Engineering Commons^™

Additive Manufacturing Of High-Performance Nanolamellar Eutectic High-Entropy Alloys, Jie Ren

Doctoral Dissertations

Additive manufacturing, also called three-dimensional (3D) printing, is an emerging technology for printing net-shaped components layer by layer for applications in automotive, aerospace, biomedical and other industries. In addition to the vast design freedom offered by this approach, metal 3D printing via laser powder-bed fusion (L-PBF) involves large temperature gradients and rapid cooling and provides exciting opportunities for producing microstructures and mechanical properties beyond those achievable by conventional processing routes. Although these extreme printing conditions enable microstructural refinement to the nanoscale for achieving high strength. However, high-strength nanostructured alloys by laser additive manufacturing often suffer from limited ductility. Eutectic high-entropy …

Monitoring Additive Manufacturing Machine Health, Jeremy Hale

Doctoral Dissertations

Additive manufacturing (AM) allows the production of parts and goods with many benefits over more conventional manufacturing methods. AM permits more geometrically complex designs, custom and low-volume production runs, and the flexibility to produce a wide variety of parts on a single machine with reduced pre-production cost and time requirements. However, it can be difficult to determine the condition, or health, of an AM machine since complex designs can increase the variability of part quality. With fewer parts produced, destructive testing is less desirable and statistical methods of tracking part quality may be less informative. Combined with the relatively more …

A Study On Early Age Properties Of Concrete For Precast And 3d Printing, Debalina Ghosh

Doctoral Dissertations

Concrete is the second-most consumed material, leading the global Portland cement production of 4.1 billion tons in 2020 and 5-8% of global Carbon dioxide (CO₂) emission annually. As with any other material and practice, the construction industry is also ever-changing to meet market demand, evolving technology, and resource limitation. In the case of concrete construction, one of the main concerns is the lack of automation. In the last few decades, some new construction methods have risen to address this concern. Some of these economic and successful practices are precast construction, self-compacting concrete (SCC), and 3D printing of concrete(3DPC). …

Enabling Nanoimprint Lithography Techniques Across Multiple Manufacturing Processes, Vincent Einck

Doctoral Dissertations

Advanced nanooptics in the areas of flat lenses, diffractive elements, and tunable emissivity require a route to high throughput manufacturing. Nanooptics are often demanding of high refractive index materials, nanometer precision and ease of fabrication. Nanoimprint lithography (NIL) is a low-cost, high throughput manufacturing technique beginning to be realized in commercial industry.^1,2 The NIL process is an ideal manufacturing candidate due to its ability to have a fast process time, efficient use of materials, repeatability and high precision while also having wide diversity of potential structures and material choices. Appling NIL techniques to other facets of manufacturing enable the …

Fundamental Understanding Of The Transient Melt Pool Dynamics, Solidification Kinetics And Build Texture In Spot-Melt Additive Manufacturing Of Ti-6al-4v, Rakesh Rajaram Kamath

Doctoral Dissertations

The overarching goal of this dissertation is to better understand the underlying process-structure relationships in play during the implementation of a spot melt strategy for metal additive manufacturing, which has become a popular alternative to the conventional raster melt strategy for site-specific microstructure control. In the first part of this dissertation, the effect of a spot melt strategy on the solidification texture, variant selection, phase fraction, and their variations along the build height of an E-PBF Ti-6Al-4V is investigated in comparison to a conventional linear melt strategy using high-energy synchrotron x-ray diffraction. In spite of the thermal excursions involved, the …

Additive Manufacturing Of Sub-Micron Features And Mechanical Linkages, David K. Limberg

Doctoral Dissertations

In recent years material constraints have become the limiting factor in several fields, including batteries, robotics, and medicine, and these needs have prompted the development of materials with programmable properties. To this end, much effort has been dedicated to designing metamaterials that have unprecedented optical, mechanical, and thermal properties, along with systems for additive manufacturing to build their complex structures with high precision and throughput. The field of additive manufacturing has proved to be a platform for innovation across many industries yet is still limited with regards to feature sizes, print rates, and diversity of materials. Mechanical devices like linkages …

Processing To Enable Direct-Write Additive Manufacturing Of Ceramics And Ceramic Composites, Austin Martin

Doctoral Dissertations

"This research focuses on the processing of novel feedstocks for and during direct-write additive manufacturing (AM), specifically the direct ink writing (DIW) and Ceramic On-Demand Extrusion (CODE) manufacturing processes, in order to produce ceramic and ceramic-based composite components. Strongly dispersed, concentrated (φ = 0.42), nanoparticle (d₅₀ ~0.3 µm), zirconia (ZrO₂) pastes were used to print densely filled, large continuous volume (≳ 1 cm³) ceramic components. An elastic shear modulus (G’) of 56,000 Pa and yield stresses between 6 and 10 Pa allowed for printed components of 34.5 mm in height over 115 layers without slumping …

