Open Access. Powered by Scholars. Published by Universities.®
- Institution
- Keyword
-
- Scanning electron microscopy (27)
- Biodiesel (16)
- Tin (15)
- Wear of materials (15)
- Copper (13)
-
- X ray diffraction analysis (13)
- Nanoparticles (11)
- Silver (11)
- Soldering alloys (11)
- X ray diffraction (10)
- Alternative fuels (9)
- Electrodeposition (9)
- Friction (9)
- Palm biodiesels (9)
- Room temperature (9)
- Tribology (9)
- Wear (9)
- Aluminum (8)
- Automotive materials (8)
- Hardness (8)
- Immersion tests (8)
- Intermetallics (8)
- Microstructure (8)
- Nickel (8)
- Corrosion (7)
- Energy dispersive spectroscopy (7)
- Cast iron (6)
- Diesel (6)
- Differential scanning calorimetry (6)
- FTIR (6)
Articles 31 - 60 of 83
Full-Text Articles in Engineering
Degradation Of Physical Properties Of Different Elastomers Upon Exposure To Palm Biodiesel
Degradation Of Physical Properties Of Different Elastomers Upon Exposure To Palm Biodiesel
A.S. Md Abdul Haseeb
Biodiesel, as an alternative fuel, is gradually receiving more popularity for use in internal combustion engines. However questions continue to arise with regard to its compatibility with elastomeric materials. The present work aims to investigate the comparative degradation of physical properties for different elastomers [e.g. ethylene propylene diene monomer (EPDM), silicone rubber (SR), polychloroprene (CR), polytetrafluroethylene (PTFE) and nitrile rubber (NBR)] upon exposure to diesel and palm biodiesel. Static immersion tests in B0(diesel), B10 (10% biodiesel in diesel), B20, B50 and B100(biodiesel) were carried out at room temperature (25 °C) for 1000 h. Different physical properties like, changes in weight …
Addition Of Cobalt Nanoparticles Into Sn-3.8ag-0.7cu Lead-Free Solder By Paste Mixing
Addition Of Cobalt Nanoparticles Into Sn-3.8ag-0.7cu Lead-Free Solder By Paste Mixing
A.S. Md Abdul Haseeb
Purpose - The purpose of this paper is to investigate the effects of addition Co nanoparticles on the characteristic properties of Sn-3.8Ag-0.7Cu solder. Design/methodology/approach - Cobalt (Co) nanoparticles were added to Sn-Ag-Cu solders by thoroughly blending various weight percentages (0-2.0 wt%) of Co nanoparticles with near eutectic SAC387 solder paste. Blending was done mechanically for 30 min to ensure a homogeneous mixture. The paste mixture was then reflowed on a hot plate at 250°C for 45 s. The melting points of nanocomposite solder were determined by differential scanning calorimetry. Spreading rate of nanocomposite was calculated following the JIS Z3198-3 standard. …
Biodiesel Feasibility Study: An Evaluation Of Material Compatibility; Performance; Emission And Engine Durability
A.S. Md Abdul Haseeb
Biodiesel, derived from the transesterification of vegetable oils or animal fats, is composed of saturated and unsaturated long-chain fatty acid alkyl esters. In spite of having some application problems, recently it is being considered as one of the most promising alternative fuels in internal combustion engine. From scientific literatures, this paper has collected and analyzed the data on both advantages and disadvantages of biodiesel over conventional diesel. Since the aim of this study is to evaluate the biodiesel feasibility in automobiles, the first section is dedicated to materials compatibility in biodiesel as compared to that in diesel. The highest consensus …
Interfacial Reactions Between Sn-3.5 Ag Solder And Ni-W Alloy Films
Interfacial Reactions Between Sn-3.5 Ag Solder And Ni-W Alloy Films
A.S. Md Abdul Haseeb
Nickel based alloys are currently being investigated in an effort to develop stable barrier films between lead free solder and copper substrate. In this study, interfacial reactions between Ni-W alloy films and Sn-3.5 Ag solder have been investigated. Ni-W alloys films with tungsten content in the range of 5.0-18.0 at.% were prepared on copper substrate by electrodeposition in ammonia citrate bath. Solder joints were prepared on the Ni-W coated substrate at a reflow temperature of 250 °C. The solder joint interface was investigated by Cross-sectional scanning electron microscopy, energy dispersive X-ray spectroscopy and electron back scatter diffraction. It has been …
