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Full-Text Articles in Engineering

Mathematical Modeling Of The 3(Н)-Quinazolin-4-Onе Synthesis Process, Ziyadullayev Mirjalol, Karimov Rikhsibay, Abdurazakov Asqar, Parmonov Asqar Feb 2021

Mathematical Modeling Of The 3(Н)-Quinazolin-4-Onе Synthesis Process, Ziyadullayev Mirjalol, Karimov Rikhsibay, Abdurazakov Asqar, Parmonov Asqar

CHEMISTRY AND CHEMICAL ENGINEERING

The aim is to optimize the conditions for the synthesis of 3(H)-quinazolin-4-one by the method of mathematical modeling to develop a technology for producing the substance of a new domestic drug used in the treatment of farm animals from helminths. In mathematical modeling, the method of a small number of squares was used. Analytical dependences of the product yield on temperature, reaction time, and molar ratios of the starting materials were determined. A system of linear equations has been compiled. The system of linear equations was performed by the matrix method (A, B, C).The average reaction rate was determined. Based …


Study Of The Influence Of Construction And Mode Parameters On The Hydrodynamics Of A Hollow Vortex Apparatus, Bakhronov Khoshim, Akhmatov Abdumalik, Juraev Dadakhon Feb 2021

Study Of The Influence Of Construction And Mode Parameters On The Hydrodynamics Of A Hollow Vortex Apparatus, Bakhronov Khoshim, Akhmatov Abdumalik, Juraev Dadakhon

CHEMISTRY AND CHEMICAL ENGINEERING

The research was to determine the more efficient design of the swirler from the point of view of hydrodynamics and heat and its optimal parameters. Various swirl designs were manufactured and tested. After preliminary studies conducted on a laboratory installation with a glass working apparatus, several swirlers were selected taking into account their hydraulic resistance, the structure of the swirling gas-liquid flow, and the amount of liquid entrainment by gas. The results of an experimental study of the hydrodynamics of a hollow vortex apparatus with one and two tangential and axial swirlers. Hydraulic losses in the channel and in the …


Ethinylation Reactions Of Some Aldehydes In The Presence Of Phenylacetylene Using High-Base Catalytic Systems, Abdurakhmanova Saida, Ikramov Abduvaxab, Ziyadullayev Odiljon, Ablakulov Lochin Feb 2021

Ethinylation Reactions Of Some Aldehydes In The Presence Of Phenylacetylene Using High-Base Catalytic Systems, Abdurakhmanova Saida, Ikramov Abduvaxab, Ziyadullayev Odiljon, Ablakulov Lochin

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the research work is the development of synthesis methods of aromatic acetylene alcohols and their various derivatives using different catalytic systems and also, determining their structure, physico-chemical and biological properties. The most effective way of synthesizing AAA is determined using selected complex catalytic systems and also, the range of catalytic activity of used catalysts is created. Acetic aldehyde, benzaldehyde and cyclohexonal, high-base catalytic systems − MOH/ДМСО∙H2O and M2CO3/ДMСO∙H2O with phenylacetylene reaction of enantioselective etynilation were investiged. Efficiency and course of chemical reaction in the process of formation acetylene alcohol affection of temperature, reaction duration, solvents, catalysts and …


Synthesis Of Meta-Altered Arylmaleinamide And Preparation Of Esters In Their Presence, Turaeva Khurshida, Yuldasheva Mukhabbat, Khaydarova Sadokat Feb 2021

Synthesis Of Meta-Altered Arylmaleinamide And Preparation Of Esters In Their Presence, Turaeva Khurshida, Yuldasheva Mukhabbat, Khaydarova Sadokat

CHEMISTRY AND CHEMICAL ENGINEERING

The development of new methods of synthesis using cheaper reagents for the preparation of maleic acid derivatives, the study of chemical properties and the determination of new directions for the practical application of maleic acid derivatives are still relevant. Therefore, the development of this work is an urgent task. The aim of this study was to obtain the synthesis of monomaleinamide compounds under various conditions to obtain arylmaleimide derivatives of maleic acid and to transfer them in a pure state for further reactions. In this study, scientific studies were carried out to find convenient methods for the preparation of monoamide …


Development Of Preparations Based On Local Components For Dust Suppression On Quarry Roads, Olikulov Fakhriyor, Mukhiddinov Bakhоdir, Vapoev Khusniddin, Zhurayev Shokhruh Feb 2021

Development Of Preparations Based On Local Components For Dust Suppression On Quarry Roads, Olikulov Fakhriyor, Mukhiddinov Bakhоdir, Vapoev Khusniddin, Zhurayev Shokhruh

