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Engineering Commons

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Materials Science and Engineering Faculty Publications and Presentations

2019

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Articles 1 - 5 of 5

Full-Text Articles in Engineering

A Parametric Study For In-Pile Use Of The Thermal Conductivity Needle Probe Using A Transient, Multilayered Analytical Model, Courtney Hollar, Austin Fleming, Kurt Davis, Ralph Budwig, Colby Jensen, David Estrada Nov 2019

A Parametric Study For In-Pile Use Of The Thermal Conductivity Needle Probe Using A Transient, Multilayered Analytical Model, Courtney Hollar, Austin Fleming, Kurt Davis, Ralph Budwig, Colby Jensen, David Estrada

Materials Science and Engineering Faculty Publications and Presentations

By utilizing an in-pile measurement, thermal conductivity can be determined under prototypic conditions over a range of burnup. In this work we develop a multilayer quadrupoles analytical model to describe the transient thermal interactions between a line heat source (i.e. needle probe) and cylindrical nuclear fuel geometry for inpile thermal conductivity measurements. A finite element analysis of the detailed needle probe geometry was compared to results from the analytical model to verify the assumptions made in the analytical model. Experimentally, the needle probe was used to measure the thermal properties of polytetrafluoroethylene (PTFE) and stainless steel 304 with three different …


Thermal Transport In Layer-By-Layer Assembled Polycrystalline Graphene Films, David Estrada, Alondra Perez Mar 2019

Thermal Transport In Layer-By-Layer Assembled Polycrystalline Graphene Films, David Estrada, Alondra Perez

Materials Science and Engineering Faculty Publications and Presentations

New technologies are emerging which allow us to manipulate and assemble 2-dimensional (2D) building blocks, such as graphene, into synthetic van der Waals (vdW) solids. Assembly of such vdW solids has enabled novel electronic devices and could lead to control over anisotropic thermal properties through tuning of inter-layer coupling and phonon scattering. Here we report the systematic control of heat flow in graphene-based vdW solids assembled in a layer-by-layer (LBL) fashion. In-plane thermal measurements (between 100 K and 400 K) reveal substrate and grain boundary scattering limit thermal transport in vdW solids composed of one to four transferred layers of …


Corrosion Initiation And Propagation On Carburized Martensitic Stainless Steel Surfaces Studied Via Advanced Scanning Probe Microscopy, Armen Kvryan, Corey M. Efaw, Kari A. Higginbotham, Olivia O. Maryon, Paul H. Davis, Elton Graugnard, Michael F. Hurley Mar 2019

Corrosion Initiation And Propagation On Carburized Martensitic Stainless Steel Surfaces Studied Via Advanced Scanning Probe Microscopy, Armen Kvryan, Corey M. Efaw, Kari A. Higginbotham, Olivia O. Maryon, Paul H. Davis, Elton Graugnard, Michael F. Hurley

Materials Science and Engineering Faculty Publications and Presentations

Historically, high carbon steels have been used in mechanical applications because their high surface hardness contributes to excellent wear performance. However, in aggressive environments, current bearing steels exhibit insufficient corrosion resistance. Martensitic stainless steels are attractive for bearing applications due to their high corrosion resistance and ability to be surface hardened via carburizing heat treatments. Here three different carburizing heat treatments were applied to UNS S42670: a high-temperature temper (HTT), a low-temperature temper (LTT), and carbo-nitriding (CN). Magnetic force microscopy showed differences in magnetic domains between the matrix and carbides, while scanning Kelvin probe force microscopy (SKPFM) revealed a 90–200 …


Open-Source Automated Chemical Vapor Deposition System For The Production Of Two-Dimensional Nanomaterials, Lizandra Williams-Godwin, Dale Brown, Richard Livingston, Tyler Webb, Lynn Karriem, Elton Graugnard, David Estrada Jan 2019

Open-Source Automated Chemical Vapor Deposition System For The Production Of Two-Dimensional Nanomaterials, Lizandra Williams-Godwin, Dale Brown, Richard Livingston, Tyler Webb, Lynn Karriem, Elton Graugnard, David Estrada

Materials Science and Engineering Faculty Publications and Presentations

The study of two- dimensional (2D) materials is a rapidly growing area within nanomaterials research. However, the high equipment costs, which include the processing systems necessary for creating these materials, can be a barrier to entry for some researchers interested in studying these novel materials. Such process systems include those used for chemical vapor deposition, a preferred method for making these materials. To address this challenge, this article presents the first open-source design for an automated chemical vapor deposition system that can be built for less than a third of the cost for a comparable commercial system. The materials and …


Toward Improving Ambient Volta Potential Measurements With Skpfm For Corrosion Studies, Corey M. Efaw, Thiago Da Silva, Paul H. Davis, Lan Li, Elton Graugnard, Michael F. Hurley Jan 2019

Toward Improving Ambient Volta Potential Measurements With Skpfm For Corrosion Studies, Corey M. Efaw, Thiago Da Silva, Paul H. Davis, Lan Li, Elton Graugnard, Michael F. Hurley

Materials Science and Engineering Faculty Publications and Presentations

Scanning Kelvin probe force microscopy (SKPFM) is used in corrosion studies to quantify the relative nobility of different microstructural features present within complex metallic systems and thereby elucidate possible corrosion initiation sites. However, Volta potential differences (VPDs) measured via SKPFM in the literature for metal alloys exhibit large variability, making interpretation and application for corrosion studies difficult. We have developed an improved method for referencing SKPFM VPDs by quantifying the closely related work function of the probe relative to an inert gold standard whose modified work function is calculated via density functional theory (DFT). By measuring and tracking changes in …