Interfacial Reaction And Dissolution Behavior Of Cu Substrate In Molten Sn-3.8ag-0.7cu In The Presence Of Mo Nanoparticles
A.S. Md Abdul Haseeb
Purpose - In electronic packaging, when solid copper comes in contact with liquid solder alloy, the former dissolves and intermetallic compounds (IMCs) form at the solid-liquid interface. The purpose of this paper is to study the effect of the presence of molybdenum nanoparticles on the dissolution of copper and the formation of interfacial IMC. Design/methodology/approach - Cu wire having a diameter of 250 μm is immersed in liquid composite solders at 250° up to 15 min. Composite solder was prepared by adding various amount of Mo nanoparticles into the Sn-3.8Ag-0.7Cu (SAC) solder paste. The dissolution behavior of Cu substrate is …
Understanding The Effects Of Addition Of Copper Nanoparticles To Sn-3.5 Ag Solder
Understanding The Effects Of Addition Of Copper Nanoparticles To Sn-3.5 Ag Solder
A.S. Md Abdul Haseeb
Purpose - The purpose of this paper is to focus on the fabrication of SAC nanocomposites solder and discuss the effects of nanoCu addition on the structure and properties of resulted nanocomposite solder. Design/methodology/ approach - Ball milling is a nonequilibrium processing technique for producing composite metal particles with submicron homogeneity by the repeated cold welding and fracture of powder particles. This method is believed to offer good processablity, precise control over the solder composition, and produce more homogeneous mixture. Findings - It is found that the melting temperature, the wetting behaviour, and hardness are improved when the Cu nanoparticles …
Failure Analysis Of Retrieved Uhmwpe Tibial Insert In Total Knee Replacement
Failure Analysis Of Retrieved Uhmwpe Tibial Insert In Total Knee Replacement
A.S. Md Abdul Haseeb
This study involves the failure analysis of an ultra high molecular polyethylene (UHMWPE) tibial insert from Apollo® Total Knee System, which was removed after 10. years of service from 70. years old female patient. The tibial insert was investigated by using a stereoscope, scanning electron microscope (SEM), infinite focus microscope (IFM) and energy disperse spectroscopy (EDS) to characterize the morphology and composition of the bearing surface. Differential scanning calorimetry (DSC) and Fourier transform spectroscopy (FTIR) were employed to characterize the degradation and crystallinity of the component. Gel-permeation chromatography (GPC) was used to measure the polyethylene tibial insert molecular weight. Results …
Structural And Mechanical Properties Of Nanostructured Tio2 Thin Films Deposited By Rf Sputtering
Structural And Mechanical Properties Of Nanostructured Tio2 Thin Films Deposited By Rf Sputtering
A.S. Md Abdul Haseeb
This study mainly aims to evaluate the effects of substrate temperatures on the mechanical properties of TiO2 thin films deposited on glass substrates by radio-frequency (RF) magnetron sputtering. All titania films possess anatase structure having a nodular morphology. AES results reveal that Si and Na ions from glass diffuse into TiO2 films at higher substrate temperatures. Micro-scratch and wear tests were conducted to evaluate their mechanical and tribological properties. The adhesion critical loads of TiO2 films deposited at room temperature, 200 and 300°C are found to be 1.51, 1.54 and 1.08N, respectively. Scratch hardness also increases from 11.5 to 13.6GPa …
Comparative Corrosive Characteristics Of Petroleum Diesel And Palm Biodiesel For Automotive Materials
A.S. Md Abdul Haseeb
