Engineering Science and Materials Commons^™

Numerical Studies For Improving Fracture Toughness Resistance Curve Testing Using Single-Edge (Notched) Tension Specimens, Yifan Huang

Electronic Thesis and Dissertation Repository

The fracture toughness resistance curve, i.e. the J-integral resistance curve (J-R curve) or the crack tip opening displacement resistance (CTOD-R) curves, is widely used in the integrity assessment and strain-based design of energy pipelines with respect to planar defects (i.e. cracks). This thesis deals with issues related to the experimental determination of the J(CTOD)-R curves using the newly-developed single-edge (notched) tension (SE(T)) specimens. In the first study, the plastic geometry factor, i.e. the η_pl factor, used to evaluate J in a J-R curve test based on …

Kinetics Of Length Scale Dependent Deformation Of Gold Microspheres And Micropillars, A Z M Ariful Islam

Electronic Thesis and Dissertation Repository

In this thesis length and time scale dependence of the operative plastic deformation mechanisms in Au is studied. Uniaxial compression tests were performed at various loading rates on FIB-milled Au micropillars and single-crystalline Au microspheres of diameter ranging from 0.8 to 6.0 µm to investigate the incipient and bulk plasticity events. Constant-load ambient-temperature creep tests were performed on the micropillars to study the time-dependent plasticity at very slow strain rates. Uniaxial compression tests were also performed on coated Au microspheres to study the effect of extrinsic constraint on the deformation mechanisms.

During uniaxial compression, both the Au micropillars and microspheres …

Doped Tio2 Nanowires For Applications In Dye Sensitized Solar Cells And Sacrifical Hydrogen Production, Qasem Alsharari

Electronic Thesis and Dissertation Repository

This thesis explores the synthesis of metal oxide 1-D nanowires using a sol-gel method in supercritical carbon dioxide (sc-CO₂), as an environmental friendly enabling solvent. Porous nanowires were synthesized and their performance was tested in dye sensitized solar cell and sacrifical hydrogen production. Titanium isopropoxide (TIP) was used as a precursor for titania synthesis while copper, bismuth and indium were examined as dopants, respectively. The sol-gel reactions were catalyzed by acetic acid in CO₂ at a temperature of 60 °C and pressure of 5000 psi. It was observed that acetic acid/monomer ratio > 4 produced nanowires while a …