Engineering Commons^™

On The Permittivity Of Xt-Cf20, Aaron Harmon, Wei Zhang, Victor Khilkevich

Electrical and Computer Engineering Faculty Research & Creative Works

In This Work, the Permittivity of a 3D-Printed Carbon Fiber-Loaded Anisotropic Material, XT-CF20, is Examined Further. the Microstructure of XT-CF20 is First Examined Via Optical Imaging and is Shown to Be Composed of Inclusions that Are Aligned with the Print Direction of the Sample. the Permittivity Tensor for the Aligned Microstructure is Then Measured using a Capacitive Measurement Technique and Simulations Are Provided to Demonstrate the Validity of This Measurement Method. the Simulated Permittivity Values for XT-CF20 Samples with Varying Infill Structures Are Then Presented and Compared to the Measured Permittivity Values of Said Samples. an Error of Less Than …

Deep Learning-Guided Prediction Of Material’S Microstructures And Applications To Advanced Manufacturing, Jianan Tang

All Dissertations

Material microstructure prediction based on processing conditions is very useful in advanced manufacturing. Trial-and-error experiments are very time-consuming to exhaust numerous combinations of processing parameters and characterize the resulting microstructures. To accelerate process development and optimization, researchers have explored microstructure prediction methods, including physical-based modeling and feature-based machine learning. Nevertheless, they both have limitations. Physical-based modeling consumes too much computational power. And in feature-based machine learning, low-dimensional microstructural features are manually extracted to represent high-dimensional microstructures, which leads to information loss.

In this dissertation, a deep learning-guided microstructure prediction framework is established. It uses a conditional generative adversarial network (CGAN) …

Microstructures And Hardness Of Tig Welded Experimental 57fe15cr25ni Steel, Parikin Parikin, Mohammad Dani, Abu Khalid Rivai, Agus Hadi Ismoyo, Riza Iskandar, Arbi Dimyati

Makara Journal of Technology

The microstructures and hardness of tungsten inert gas (TIG) welded experimental 57Fe15Cr25Ni steel were investigated through optical–scanning electron microscopy analyses and with a hardness tester, respectively. The welding process restructured the constituent atoms into regular and irregular crystal lattices. Rapid cooling of the weld metal allowed the formation of a dendritic (columnar) structure, with porous grains. By contrast, slow cooling influenced HAZ and led to the formation of grain structures. The crystal lattice became more organized and larger than other zones. Meanwhile, the base metal formed circular nets that covered large area inside thick and thin grain boundaries. The diffraction …

Multilayered Planar Periodic Subwavelength Microstructures For Generating And Detecting Circularly Polarized Thermal Infrared Radiation, Samuel Lanning Wadsworth

Electronic Theses and Dissertations

Generation and detection of circularly-polarized (CP) radiation in the 8- to 12-μm band of the infrared (IR) spectrum is crucial for polarization sensing and imaging scenarios. There is very little naturally occurring CP radiation in the long-wave IR band, so that useful functionalities may be obtained by exploiting preferential radiation and transmission characteristics of engineered metamaterials. Conventional CP devices in the IR utilize birefringent crystals, which are typically bulky and expensive to manufacture. The operation of these devices is generally optimized at a single wavelength. Imaging in the long-wave IR is most often broadband, so that achromatic CP-device behavior is …

Electrode Of Metallic Oxides Coated Titanium With Interlayer, Yi Tang, Li-Kun Xu, Yong-Lei Xin, Jun-Tao Wang, Ping Long

Journal of Electrochemistry

Various Ti/IrRuSn,Ti/IrTa/IrRuSn and Ti/IrTaSn/IrRuSn oxide electrodes were prepared by sol-gel method.The surface morphology and microstructure were analysed with FESEM and XRD.The electrochemical activity and stability were investigated using electrochemical technologies including chlorine and oxygen evolving potential measurements,cyclic voltammetry,accelerated life test,and alternative electrolysis.The results indicate that the electrodes with interlayers present more cracks on the surface and a little bigger average grain size,with particles of different shapes precipitated in the cracks.The electroactive sites are increased and the selectivity for the chlorine evolving reaction is enhanced,but the current efficiency for the chlorine production is somewhat lowered by the addition of different interlayers.The …

Microstructure And Electrical Performance Of Sputter-Deposited Hafnium Oxide (Hfo2) Thin Films, Brandon Adrian Aguirre