Corrosive characteristics of biodiesel are important for long term durability of engine parts. The present study aims to compare the corrosion behavior of aluminum, copper and stainless steel in both petroleum diesel and palm biodiesel. Immersion tests in biodiesel (B100) and diesel (B0) were carried out at 80 °C for 1200 h. At the end of the test, corrosion characteristic was investigated by weight loss measurements and changes on the exposed metal surface. Surface morphology was examined by optical microscope and scanning electron microscopy with energy dispersive X-ray analysis (SEM/EDS). Fuels were analyzed by using TAN analyzer, FTIR, GCMS and …
Compatibility Of Elastomers In Palm Biodiesel
Compatibility Of Elastomers In Palm Biodiesel
A.S. Md Abdul Haseeb
In recent time, environmental awareness and concern over the rapid exhaustion of fossil fuels have led to an increased popularity of biodiesel as an alternative fuel for automobiles. However, there are concerns over enhanced degradation of automotive materials in biodiesel. The present study aims to investigate the impact of palm biodiesel on the degradation behavior of elastomers such as nitrile rubber (NBR), polychloroprene, and fluoro-viton A. Static immersion tests in B0 (diesel), B10 (10% biodiesel in diesel), B100 (biodiesel) were carried out at room temperature (25 °C) and at 50 °C for 500 h. At the end of immersion test, …
Influence Of Ni Nanoparticle On The Morphology And Growth Of Interfacial Intermetallic Compounds Between
A.S. Md Abdul Haseeb
TiO2 thin films were deposited on unheated and heated glass substrates at an elevated sputtering pressure of 3 Pa by radio frequency (RF) reactive magnetron sputtering. TiO2 films deposited at room temperature were annealed in air for 1 h at various temperatures ranging from 300 to 600 °C. The structural and optical properties of the thin films were investigated using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and ultraviolet-visible-near infrared (UV-VIS-NIR) spectrophotometry. XRD results show that as-grown and post-annealed TiO2 films have anatase crystal structure. Higher substrate and annealing temperatures result in a slight increase of crystallinity. TiO2 …
Corrosion Characteristics Of Copper And Leaded Bronze In Palm Biodiesel
Corrosion Characteristics Of Copper And Leaded Bronze In Palm Biodiesel
A.S. Md Abdul Haseeb
Biodiesel has become more attractive as alternative fuel for automobiles because of its environmental benefits and the fact that it is made from renewable sources. However, corrosion of metals in biodiesel is one of the concerns related to biodiesel compatibility issues. This study aims to characterize the corrosion behavior of commercial pure copper and leaded bronze commonly encountered in the automotive fuel system in diesel engine. Static immersion tests in B0, B50 and B100 fuels were carried out at room temperature for 2640 h. Similar immersion tests in B0, B100 and B100 (oxidized) fuels were also conducted at 60 °C …
Effect Of Temperature On Tribological Properties Of Palm Biodiesel
Effect Of Temperature On Tribological Properties Of Palm Biodiesel
A.S. Md Abdul Haseeb
Biodiesel, as an alternative fuel is steadily gaining attention to replace petroleum diesel partially or completely. The tribological performance of biodiesel is crucial for its application in automobiles. In the present study, effect of temperature on the tribological performance of palm biodiesel was investigated by using four ball wear machine. Tests were conducted at temperatures 30, 45, 60 and 75 °C, under a normal load of 40 kg for 1 h at speed 1200 rpm. For each temperature, the tribological properties of petroleum diesel (B0) and three biodiesel blends like B10, B20, B50 were investigated and compared. During the wear …
Adhesion And Wear Behavior Of Nanostructured Titanium Oxide Thin Films
Adhesion And Wear Behavior Of Nanostructured Titanium Oxide Thin Films
A.S. Md Abdul Haseeb
No abstract provided.
