Engineering Science and Materials Commons^™

Elastic Properties Of The Non-Mixing Copper Donor Assisted Material In Friction Stir Welding Of Aluminum Alloys Using Nanoindentation, M. Ojha, A. H. Al-Allaq, Y. S. Mohammed, S. N. Bhukya, Z. Wu, A. A. Elmustafa

Mechanical & Aerospace Engineering Faculty Publications

Friction stir welding of high-strength materials such as steels is the impeded by the lack of the vast heat input needed to start the process. Contact friction is considered the most dominant source of heat generation for FSW steels which tends to cause severe wear conditions of the tool hear. To relieve the extreme wear conditions that occur on the tool heads because of FSW steels, we introduce the non-mixing Cu donor stir material to friction stir welding of aluminum alloys. The elastic properties of the Cu donor assisted friction stir welded aluminum alloys are measured using nanoindentation. The hardness …

Synthesis And Consolidation Of Metal Oxide Nanocrystals Via Nonthermal Plasma, Austin Cendejas

McKelvey School of Engineering Theses & Dissertations

Nonthermal plasmas offer a unique nonequilibrium environment that has been leveraged in a wide variety of applications in the fields of material processing, lighting, and waste management to name a few. In all of these cases, the plasma serves as a source of high energy electrons, ions, reactive gas species, and radicals that interact in several ways with surfaces brought into contact with the plasma. Specifically, nonthermal plasmas have been shown to be very successful in achieving continuous, high-throughput, monodisperse nanocrystals of a wide variety of materials. The crystallinity of nanoparticles synthesized in nonthermal plasmas can be attributed to the …

Imparities Of Shear Avalanches Dynamic Evolution In A Metallic Glass, Yin Du, Qing Zhou, Qian Jia, Yidi Shi, Haifeng Wang, Jian Wang

Department of Mechanical and Materials Engineering: Faculty Publications

The imparities of shear avalanches dynamic evolution under nanoindentation originating from the soft regions and the stiff matrix were explored in a metallic glass by statistical and dynamic analysis. Upon the continuous indentation process, the dynamic state of the stiff matrix exhibits a transition from a chaotic behavior to a self-organized critical (SOC) behavior, whereas the soft regions are domi-nated by the SOC behavior throughout the indentation process. The mechanism was clarified by the evolution of the cut-off size of shear avalanches. These findings might advance our fundamental understanding of inhomogeneous deformation on microscale.

IMPACT STATEMENT The shear avalanches dynamic …

In Situ Mechanical Characterization Of The Mixed- Mode Fracture Strength Of The Cu/Si Interface For Tsv Structures, Chenglin Wu, Congjie Wei, Yanxiao Li

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

In situ nanoindentation experiments have been widely adopted to characterize material behaviors of microelectronic devices. This work introduces the latest developments of nanoindentation experiments in the characterization of nonlinear material properties of 3D integrated microelectronic devices using the through-silicon via (TSV) technique. The elastic, plastic, and interfacial fracture behavior of the copper via and matrix via interface were characterized using small-scale specimens prepared with a focused ion beam (FIB) and nanoindentation experiments. A brittle interfacial fracture was found at the Cu/Si interface under mixed-mode loading with a phase angle ranging from 16.7° to 83.7°. The mixed-mode fracture strengths were extracted …

Mechanical Characterizations Of 3d-Printed Plla/Steel Particle Composites, Hozhabr Mozafari, Pengfei Dong, Haitham Hadidi, Michael P. Sealy, Linxia Gu

Department of Mechanical and Materials Engineering: Faculty Publications

The objective of this study is to characterize the micromechanical properties of poly-L-lactic acid (PLLA) composites reinforced by grade 420 stainless steel (SS) particles with a specific focus on the interphase properties. The specimens were manufactured using 3D printing techniques due to its many benefits, including high accuracy, cost effectiveness and customized geometry. The adopted fused filament fabrication resulted in a thin interphase layer with an average thickness of 3 μm. The mechanical properties of each phase, as well as the interphase, were characterized by nanoindentation tests. The effect of matrix degradation, i.e., imperfect bonding, on the elastic modulus of …

