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Makara Journal of Technology

2003

Heteropoly acid

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Role Of K3-Xhxpw12o40 As A Catalyst In Selective Catalysis Of Methylamine Synthesis From Ammonia And Methanol, Mohammad Nasikin Dec 2003

Role Of K3-Xhxpw12o40 As A Catalyst In Selective Catalysis Of Methylamine Synthesis From Ammonia And Methanol, Mohammad Nasikin

Makara Journal of Technology

Role of K3-xHxPW12O40 as a Catalyst in Selective Catalysis of Methylamine Synthesis from Ammonia and Methanol. Synthesize of methylamine from methanol and ammonia was studied in this research work using a partially potassium heteropoly salt (K3-xHxPW12O40 abbreviated as KPW) as a catalyst. KPW was prepared from heteropoly salt and potassium carbonate by using ion exchange method. The reaction was conducted at 600 ~ 800K and at the atmospheric pressure. Reactor used was a continue flow reactor with W/F=0,1~0,9g-kat.mnt./cc.Concentration of reactants and products were analyzed by gas chromathography while catalyst structure was observed by XRD (X-ray diffraction). Isothermal adsorption method was …