Characterization Of High Cycle Fatigue And Laser-Aided Machining And Polishing Of Additively Manufactured Materials, Mohammad Masud Parvez

Doctoral Dissertations

“Additive manufacturing (AM) and laser-aided machining and polishing (LAMP) of materials are emerging manufacturing processes both for research and industrial sectors. The AM process can manufacture near-net-shape parts with complex geometries. Meanwhile, the LAMP process integrated with an AM system offers a high processing rate, minimum heat-affected zone, and easily adjustable process parameters during machining and polishing. In mechanical properties characterization of AM metals and alloys, fatigue is a vitally important test method to understand the behavior of materials in cycling loading and unloading circumstances since most mechanical failures of structures are due to fatigue. To characterize AM metal fatigue …

Identifying An Optimization Technique For Maker Usage To Address Covid-19 Supply Shortfalls, Michael J. Wilson

Doctoral Dissertations

Fused Deposition Modeling (FDM) can be purchased for under five hundred dollars. The availability of these inexpensive systems has created a large hobbyist (or maker) community. For makers, FDM printing is used numerous uses.

With the onset of the COVID-19 pandemic, the needs for Personal Protective Equipment (PPE) skyrocketed. COVID-19 mitigation strategies such as social distancing, businesses closures, and shipping delays created significant supply shortfalls. The maker community stepped in to fill gaps in PPE supplies.

In the case of 3DP, optimization remains the domain of commercial entities. Optimization is, at best, ad-hoc for makers. With the need to PPE …

Structural Stability Of Thermosets During Material Extrusion Additive Manufacturing, Stian K. Romberg

Doctoral Dissertations

Over the past decade, the scale of polymer additive manufacturing has been revolutionized with machines that print massive thermoplastic parts with greater geometric complexity than can be achieved by traditional manufacturing methods. However, the heat required to print thermoplastics consumes energy and induces thermal gradients that can reduce manufacturing flexibility and final mechanical properties. With the ability to be extruded at room temperature and excellent compatibility with fibers and fillers, thermoset resins show promise to decrease the energy consumption, expand the manufacturing flexibility, and broaden the material palette offered by large-scale polymer additive manufacturing. However, structural instability in the uncured …

3d Printing Of Hybrid Architectures Via Core-Shell Material Extrusion Additive Manufacturing, Robert Cody Pack

Doctoral Dissertations

Biological materials often employ hybrid architectures, such as the core-shell motif present in porcupine quills and plant stems, to achieve unique properties and performance. Drawing inspiration from these natural materials, a new method to fabricate lightweight and stiff core-shell architected filaments is reported. Specifically, a core-shell printhead conducive to printing highly loaded fiber-filled inks, as well as a new low-density syntactic foam ink, are utilized to 3D-print core-shell architectures consisting of a syntactic epoxy foam core surrounded by a stiff carbon fiber-reinforced epoxy composite shell. Effective printing of test specimens and structures with controlled geometry, composition, and architecture is demonstrated …

Process-Structure-Property Relationships In 3d-Printed Epoxy Composites Produced Via Material Extrusion Additive Manufacturing, Nadim S. Hmeidat

Doctoral Dissertations

Extrusion-based additive manufacturing (AM) technologies, such as direct ink writing (DIW), offer unique opportunities to create composite materials and novel multi-material architectures that are not feasible using other AM technologies. DIW is a novel 3D-printing approach in which viscoelastic inks, with favorable rheological properties, are extruded through fine nozzles and patterned in a filament form at room temperature.

Recent developments in DIW of polymer composites have led to expanding the range of materials used for printing, as well as introducing novel deposition strategies to control filler orientation and create improved functional/structural composite materials. Despite these substantial advancements, the successful and …

Development Of Data Science Tools For Part Qualification In Additive Manufacturing, Sujana Chandrasekar

Doctoral Dissertations

In recent years, metal additive manufacturing processes have become popular choices for part production especially for low volume, high complexity parts. To enable widespread adoption of these methods, it is essential to understand the link between process parameters and part properties. This is particularly because additive manufacturing processes cause inherently complex thermo-mechanical cycles and drastically different local process conditions within a part, compared to conventional manufacturing processes like casting and forging. Additionally, properties of feedstock material like metal powder impact final part properties. The focus of this dissertation is on development of data-driven methods using in situ monitoring, as a …

Experimental Characterization And Crystal Plasticity Modeling Of Mechanical Properties And Microstructure Evolution Of Additively Manufactured Inconel 718 Superalloy, Saeede Ghorbanpour