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the work is to develop dust-collecting preparations based on local raw materials for the suppression of man-made dust formed on quarry paths. For this purpose, 4 types of the drug were created in the laboratory on the basis of domestic raw materials for dust suppression. The dependence of the viscosity and density of the created preparations on the concentration of components and temperature is studied. For the preparation of the solution of the created drug, a semi-industrial installation is created, which presents the general view and the process of preparing the solution. The spray of the prepared …


Synthesis And Research Of Chelate Forming Sorbent Based On Carbamide, Formaldehyde, Ditizone, Chorieva Nigora, Ermuratova Nilufar, Turaev Khayit, Kasimov Sherzod Feb 2021

Synthesis And Research Of Chelate Forming Sorbent Based On Carbamide, Formaldehyde, Ditizone, Chorieva Nigora, Ermuratova Nilufar, Turaev Khayit, Kasimov Sherzod

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this study is the synthesis and study of a chelating sorbent for the extraction of ions of non-ferrous and noble metals. To achieve this goal, a sulfur-containing chelating sorbent based on carbamide, formaldehyde, and dithizone was synthesized and studied. The optimal conditions for the synthesis of the sorbent have been determined and studies have been carried out on the influence of the molar ratios of the starting materials on the composition, and physicochemical properties of the synthesized sorbent. The optimum temperature of polycondensation was taken as 90 °C, the reaction time is 2.5-3 hours, as a result, …


Synthesis And Spectroscopic Study Of Complex Compounds Of Mn(Ii), Co(Ii), Ni(Ii), Cu(Ii) And Zn(Ii) Acetates With 2-Aminobenzimidazole, Gapurova Lobar, Kadirova Shakhnoza, Rakhmonоva Dilnoza, Olimova Manzura Feb 2021

Synthesis And Spectroscopic Study Of Complex Compounds Of Mn(Ii), Co(Ii), Ni(Ii), Cu(Ii) And Zn(Ii) Acetates With 2-Aminobenzimidazole, Gapurova Lobar, Kadirova Shakhnoza, Rakhmonоva Dilnoza, Olimova Manzura

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the work is to develop a synthesis procedure and obtain new complex compounds of transition metal acetates with 2-aminobenzimidazole (L), to study the composition and structure of the synthesized compounds by elemental, thermal, X-ray phase analysis and IR spectroscopy. A procedure for the synthesis of new complex compounds of Mn(II), Cо(II), Ni(II), Cu(II) and Zn acetates with 2-aminobenzimidazole was developed and the composition and structure of the synthesized complex compounds were studied using modern physicochemical methods. Coordination competing donor centers, electronic and geometric structures of the ligand molecule were studied on the basis of a quantum-chemical calculation …


Effect Of Light On The Resistance Of Bi/Pb Superconductors Synthesized By Solar Energy, Gulamova Dilbara, Echonkulov Elyor, Jalilov Dilshod, Bobokulov Sirojiddin Feb 2021

Effect Of Light On The Resistance Of Bi/Pb Superconductors Synthesized By Solar Energy, Gulamova Dilbara, Echonkulov Elyor, Jalilov Dilshod, Bobokulov Sirojiddin

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the work is to expand the capabilities of solar technologies and areas of practical use of superconductors. The effect of white light on the interaction of superconducting ceramics with a magnet at room temperature was investigated. It has been established that the magnet is “ejected” by ceramic samples of nominal Bi1,7Pb0,3Sr2Ca(n-1)CunOy, (n = 5-20) under the influence of white light and there is no effect in the dark. The resistance of Bi/Pb superconducting ceramics is reduced by exposure to light compared to resistance in the dark. The resistance of ceramics containing higher superconducting higher superconducting phases Tc …


Spectrophotometric Color Determination Of Ceramic Pigments For Construction Ceramics And Regional Innovation System, Kadyrova Dilorom, Mansurov Yulbarskhon, Abdusattarov Shakirjan Feb 2021

Spectrophotometric Color Determination Of Ceramic Pigments For Construction Ceramics And Regional Innovation System, Kadyrova Dilorom, Mansurov Yulbarskhon, Abdusattarov Shakirjan

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this work is the spectrophotometric determination of the color of ceramic pigments for the development of technology for the production of high-quality ceramic paints of a wide color palette for decorating building ceramics, porcelain and faience products. In this regard, using the principles of heterovalent isomorphic substitution of atoms in crystals, the compositions of ceramic pigments were designed on the basis of the anorthite derivatives containing transition elements with the general formula Са1-хMexAl2+xSi2-xО8, where calcium and silicon ions were replaced by aluminum and transition element, Ме – Cо, Ni, Fe, Cr. The color characteristics were taken on …