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Surface Structure Of Alkylsilylated Hzsm-5 As Phase-Boundary Catalyst, Hadi Nur, Yun Hau Ng, Mohd Nazlan Mohd Muhid, Halimaton Hamdan
Surface Structure Of Alkylsilylated Hzsm-5 As Phase-Boundary Catalyst, Hadi Nur, Yun Hau Ng, Mohd Nazlan Mohd Muhid, Halimaton Hamdan
Yun Hau Ng
The need for cleaner environment concerns motivates the development of more efficient catalytic system. Based on this consideration, recently a novel catalyst named "Phase-boundary catalyst", a bimodal amphiphilic solid catalyst, was proposed. It was demonstrated that the catalytic system containing phase-boundary catalyst required neither stirring to make an emulsion nor addition of a co-solvent to make a homogeneous solution to drive the reaction. The driving force that has prompted this paper is to investigate the surface structure of alkylsilylated HZSM-5 as phase-boundary catalyst. Temperature Programmed Desorption (TPD) of ammonia and, 13C and 29Si MAS NMR spectroscopy were used to elucidate …