Investigations On Tio2 And Ag Based Single And Multilayer Films For Window Glazings
Investigations On Tio2 And Ag Based Single And Multilayer Films For Window Glazings
A.S. Md Abdul Haseeb
In this investigation, TiO2 and Ag based single and multilayer-films were deposited on microscope glass slides with varying individual layer thicknesses by radio-frequency reactive magnetron sputtering. Prior to multilayer development, single layers of Ag and TiO2 were deposited and characterized. All the films were prepared at an elevated pressure of 3 Pa at room temperature. It was found that single layer of TiO2 showed anatase polycrystalline structure. It also exhibited high visible transmittance of above 80% and higher refractive index of 2.31 at a wavelength of 550 nm. The indirect optical band gap of the TiO2 films was estimated as …
Influence Of Substrate Temperatures On Structural, Morphological And Optical Properties Of Rf-Sputtered Anatase Tio 2 Films
A.S. Md Abdul Haseeb
In this investigation, TiO 2 thin films were deposited on glass substrates at varying substrate temperatures from room temperature to 300 °C by radio-frequency (RF) magnetron sputtering at an elevated sputtering pressure of 3 Pa. As-deposited TiO 2 films were characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), field emission Auger electron microscopy (FEAES), and UV-visible-NIR spectrophotometry. The XRD results reveal that all the as-deposited films possessing the anatase structure and crystallinity of TiO 2 films appears to deteriorate slightly at higher substrate temperatures. The crystallite size of the as-deposited films at different substrate temperatures …
Selective Area Rare-Earth Doping Of Planar Glass Samples For Monolithic Integration Of Optically Passive And Active Waveguides
A.S. Md Abdul Haseeb
Successful demonstration of selective area doping of planar glass samples for monolithic integration of optically passive and active devices on a single chip is presented. Salt solution of erbium was delivered onto pre-sintered germano-silicate samples via a syringe. The samples were then consolidated to form dense glass layers containing regions doped with rare earth. Erbium tri-chloride solution, 0.1 M, was used during the solution doping phase, with the resulting erbium atomic percentage ranging from more than 0.1-0.4%, increasing linearly with the number of drips applied. © 2008 Elsevier GmbH. All rights reserved.
Structural Investigations On Nanocrystalline Ni-W Alloy Films By Transmission Electron Microscopy
Structural Investigations On Nanocrystalline Ni-W Alloy Films By Transmission Electron Microscopy
A.S. Md Abdul Haseeb
Electrodeposited Ni-W alloys have been investigated in the as-deposited state by transmission electron microscopy in order to investigate the microstructural features in dependence of the tungsten content. Within the tungsten content range from 7 at.% up to 12 at.%, the microstructure is nanocrystalline characterized by a bimodal grain size distribution, consisting out of 20 to 200 nm sized grains and also larger grains with several 100 nm characteristic dimension. No clear trend in microstructure formation is visible with W content or deposition conditions in the investigated W content range. Only solid solution phase characteristics were observed. The lattice constant is …
Spreading Profile Of Dopant Solution On Pre-Sintered Silica Layers For Selective Area Doping Of Integrated Optic Planar Glass Samples
A.S. Md Abdul Haseeb
The spread profile of potassium-permanganate (KMnO4) dye on a porous pre-sintered silica layer deposited via Flame Hydrolysis Deposition is presented. The work is aimed at controlling the dopant profile on the resulting glass layer for optically passive and active devices integration. KMnO4 is used as it allows visual qualification of its spread on the soot layer. Pre-sintered silica layers allow for application of dopants into the glass matrix via adsorption and pore retention. Selective area doping is achieved by applying specific volumes of the dye onto pre-selected areas on the sample using a micropipette. Higher dye volumes applied would result …
Effects Of Annealing Treatment On Optical Properties Of Anatase Tio 2 Thin Films
Effects Of Annealing Treatment On Optical Properties Of Anatase Tio 2 Thin Films
A.S. Md Abdul Haseeb
