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Full-Text Articles in Materials Science and Engineering

Optimization And Characterization Of Novel Injection Molding Process For Metal Matrix Syntactic Foams, Myranda Spratt, Joseph William Newkirk Dec 2020

Optimization And Characterization Of Novel Injection Molding Process For Metal Matrix Syntactic Foams, Myranda Spratt, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Metal matrix syntactic foams are particulate composites comprised of hollow or porous particles embedded in a metal matrix. These composites are difficult to manufacture due primarily to the lightweight, relatively fragile filler material. In this work, an injection molding process was developed for metal matrix syntactic foams. First, an aqueous binder was optimized for low-pressure injection molding. A mixture model was used to optimize the composition of the binder to achieve the highest relative density. The model predicted the maximum relative density was at a binder composition (in vol.%) of 7% agar, 4% glycerin, and 89% water. Second, this binder …


Microstructural Influence On Mechanical Properties Of A Lightweight Ultrahigh Strength Fe-18mn-10al-0.9c-5ni (Wt%) Steel, Michael Piston, Laura Bartlett, Krista R. Limmer, Daniel M. Field Oct 2020

Microstructural Influence On Mechanical Properties Of A Lightweight Ultrahigh Strength Fe-18mn-10al-0.9c-5ni (Wt%) Steel, Michael Piston, Laura Bartlett, Krista R. Limmer, Daniel M. Field

Materials Science and Engineering Faculty Research & Creative Works

This study evaluates the role of thermomechanical processing and heat treatment on the microstructure and mechanical properties of a hot rolled, annealed, and aged Fe-18Mn-10Al-0.9C-5Ni (wt%) steel. The steel exhibited rapid age hardening kinetics when aged in the temperature range of 500-600 ⁰C for up to 50 h, which has been shown in other work to be the result of B2 ordering in the ferrite and K-carbide precipitation within the austenite matrix. The ultimate tensile strength increased from 1120 MPa in the annealed condition to 1230 MPa after 2 h of aging at 570 ⁰C. Charpy V-notch toughness was evaluated …


Scale Formation On 430 Stainless Steel In A Simulated Slab Combustion Reheat Furnace Atmosphere, Richard Osei, Semen Naumovich Lekakh, Ronald J. O'Malley Sep 2020

Scale Formation On 430 Stainless Steel In A Simulated Slab Combustion Reheat Furnace Atmosphere, Richard Osei, Semen Naumovich Lekakh, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Scale formed during slab reheating can be difficult to remove by high-pressure descaling, having a negative impact hot roll surface quality. A large-capacity thermogravimetric apparatus that replicates the combustion atmosphere and temperature in a slab reheat furnace was used to investigate scale formation on 430 stainless steel. Effects of reheating parameters (temperature, time and atmosphere) on oxidation kinetics were investigated. Oxidized samples were characterized by scanning electron microscopy, Raman spectroscopy and x-ray diffraction to document the microstructure and morphology of scale. Mechanisms for the formation of multi-layered oxide structures that complicate oxidation kinetics and scale removal are discussed.


A Modified Johnson-Cook Model Incorporating The Effect Of Grain Size On Flow Stress, S. Ganguly, Mario F. Buchely, K. Chandrashekhara, Semen Naumovich Lekakh, Ronald J. O'Malley Sep 2020

A Modified Johnson-Cook Model Incorporating The Effect Of Grain Size On Flow Stress, S. Ganguly, Mario F. Buchely, K. Chandrashekhara, Semen Naumovich Lekakh, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties of steel are influenced by grain size, which can change through mechanisms such as nucleation and growth at elevated temperatures. However, the classic Johnson-Cook model that is widely used in hot deformation simulations does not consider the effect of grain size on flow stress. In this study, the Johnson-Cook model was modified to incorporate the effects of austenite grain size on flow stress. A finite element model was employed to characterize the effects of grain size on the flow stress for different steel grades over a range of temperatures (900⁰ to 1300⁰). Simulation results show good agreement …


New Experimental Apparatus To Investigate Hot Tearing Behavior In Steel, Yanru Lu, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh, Mario F. Buchely Sep 2020

New Experimental Apparatus To Investigate Hot Tearing Behavior In Steel, Yanru Lu, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh, Mario F. Buchely

Materials Science and Engineering Faculty Research & Creative Works

Hot tearing is a complex thermomechanical phenomenon occurring in the semi-solid region. Strain in this region can induce cracking and localized alloying element segregation. An apparatus for investigating hot tearing was developed utilizing a servo-motor controlled cylinder to apply a pre-determined amount of strain to the solidifying shell. A special mold was developed using filling and solidification modeling to ensure that dendrite growth was perpendicular to applied strain. A computer-automated system was utilized to control the strain and strain rate and measure the force and displacement. Solidification experiments utilizing AISI 1020 steel validated the apparatus capabilities and optimized testing parameters.


