understanding of manufacturing large Zr- based metallic glass part by laser based additive manufacturing technology, which breaks the size limitation. The first research issue proposes and develops a new additive manufacturing technology, named Laser-Foil-Printing (LFP). Sheet foils of LM105 (Zr_52.5Ti₅Al₁₀Ni_14.6Cu_17.9 (at. %)) metallic glass are used as feed …

Investigation Of Microstructure And Mechanical Properties By Direct Metal Deposition, Jingwei Zhang

Doctoral Dissertations

"Microstructure and properties of Direct Metal Deposition (DMD) parts are very crucial to meeting industrial requirements of parts quality. Prediction, and control of microstructure and mechanical properties have attracted much attention during conventional metal manufacturing process under different conditions. However, there is few investigations focused on microstructure simulation and mechanical properties control under different process parameters during DMD process. This dissertation is intended to develop a multiscale model to investigate Ti6Al4V grain structure development and explore Ti6Al4V based functionally graded material (FGM) deposit properties during DMD process. The first research topic is to investigate and develop a cellular automaton-finite element …

Additive Manufacturing Of High Entropy Alloys -- A Review, Wenyuan Cui, Xinchang Zhang, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

High-entropy alloys have attracted increasingly interest due to their unique compositions, microstructures and mechanical properties. Additive manufacturing has been recognized as a promising technology to fabricate the high-entropy alloys in the recent years. The purpose of this paper is to review the current research progress in high-entropy alloys by additive manufacturing process. It will first highlight the important theory of the high-entropy alloys. The next aspect is to summarize current additive manufacturing methods applied for the high entropy alloys. At last, the correlation between the microstructures and the mechanical properties of the high-entropy alloys will be examined and discussed.

Additive Manufacturing Of Glass Using A Filament Fed Process, Junjie Luo

Doctoral Dissertations

"There are many scientific and engineering applications of glass including optics, communications, electronics, and hermetic seals, there has been minimal research towards the Additive Manufacturing (AM) of transparent glass parts. The special thermal and optical properties of glasses make them hard to be printed using conventional AM techniques. In this dissertation, two different AM techniques for glass AM were developed, Selective Laser Melting (SLM) and filament fed process.

Semi-transparent parts were printed with SLM process. However, the filament fed process was found to be more robust and promising for printing optically transparent glass parts. Therefore, this dissertation is focused on …

Error Mapping Of Build Volume In Selective Laser Melting, Ninad Kulkarni

Masters Theses

“Selective laser melting is one of the commonly used additive manufacturing processes employed for production of functional part. Therefore, quality aspects such as dimensional accuracy have become a point of great interest. Like all of the other additive manufacturing processes selective laser melting process suffers from the issue if having wide range of process parameters making the process control a complex task. Additionally, issues specific to the selective laser melting process such as position dependency of accuracy of the part, makes it difficult to predict the resulting dimensional inconsistencies in the part manufactured by this processes. This research is an …

Effect Of Build Parameters On Mechanical Properties Of Ultem 9085 Parts By Fused Deposition Modeling, Krishna Prasanth Motaparti

Masters Theses

"Additive manufacturing is a fabrication technique that is used to build components by depositing material in a layer-by-layer manner. Fused Deposition Modeling (FDM) is one of the additive manufacturing techniques which is widely used for prototyping and production applications of thermoplastic components. In load bearing applications, the flexural and compression forces often coexist. In order to avoid failure under these loads, it is essential to study the mechanical properties of the components fabricated by FDM. The main focus of this research is to study the mechanical properties of the fabricated components and to comprehend their dependence on various build parameters. …

Freeze-Form Extrusion Fabrication Of Boron Carbide, Aaron Scott Thornton

Masters Theses

"Boron carbide is a safe, alternative to beryllium as a material for aerospace structures since it is also light-weight and exhibits high strength. This paper discusses a study of the Freeze-form Extrusion Fabrication (FEF) process to fabricate parts from boron carbide. Process parameters and hardware were modified to fabricate boron carbide specimens free of printed defects. Four-point bending tests were performed to measure the flexural strength of fabricated specimens. Observations of the presence of voids caused by ice crystals in fabricated parts led to further development and characterization of the boron carbide paste used with the FEF process. Additives were …

Performance Metrics For Powder Feeder Systems In Additive Manufacturing, Venkata Sivaram Bitragunta

Masters Theses

"In blown powder Direct Metal Deposition (DMD) process, parts are built by adding metal powder on the melt pool created by the laser system. At low feed rates powder feeder systems have perturbations. The study focused on relationship between the perturbation frequencies by inherent powder feeder designs and its impact on deposition quality. Performance metric determine the relation between perturbations in the powder flow and quality of the deposit. To determine performance metric, various powder feeder designs were analyzed. Perturbation frequencies were introduced to the disk feeder design. The quality of the deposit was determined by the surface roughness of …

Characterization Of 304l Stainless Steel By Means Of Minimum Input Energy On The Selective Laser Melting Platform, Ben Brown

Masters Theses

"Developing parameter sets for new materials on the Selective Laser Melting (SLM) platform has traditionally been done through the use of single line processing windows and a basic design of experiments (DOE) which would include varying machine parameters to maximize density. This study expands the traditional method by determining the main effects statistically for density, allowing for a more in depth analysis wherein the experimental results are statistically correlated to the variable machine parameters used. With this analysis, parameter optimization with respect to achieving near full density, while also considering build rates, can be performed. New parameters for 304L stainless …