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Full-Text Articles in Engineering

Spark Plasma Sintering Of 2d Nitride And Carbide Based Ceramics, Archana Loganathan Jun 2019

Spark Plasma Sintering Of 2d Nitride And Carbide Based Ceramics, Archana Loganathan

FIU Electronic Theses and Dissertations

Two-dimensional (2D) nanomaterials have stimulated significant interest among materials community due to a wide variety of application ranging from functional to structural properties. Boron nitride nanosheets (BNNS), boron-carbon-nitride (BCN), and MXene (Mn+1Xn, transition metal carbides, nitrides or carbonitrides) belongs to 2D materials family with van der Waals bonding between the layers. The research on synthesis and properties of BNNS, BCN and MXene have been predominantly explored for single- or multi-layered 2D nanosheets. In this study, the focus is to synthesize bulk layered BNNS and BCN using single or multilayered 2D nanomaterials by spark plasma sintering (SPS). …


Influence Of Leading Edge Oscillatory Blowing On Time-Accurate Dynamic Store Separation, Ryan G. Saunders Mar 2019

Influence Of Leading Edge Oscillatory Blowing On Time-Accurate Dynamic Store Separation, Ryan G. Saunders

Theses and Dissertations

The primary objective of this research is to support the static and dynamic characterization and the time-accurate dynamic load data acquisition of store separation from a cavity with leading edge oscillatory blowing. Developing an understanding of, and potentially controlling, pitch bifurcation of a store release is a motivation for this research. The apparatus and data acquisition system was used in a two-part experiment to collect both static and dynamic testing data in the AFIT low speed wind tunnel in speeds of 60, 100, and 120 mph, from Reynolds numbers varying from 5.5x104 to 4.6x105, depending on reference …


Tailoring The Mechanical And Optical Properties Of Silicon-Niobium-Nitride Composite Coatings, Cristian Orozco Jan 2019

Tailoring The Mechanical And Optical Properties Of Silicon-Niobium-Nitride Composite Coatings, Cristian Orozco

Open Access Theses & Dissertations

Nitride nanocomposite thin films have generated significant attention as a result of their robust mechanical properties, excellent triobology, and good chemical (corrosion) stability. Due to their excellent hardness and high wear resistance NbN coatings have found use in a wide variety of applications such as the coating of cutting tools and to strengthen the surface mechanical properties of superconducting cavities. The mechanical properties of NbN can be further improved through mixing with Si3N4, leading to the formation of a nanocomposite structure. NbN-Si3N4 nanocomposite coatings have been actively studied due to their high hardness, high elastic modulus, and high resistance to …


Mechanical Properties And Degradation Of High Capacity Battery Electrodes: Fundamental Understanding And Coping Strategies, Yikai Wang Jan 2019

Mechanical Properties And Degradation Of High Capacity Battery Electrodes: Fundamental Understanding And Coping Strategies, Yikai Wang

Theses and Dissertations--Chemical and Materials Engineering

Rechargeable lithium ion and lithium (Li) metal batteries with high energy density and stability are in high demand for the development of electric vehicles and smart grids. Intensive efforts have been devoted to developing high capacity battery electrodes. However, the known high capacity electrode materials experience fast capacity fading and have limited cycle life due to electromechanical degradations, such as fracture of Si-based electrodes and dendrite growth in Li metal electrodes. A fundamental understanding of electromechanical degradation mechanisms of high capacity electrodes will provide insights into strategies for improving their electrochemical performance. Thus, this dissertation focuses on mechanical properties, microstructure …