In this investigation, anatase TiO 2 thin films were grown by radio frequency magnetron sputtering on glass substrates at a high sputtering pressure and room temperature. The anatase films were then annealed at 300-600 °C in air for a period of 1 hour. To examine the structure and morphology of the films, X-ray diffraction (XRD) and atomic force microscopy (AFM) methods were used respectively. From X-ray diffraction patterns of the TiO 2 films, it was found that the as-deposited film showed some differences compared with the annealed films and the intensities of the peaks of the crystalline phase increased with …
Production And Purification Of Zircon Opacifier From Zircon Found In The Coastal Area Of Bangladesh
Production And Purification Of Zircon Opacifier From Zircon Found In The Coastal Area Of Bangladesh
A.S. Md Abdul Haseeb
In this study the potentiality of Bangladesh zircon as a raw material for opacifier was examined. Preparation of zircon flour was done by both wet and dry ball milling. Wet milling of zircon was found to be much efficient than dry milling. Zircon flour of peak size 8 μm obtained by wet milling was purified by leaching in concentrated H2SO4 acid. Leaching time was varied from 2 to 20 h and sulphuric acid concentration ranged from 10 to 80 ml/l. Both un-purified and purified Bangladesh zircon flour were tested for their performance as opacifier in a couple of local ceramic …
Friction And Wear Characteristics Of Electrodeposited Nanocrystalline Nickel-Tungsten Alloy Films
Friction And Wear Characteristics Of Electrodeposited Nanocrystalline Nickel-Tungsten Alloy Films
A.S. Md Abdul Haseeb
Electrodeposited nanocrystalline nickel-tungsten alloys are being investigated as an attractive alternative to electrodeposited nickel for applications involving fabrication of micro electro mechanical systems (MEMS). Ni-W alloys are also being considered as an environmentally friendly alternative to hard chrome plating in some cases. In applications involving sliding contacts such as in micro-gears in MEMS, mould inserts, etc., tribological properties of Ni-W alloys would be of relevance. In this work, the sliding friction and wear characteristics of Ni-W alloys with different tungsten contents were investigated and compared with that of nickel film deposited from sulphamate bath commonly used in microfabrication. For wear …
Liga Fabrication Of Nanocrystalline Ni-W Alloy Micro Specimens From Ammonia-Citrate Bath
Liga Fabrication Of Nanocrystalline Ni-W Alloy Micro Specimens From Ammonia-Citrate Bath
A.S. Md Abdul Haseeb
Ammonia-citrate bath has been investigated for the deposition of nano crystalline Ni-W alloy micro components using the LIGA process. First the bath stability and deposit characteristics were studied. Fabrication of micro specimens were then carried out on silicon substrates covered with novolac as well as thick PMMA resist for LIGA. Effects of different parameters like current density, nickel ion and tungsten ion concentration in the bath, deposition time etc. on the deposit characteristics and current efficiency were studied. The deposited Ni-W samples were characterized by scanning electron microscopy, energy depressive X-ray spectroscopy, light optical microscopy and X-ray diffraction. Results show …
Liga Fabrication Of Nanocrystalline Ni-W Alloy Micro Specimens From Ammonia-Citrate Bath
Liga Fabrication Of Nanocrystalline Ni-W Alloy Micro Specimens From Ammonia-Citrate Bath
A.S. Md Abdul Haseeb
Ammonia-citrate bath has been investigated for the deposition of nano crystalline Ni-W alloy micro components using the LIGA process. First the bath stability and deposit characteristics were studied. Fabrication of micro specimens were then carried out on silicon substrates covered with novolac as well as thick PMMA resist for LIGA. Effects of different parameters like current density, nickel ion and tungsten ion concentration in the bath, deposition time etc. on the deposit characteristics and current efficiency were studied. The deposited Ni-W samples were characterized by scanning electron microscopy, energy depressive X-ray spectroscopy, light optical microscopy and X-ray diffraction. Results show …
Thermal Stability Of Electrodeposited Liga Ni-W Alloys For High Temperature Mems Applications
Thermal Stability Of Electrodeposited Liga Ni-W Alloys For High Temperature Mems Applications
A.S. Md Abdul Haseeb