Doctoral Dissertations

In this thesis, the mechanical behavior of the additively manufactured (AM) IN718 nickel-based superalloy and their correlations with the evolution of microstructure are studied comprehensively. The effects of manufacturing parameters, build orientations, and post processing procedures, i.e. standard heat treatment and hot isostatic pressing (HIP), on various mechanical properties including monotonic compression and tension strength, low cyclic fatigue performance, high cyclic fatigue behaviour, and fatigue crack growth behavior are investigated. Due to the high temperature applications of the IN718 alloy, elevated temperature properties are examined as well. Electron Backscattered Diffraction (EBSD) technique is employed to measure the initial and deformed …

Fabrication, Characterization Of High-Entropy Alloys And Deep Learning-Based Inspection In Metal Additive Manufacturing, Wenyuan Cui

Doctoral Dissertations

"Alloying has been used to confer desirable properties to materials. It typically involves the addition of small amounts of secondary elements to a primary element. In the past decade, however, a new alloying strategy that involves the combination of multiple principal elements in high concentrations to create new materials called high- entropy alloys (HEAs) has been in vogue. In the first part, the investigation focused on the fabrication process and property assessment of the additive manufactured HEA to broaden its engineering applications. Additive manufacturing (AM) is based on manufacturing philosophy through the layer-by-layer method and accomplish the near net-shaped components …

Additively Manufactured Metallic Cellular Structures, Okanmisope Aziel Fashanu

Doctoral Dissertations

"Cellular structures are lightweight structures with excellent mechanical, thermal, and acoustic properties. They offer promise in a series of applications, including lightweight applications, sandwich cores, mechanical damping, acoustic absorption, strain isolation, and thermal management. The manufacturing of these complex cellular structures is expensive and time-consuming, which hinders the adoption of these structures in many industries. Advancement in manufacturing technologies, such as additive manufacturing (AM), however, have changed this. AM allows for the rapid and less expensive manufacturing of complex cellular structures. This work aimed to investigate the performance of additively manufactured cellular structures for lightweight and sandwich core applications. In …

Layer-To-Layer Feedback Control For Direct Energy Deposition Additive Manufacturing, Michelle Gegel

Doctoral Dissertations

"Additive manufacturing (AM) has garnered much attention in recent years, some calling it the fourth industrial revolution. It was first used to create rapid prototypes, although recent efforts have been made to advance the technology towards production of functional parts. This requires advancement in the materials used in AM, as well as the ability to produce quality parts repeatably. More specifically, direct energy deposition (DED) of metal powders is a process capable of producing and repairing parts with complex geometries; however, it is not widely used in industry due to challenges with quality control. In this process, metal powder is …

Fabrication And Characterization Of Multifunctional Composites, Aditya R. Thakur

Doctoral Dissertations

“This study details the research to facilitate fabrication and characterization of novel structural composites reinforced with carbon fibers. Across industries, materials with high performance-to-weight ratio are sought after. Using carbon fibers as secondary phases in these proposed composites, specific characteristics can be tailored in these materials to manufacture strong, lightweight, high performance structures. The first part of the research focused on the improvement in the mechanical properties of the composites using carbon fiber reinforcement. As a part of this study, toughened ceramic composites with predictable failure patterns were produced using carbon fiber inclusions. A closed-form analytical model was developed to …

Increasing The Functionality Of Additive Manufacturing Through Atmospheric Microplasma And Nanotechnology, Alexander Jon Ulrich

Doctoral Dissertations

Additive Manufacturing (AM) has been changing the manufacturing landscape for the last 20 years. As the interest and demand for both polymer and metal-based 3D printing has grown, the materials and machines used have increased in capabilities. Despite the growth and advancement, there are still a large number of improvements that can be made to add functionality to 3D printers. Metal AM, a subcategory of 3D printing, has garnered much attention among industrial applications with large companies such as General Electric trying to implement the technology to increase innovative designs for motors. Some of the limitations on AM have to …

Mechanical Performance Of Structural Systems With Missing Members: From Buildings To Architected Materials, Panagiotis Pantidis

Doctoral Dissertations

Structural systems are potentially subjected to damage initiating scenarios throughout the course of their service time. Depending on the nature and extent of the damaging event, they may experience significant reduction or even complete loss of their mechanical performance. This dissertation delves into the mechanics of structural systems under the notion of missing members from their domain, investigating types of structural systems: a) multi-story steel framed buildings, and b) materials with a truss-lattice microstructure. Part I of the dissertation investigates the performance of multi-story steel framed buildings under a column removal scenario, developing an analytical framework for their quasi-static robustness …

Design, Fabrication, And Characterization Of Functionally Graded Materials, Sreekar Karnati

