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Materials Science and Engineering

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Binders

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Full-Text Articles in Mechanical Engineering

Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez Aug 2011

Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Particle size, binder content and the post-processing schedule are important parameters that affect the microstructure, and, hence, the mechanical properties of parts produced using the indirect selective laser sintering process. 13-93 bioactive glass, with mean particle sizes ranging from 10 μm to 44 μm, is mixed with different amounts of stearic acid binder to fabricate green scaffolds. Through the design of the post-processing schedule, the time required for postprocessing the green scaffolds is reduced from the initial 80 hrs to 12 hrs. The compressive strength varies from 41 MPa for a part with~60% porosity to 157 MPa for a part …


Freeze-Form Extrusion Fabrication Of Composite Structures, Ming-Chuan Leu, Lie Tang, Bradley K. Deuser, Robert G. Landers, Greg Hilmas, Shi C. Zhang, Jeremy Lee Watts Aug 2011

Freeze-Form Extrusion Fabrication Of Composite Structures, Ming-Chuan Leu, Lie Tang, Bradley K. Deuser, Robert G. Landers, Greg Hilmas, Shi C. Zhang, Jeremy Lee Watts

Mechanical and Aerospace Engineering Faculty Research & Creative Works

A Freeze-form Extrusion Fabrication (FEF) process capable of making three-dimensional (3D) parts and structures with graded composite materials is presented in this paper. The process development includes the design and manufacture of a gantry machine with a triple-extruder mechanism and the associated electronics hardware and computer software for fabricating functionally graded parts from multiple aqueous pastes. A rheological behavior study with Al2O3 paste is performed to identify an efficient binder for transforming the paste into a pseudoplastic with a high yield stress. A green part is first fabricated using the triple-extruder FEF machine in a layer-by-layer manner …


Selective Laser Sintering Of 13-93 Bioactive Glass, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez Aug 2010

Selective Laser Sintering Of 13-93 Bioactive Glass, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Bioactive glasses are more promising than biopolymers in fabricating scaffolds for bone tissue repair because they convert to hydroxyapatite, when implanted in vivo. Both direct and indirect selective laser sintering (SLS) methods of 13-93 bioactive glass were considered in this research to study the feasibility of fabricating scaffolds for bone repair applications. Stearic acid was used as the binder in the indirect method to fabricate the scaffolds. The green scaffolds underwent binder burnout and sintering at various soaking conditions between 675⁰C and 700⁰C, achieving a maximum compressive strength of 23.6 MPa, which is higher than that of the human cancellous …


Optimization Of Selective Laser Sintering Process For Fabrication Of Zirconium Diboride Parts, Ming-Chuan Leu, Shashwatashish Pattnaik, Greg Hilmas Aug 2010

Optimization Of Selective Laser Sintering Process For Fabrication Of Zirconium Diboride Parts, Ming-Chuan Leu, Shashwatashish Pattnaik, Greg Hilmas

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Selective Laser Sintering (SLS) was investigated to fabricate Zirconium Diboride (ZrB2) parts for ultra-high temperature applications. Experiments were conducted to determine values of SLS process parameters (laser power, scan speed, line spacing, and layer thickness) that can be used to build ZrB2 parts with high integrity and sharp geometrical features. A sacrificial plate with a proper number of layers (determined from experimentation) separated from the main part was built in order to reduce thermal gradients when building the main part. The sacrificial plate was found to assist in eliminating cracks in the bottom of the main part. …


Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan Aug 2008

Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Using the Selective Laser Sintering (SLS) process, both flexural test bars and 3D fuel injector components have been fabricated with zirconium diboride (ZrB2) powder. Stearic acid was selected as the binder. Values of SLS process parameters were chosen such that the green parts could be built with sharp geometrical features and that the sintered parts could have good mechanical properties. After binder burnout and sintering, the SLS fabricated ZrB2 test bars achieved 80% theoretical density, and the average flexural strength of the sintered samples was 195 MPa. These values demonstrate the feasibility of the SLS process for …