For thermally stable LIGA materials for high temperature MEMS applications LIGA Ni-W layers and micro testing samples with different compositions (15 and 5 at% W) were electrodeposited. In order to investigate the thermal stability the Ni-W layers were annealed at different temperatures (300-700°C) and for different durations (1, 4, 16 h). Their microstructure and micro-hardness were than analysed after annealing and compared with those of as-deposited states. The observed microstructures show, in comparison to pure LIGA nickel, a small grain growth and a relatively stable structure up to 700°C. The micro-hardness values of the LIGA Ni-W layers are higher than …
Study Of The Wear Behaviour Of Al-4.5% Cu-3.4% Fe In Situ Composite: Effect Of Thermal And Mechanical Processing
A.S. Md Abdul Haseeb
Al-Cu-based MMCs reinforced by Al-Fe intermetallics are investigated for their wear behaviour. The composite (Al-4.5 mass% Cu-3.4 mass% Fe) was produced by solidification processing where the Al-Fe-based intermetallic formed in situ in a matrix of mainly Al-Cu alloy. The effects of thermal and mechanical processing, viz., as-cast condition, solution treatment, aging and hot rolling on the wear behaviour of the composites were examined. The composites were characterized by optical microscopy, SEM, microhardness measurements and X-ray diffraction. The wear behaviour of the composites was studied in a pin-on-disc type wear apparatus. The as-cast in situ composite exhibited the highest wear rate. …
Tribo-Surface Characteristics Of Al-B4c And Al-Sic Composites Worn Under Different Contact Pressures
Tribo-Surface Characteristics Of Al-B4c And Al-Sic Composites Worn Under Different Contact Pressures
A.S. Md Abdul Haseeb
Tribo-surface characteristics of two aluminium metal matrix composites (Al-MMC) of compositions Al-13 vol%B4C and Al-13 vol%SiC sliding against a commercial phenolic brake pad have been investigated under dry conditions. The wear tests were carried out using a pin-on-disc type apparatus at a linear speed of 1.62 m s-1 under contact pressures ranging from 0.75 to 3.00 MPa. The coefficient of friction was recorded on line. Wear rates were calculated from mass loss measurements. Scanning electron microscope equipped with energy dispersive X-ray spectroscopy was used to examine the tribo-surface. It is found that wear rate of both composites increases with increasing …
Chemical And Structural Nature Of Tribo-Surface Of Aluminium-Sic Composites At Nanometre And Micrometre Length Scales
A.S. Md Abdul Haseeb
The worn surface of Al-SiC metal matrix composites (MMC) sliding against phenolic brake pad at a linear sliding speed of 1.62 m s-1 under contact pressures of 0.75-3.00 MPa in a pin-on-disc apparatus was investigated. XPS was used to extract information from the top few nanometres of the worn surface, while scanning electron microscopy and energy dispersive X-ray microanalysis (SEM-EDX) provided information from within a few micrometres. Results reveal that the surface of Al-SiC undergoes significant chemical and physical changes during wear. The tribo-surface on Al-SiC is converted into a mixture that contains the constituents of Al-SiC and the phenolic …
Modeling Of The Effects Of Athermal Flow Strength And Activation Energy For Dislocation Glide On The Nanoindentation Creep Of Nickel Thin Film At Room Temperature
A.S. Md Abdul Haseeb
Nanoindentation creep behaviour of nickel at room temperature has been modeled based on the obstacle-controlled dislocation glide mechanism. Using the model, the effects of two important materials parameters viz. the activation free energy required by dislocation to overcome an obstacle without any aid from external stress, ΔF and the athermal flow strength, τ0, which is the flow strength of solids at 0 K are systematically studied. It has been found that ΔF plays a dominant role in room temperature creep properties of nickel. The role of ΔF is particularly dominant in determining the time dependent deformation. On the other hand, …
A Technical Note On The Production Of Zirconia And Zircon Brick From Locally Available Zircon In Bangladesh
A.S. Md Abdul Haseeb
In this study, the potentiality of Bangladesh zircon as a raw material for zirconia and zircon brick production was examined. Decomposition of zircon (ZrSiO4) into zirconia (ZrO2) was attempted by using caustic soda (NaOH) as the decomposition agent. 5-10 μm size zircon, 5-30 wt.% NaOH, and decomposition temperatures ranging from 1300 to 1500°C were investigated. X-ray diffraction method using Mo Kα radiation was used in order to find out the extent of decomposition of zircon into zirconia. Zircon bricks of 0.06 mm× 0.06 mm× 0.025 mm shaped were made under a pressure of 15 MPa. Carboxi methyal cellulose (CMC) and …