Doctoral Dissertations

“The aim of this research was to investigate the feasibility of fabricating custom designed, graded materials using Laser Metal Deposition (LMD) that will cater for functionality and unconventional repair. The ultimate goal of the project is to establish the versatility of LMD for fabricating advanced materials and tackling problems that have been conventionally difficult or in cases infeasible. In order to accomplish these goals, this research involved investigations into, the feasibility of using elemental powders as modular feedstocks, the feasibility of fabricating tailored gradients with these custom compositions, and finally leveraging the advantages of grading materials using LMD to successfully …

Remanufacturing Of Precision Metal Components Using Additive Manufacturing Technology, Xinchang Zhang

Doctoral Dissertations

"Critical metallic components such as jet engine turbine blades and casting die/mold may be damaged after servicing for a period at harsh working environments such as elevated temperature and pressure, impact with foreign objects, wear, corrosion, and fatigue. Additive manufacturing has a promising application for the refurbishment of such high-costly parts by depositing materials at the damaged zone to restore the nominal geometry. However, several issues such as pre-processing of worn parts to assure the repairability, reconstructing the repair volume to generate a repair tool path for material deposition, and inspection of repaired parts are challenging. The current research aims …

Freeform Extrusion Fabrication Of Advanced Ceramics And Ceramic-Based Composites, Wenbin Li

Doctoral Dissertations

"Ceramic On-Demand Extrusion (CODE) is a recently developed freeform extrusion fabrication process for producing dense ceramic components from single and multiple constituents. In this process, aqueous paste of ceramic particles with a very low binder content ( < 1 vol%) is extruded through a moving nozzle to print each layer sequentially. Once one layer is printed, it is surrounded by oil to prevent undesirable water evaporation from the perimeters of the part. The oil level is regulated just below the topmost layer of the part being fabricated. Infrared radiation is then applied to uniformly and partially dry the top layer so that the yield stress of the paste increases to avoid part deformation. By repeating the above steps, the part is printed in a layer-wise fashion, followed by post-processing. Paste extrusion precision of different extrusion mechanisms was compared and analyzed, with an auger extruder determined to be the most suitable paste extruder for the CODE system. A novel fabrication system was developed based on a motion gantry, auger extruders, and peripheral devices. Sample specimens were then produced from 3 mol% yttria stabilized zirconia using this fabrication system, and their properties, including density, flexural strength, Young's modulus, Weibull modulus, fracture toughness, and hardness were measured. The results indicated that superior mechanical properties were achieved by the CODE process among all the additive manufacturing processes. Further development was made on the CODE process to fabricate ceramic components that have external/internal features such as overhangs by using fugitive support material. Finally, ceramic composites with functionally graded materials (FGMs) were fabricated by the CODE process using a dynamic mixing device"--Abstract, page iv.

Repair Of Metallic Components Using Hybrid Manufacturing, Renwei Liu

Doctoral Dissertations

"Many high-performance metal parts users extend the service of these damaged parts by employing repair technology. Hybrid manufacturing, which includes additive manufacturing (AM) and subtractive manufacturing, provides greater build capability, better accuracy, and surface finish for component repair. However, most repair processes still rely on manual operations, which are not satisfactory in terms of time, cost, reliability, and accuracy. This dissertation aims to improve the application of hybrid manufacturing for repairing metallic components by addressing the following three research topics. The first research topic is to investigate and develop an efficient best-fit and shape adaption algorithm for automating 3D models' …

Hierarchical Control Of Complex Manufacturing Processes, Hesam Zomorodi Moghadam

Doctoral Dissertations

"The need for changing the control objective during the process has been reported in many systems in manufacturing, robotics, etc. However, not many works have been devoted to systematically investigating the proper strategies for these types of problems. In this dissertation, two approaches to such problems have been suggested for fast varying systems. The first approach, addresses problems where some of the objectives are statically related to the states of the systems. Hierarchical Optimal Control was proposed to simplify the nonlinearity caused by adding the statically related objectives into control problem. The proposed method was implemented for contour-position control of …

Nanotechnology And Additive Manufacturing Platforms For Clinical Medicine: An Investigation Of 3d Printing Bioactive Constructs And Halloysite Nanotubes For Drug Delivery And Biomaterials, Jeffery A. Weisman

Doctoral Dissertations

Personalized medicine requires the development of new technologies for controlled or targeted drug delivery. Three-dimensional (3D) printing and additive manufacturing techniques can be used to generate customized constructs for bioactive compound delivery. Nanotechnology in the form of nanoparticles, used as a stand-alone construct or for material enhancements, can significantly improve established biomaterials such as PMMA based bone cements or enable new technology to have enhanced capabilities. Combinations of the technologies can be used in such applications as infectious disease treatments, chemotherapeutic targeted drug delivery or targeted delivery of nearly any bioactive compound.

Chemotherapeutic or antibiotic enhanced 3D printing filaments were …