Open Access Theses & Dissertations

Hafnium oxide (HfO2) based dielectrics have been currently considered as the possible replacements for the traditional gate-oxide (SiO2) of the complementary metal-oxide semiconductor (CMOS) devices. The high dielectric constant, wide band gap, and thermal stability in contact with Si make HfO2 a potential material for application in CMOS devices. The performance of HfO2 as a gate oxide material, however, depends on its quality and interface structure with Si. In this work, HfO2 thin films have been deposited by rf sputtering onto Si(100) substrates under varying growth temperatures (Ts). The objective of the work is to understand the growth and microstructure …

High Performance Zno Varistors Prepared From Nanocrystalline Precursors For Miniaturised Electronic Devices, Suresh Pillai, Declan Mccormack, John Kelly, Raghavendra Ramesh

Articles

An industrially viable solution-based processing route using minimal amounts of solvent has been used to prepare bulk quantity nanopowders (average particle size 15.3 nm) for the fabrication of ZnO varistors. The xerogels, calcined powders and sintered materials were fully characterised. The preparation of varistors from nanopowders has been optimised by studying the effect of temperature on grain growth, densification and breakdown voltage. The varistors are prepared by sintering at 1050 C for 2 hours, a temperature that is significantly lower than that used in the current industrial process. Highly dense varistor discs prepared from the sintered material produce devices, with …

Impact Of Local Attenuation Approximations When Estimating Correlation Length From Backscattered Ultrasound Echoes, Timothy A. Bigelow, William D. O'Brien

Timothy A. Bigelow

Estimating the characteristic correlation length of tissue microstructure from the backscattered power spectrum could improve the diagnostic capability of medical ultrasound. Previously, size estimates were obtained after compensating for source focusing, the frequency-dependent attenuation along the propagation path (total attenuation), and the frequency-dependent attenuation in the scattering region (local attenuation). In this study, the impact of approximations of the local attenuation on the scatterer size estimate was determined using computer simulations and theoretical analysis. The simulations used Gaussian impedance distributions with an effective radius of 25 μm randomly positioned in a homogeneous half-space sonified by a spherically focused source (f/1 …

Signal Processing Strategies That Improve Performance And Understanding Of The Quantitative Ultrasound Spectral Fit Algorithm, Timothy A. Bigelow, William D. O'Brien

Timothy A. Bigelow

Quantifying the size of the tissue microstructure using the backscattered power spectrum has had limited success due to frequency-dependent attenuation along the propagation path, thus masking the frequency dependence of the scatterer size. Previously, the SPECTRAL FIT algorithm was developed to solve for total attenuation and scatterer size simultaneously [Bigelow et al., J. Acoust. Soc. Am. 117, 1431-1439 (2005)]. Herein, the outcomes from signal processing strategies on the SPECTRAL FIT algorithm are investigated. The signal processing methods can be grouped into two categories, viz., methods that improve the performance of the algorithm and methods that provide insight. The methods that …

Scatterer Size Estimation In Pulse-Echo Ultrasound Using Focused Sources: Calibration Measurements And Phantom Experiments, Timothy A. Bigelow, William D. O'Brien

Timothy A. Bigelow

In a companion paper [T. A. Bigelow and W. D. O'Brien Jr., J. Acoust. Soc. Am. 116, 578 (2004)], theory, supported by simulations, showed that accurate scatterer size estimates could be obtained using highly focused sources provided that the derived generalized attenuation-compensation function was used and the velocity potential field near the focus could be approximated as a three-dimensional Gaussian. Herein, the theory is further evaluated via experimental studies. A calibration technique is developed to find the necessary equivalent Gaussian dimensions for a focused source using reflections obtained from a rigid plane scanned through the focus. Then, the theoretical analysis …

Scatterer Size Estimation In Pulse-Echo Ultrasound Using Focused Sources: Theoretical Approximations And Simulation Analysis, Timothy A. Bigelow, William D. O'Brien

Timothy A. Bigelow

The speckle in ultrasound images has long been thought to contain information related to the tissue microstructure. Many different investigators have analyzed the frequency characteristics of the backscattered signals to estimate the scatterer acoustic concentration and size. Previous work has been mostly restricted to unfocused or weakly focused ultrasound sources, thus limiting its implementation with diagnostically relevant fields. Herein, we derive equations capable of estimating the size of a-scatterer for any reasonably focused source provided that the velocity potential field in the focal region can be approximated as a three-dimensional Gaussian beam, scatterers are a sufficient distance from the source, …