Artificial Neural Network And Finite Element Modeling Of Nanoindentation Tests On Silica, Kianoosh Koocheki

Department of Civil and Environmental Engineering: Dissertations, Theses, and Student Research

Two major forms of Silica include the crystalline form named Quartz which consist of the sand grains in nature, and amorphous form named Silica Glass or Fused Silica which is commonly known as glass. Fused Silica is an amorphous crystal that can show plastic behavior at micro-scale despite its brittle behavior in large scales. Due to the amorphous and ductile nature of Fused Silica, this behavior may not be explained well using the traditional dislocation-based mechanism of plasticity for crystalline solids. The crystal plasticity happens due to shear stress and stored energy in the material as dislocations which does not …

Analysis Of Corrosion-Induced Diffusion Layer In Zk60a Magnesium Alloy.Pdf, Shumin Li

Shumin Li

Constitutive Modeling And Experiments For The Micro And Nano Behaviors In Metals, Cheng Zhang

LSU Doctoral Dissertations

This work addresses the micro- and nano-behaviors in metals through constitutive modeling and experiments. The size effect encountered during nanoindentation experiments, which is known as indentation size effect (ISE), is investigated for metal materials. The ISE is believed to be related with the strain gradient at small indentation depths. Geometrically necessary dislocations (GNDs) are formed in order to accommodate the strain gradient, which results in the increase in the material hardness. The grain boundaries in polycrystalline materials play an important role on the material hardness during nanoindentation experiments as there is a soften-hardening segment in the curve of hardness as …

An Atomic Force Microscopy Nanoindentation Study Of Size Effects In Face-Centered Cubic Metal And Bimetallic Nanowires, Erin Leigh Wood

Graduate College Dissertations and Theses

The enhancement of strength of nanoscale materials such as face-centered cubic metal nanowires is well known and arises largely from processes mediated by high energy surface atoms. This leads to strong size effects in nanoscale plasticity; ,smaller is stronger. Yet, other factors, such as crystalline defects also contribute greatly to the mechanical properties. In particular, twin boundaries, which are pervasive and energetically favorable defects in face-centered cubic metal nanowires, have been shown to greatly enhance the strength, furthermore this increase in strength has been shown to be directly influenced by the twin density. However, attempts to control the …

New Topics On Nanoindentation Of Polymers And Composite Materials, Ricardo Martinez-Hernandez

Open Access Theses & Dissertations

In this study, nanoindentation was used to determine Young's modulus of homogeneous plastic materials as well as inhomogeneous epoxy woven fabric composites using various indenters. In the first part, homogeneous PMMA and polycarbonate were characterized using conical and spherical indenters. The conventional approach of the inverse analysis was modified in order to account for effects obtained during spherical nanoindentation. The experimental results were verified using FEA analysis in ABAQUS. It was found that viscous effects were present in conical nanoindentations which led to an overestimation of contact stiffness. The second part, the response of carbon and glass fiber woven fabric …

Methods For Characterizing Mechanical Properties Of Wood Cell Walls Via Nanoindentation, Yujie Meng

Masters Theses

Nanoindentation is a method of contacting a material whose mechanical properties are unknown with another material whose properties are known. Nanoindentation has the advantage of being able to probe a material’s microstructure while being sensitive enough to detect variations in mechanical properties. However, nanoindentation has some limitations as a testing technique due to the specific formation and structure of some biomaterials. The main objective of this research is to identify any factors that influence the nanoindentation measurement of wood cell walls (a typical biomaterial).

The function of the embedding media in describing the properties of wood cells is poorly understood. …

Synthesis, Structure And Properties Of Nanolayered Dlc/Dlc Films, Pankaj Gupta

LSU Master's Theses

Diamondlike carbon (DLC) films have been explored extensively in the past due to their highly attractive properties. However, the high level of internal stress developed during growth prevents deposition of thick films. Synthesis of DLC/DLC multilayers (DDM) presents a venue to overcome this drawback. In the present study, DLC films and DDM were deposited on Si substrate using dc plasma of CH₄ and Ar gas mixture. FTIR was used to analyze the structure of the DLC films. Mechanical properties of the films were characterized by microhardness testing and nanoindentation. The tribological properties were studied by conducting pin-on-disc experiments in …