Interactions Between Dry Vibratable Tundish Linings And Steel Melts, Tyler M. Richards, Ronald J. O'Malley, Jeffrey D. Smith, Todd P. Sander Sep 2020

Interactions Between Dry Vibratable Tundish Linings And Steel Melts, Tyler M. Richards, Ronald J. O'Malley, Jeffrey D. Smith, Todd P. Sander

Materials Science and Engineering Faculty Research & Creative Works

Interactions between two tundish working linings and molten steel were investigated using industrial samples and laboratory testing. Periclase-based dry vibe linings from two production facilities were sampled and examined after casting: one containing 30 wt.% olivine and one without olivine. Cathodoluminescence imaging, secondary electron microscopy, energydispersive spectroscopy and x-ray diffraction analysis were performed to characterize the interactions. An experiment was developed to replicate the conditions found in a production tundish on the laboratory scale. Results comparing interactions observed in laboratory lining tests and commercial lining samples for the two lining materials are presented and discussed.


Peritectic Behavior Detection In The Fe-C-Mn-Al-Si Steel System Using Fiber Optic Temperature Mapping, Muhammad Roman, Damilola Balogun, Rex E. Gerald Ii, Laura Bartlett, Jie Huang, Ronald J. O'Malley Sep 2020

Peritectic Behavior Detection In The Fe-C-Mn-Al-Si Steel System Using Fiber Optic Temperature Mapping, Muhammad Roman, Damilola Balogun, Rex E. Gerald Ii, Laura Bartlett, Jie Huang, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Peritectic reactions can cause surface defects and breakouts in continuous casting and the peritectic region is often avoided by adjusting the chemical composition of the steel to cast outside of the peritectic sensitivity range. However, the combined effects of C, Mn, Al, and Si on the boundaries that map peritectic region are still disputed for many advanced high strength steel grades. An apparatus for performing controlled solidification experiments is being developed to characterize the effects of chemical composition on the uniformity of shell growth during solidification using a copper chill mold with an embedded fiber-optic temperature sensor that enables high …


The Influence Of Ti, Nb And V On The Hot Ductility Of As-Cast Microalloyed Steels, Madhuri Varadarajan, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh Sep 2020

The Influence Of Ti, Nb And V On The Hot Ductility Of As-Cast Microalloyed Steels, Madhuri Varadarajan, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh

Materials Science and Engineering Faculty Research & Creative Works

Microalloying with Ti, Nb and V, both individually and in combination, is a common method for producing steels with high strength and toughness. However, interaction with other elements and impurities can lead to cracking during continuous casting and rolling. The hot ductility of commercially cast V, Nb and Nb-V-Ti steels has been investigated using two experimental methods: tensile testing utilizing a servo-hydraulic load frame with a resistance furnace and thermomechanical testing using rapid joule heating. The temperature-dependent ductility of these steels is compared for both test methods. Factors that influence the ductility of these steels are discussed.


A Spatially Distributed Fiber-Optic Temperature Sensor For Applications In The Steel Industry, Muhammad Roman, Damilola Balogun, Yiyang Zuang, Rex E. Gerald Ii, Laura Bartlett, Ronald J. O'Malley, Jie Huang Jul 2020

A Spatially Distributed Fiber-Optic Temperature Sensor For Applications In The Steel Industry, Muhammad Roman, Damilola Balogun, Yiyang Zuang, Rex E. Gerald Ii, Laura Bartlett, Ronald J. O'Malley, Jie Huang

Materials Science and Engineering Faculty Research & Creative Works

This paper presents a spatially distributed fiber-optic sensor system designed for demanding applications, like temperature measurements in the steel industry. The sensor system employed optical frequency domain reflectometry (OFDR) to interrogate Rayleigh backscattering signals in single-mode optical fibers. Temperature measurements employing the OFDR system were compared with conventional thermocouple measurements, accentuating the spatially distributed sensing capability of the fiber-optic system. Experiments were designed and conducted to test the spatial thermal mapping capability of the fiber-optic temperature measurement system. Experimental simulations provided evidence that the optical fiber system could resolve closely spaced temperature features, due to the high spatial resolution and …