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A Guide To Fifty Years Of Research At Montana Tech: Part 3-Decontamination Of Ratioactively Contaminated Steel By Melt Refining/Slagging Processing, Larry G. Twidwell, Samuel A. Worcester

Metallurgy

This presentation includes a discussion of the research conducted at Montana Tech in the Department of Metallurgical and Materials Engineering. The discussion is focused on Decontamination of Radioactively Contaminated Steel by Melt Refining/Slagging. This presentation is based on the research of Master of Science graduate students, industrial and academic colleagues, at the Montana College of Mineral Science and Technology (which morphed to Montana Tech [1977], then to Montana Tech of The University of Montana [2000], then to Montana Technological University [2019]). The referenced work of each of the graduate students in this presentation is gratefully acknowledged. The following summary presentation …

High-Pressure Slurry Ablation For Improving Separation Of Copper/Molybdenum And Flotation Of Gold Tailings, Mitchell Harvey

Graduate Theses & Non-Theses

Disa Technologies’ High-Pressure Slurry Ablation (HPSA) is a patented particle attrition technology for the comminution and selective liberation of minerals. Two slurry streams are pumped at high pressure through opposing nozzles and collisions between solid particles suspended in the slurry streams cause breakage of the feed material. HPSA was evaluated for improving the rougher flotation of molybdenite from Cu-Mo bulk concentrate and gold-bearing pyrite from gold tailings.

Copper/molybdenum samples were provided by Montana Resources in Butte, Montana. A two-factor factorial design of experiments was used to identify HPSA operating conditions which gave the highest increase in flotation performance. Variables were …

Optimization Of Porosity In Cold Spray Produced Copper And Zinc Coatings, Cameron Hughes

Graduate Theses & Non-Theses

Since its invention in 1981, the cold spray (CS) additive manufacturing (AM) process has been studied and optimized to produce well-adhered, dense material coatings. CS can operate at a wide range of temperatures if the feed material remains in a solid state. Copper and zinc were studied to characterize and understand the effects of heating element voltage, travel speed, and standoff distance on deposit porosity, grain size, microhardness, and coating thickness. Samples were sprayed on 3.2 mm x 25 mm x 150 mm 6061 aluminum substrates. Sections were taken from the middle of the samples to represent steady-state conditions. Sample …

The Tempering Response Of Cpm® 3v Tool Steel Investigated Through Tensile Testing And Microstructural Observations, Stephen A.C. Hanson

Graduate Theses & Non-Theses

Heat treatment, tensile testing failure analysis, and microstructural evaluation of the Crucible Industries tool steel CPM® 3V was undertaken to investigate CPM® 3V’s tempering response for the following samples: As-Hardened (no tempering); tempered at 450°C, 550°C, 650°C, and 700°C; and As-Received (annealed). CPM® 3V tool steel is manufactured by Crucible Industries using their proprietary Crucible Particle Metallurgy (CPM®) technology. This material was heat-treated at four different tempering temperatures and was evaluated for tensile properties according to ASTM E8. A TMS landmark tensile fixture was used to establish the ultimate tensile strength and the yield strength of the material for the …

Technical Feasibility Of Selectively Separating Rare Earth Elements By Vapor Phase Extraction And Condensation, Katie Lyons

Graduate Theses & Non-Theses

Experiments were performed to evaluate the technical feasibility of selectively separating selected rare earth halides (bromides and chlorides) using a volatilization and condensation technique. Initially, optimum chloridizing and bromidizing roast parameters were secured in studies performed on reagent grade rare earth oxide samples and subsequently confirmed in tests performed on mineral ore and concentrate samples. The volatilization and condensation experiments were performed by placing the subject rare earth halide samples in an argon-purged multiple-zone tube furnace wherein the temperature profile was controlled to establish separate vaporization and condensation regions. Following each experiment, condensate and solid residue samples were analyzed to …

Vacuum Brazing Of Diamond To Tungsten Carbide, Zhiyong Yin

Graduate Theses & Non-Theses

Diamond tools are increasingly gaining importance as cutting and drilling materials for a wide variety of industrial applications. Polycrystalline diamond (PCD) is the main ultrahard material commercially used in the oil and gas drilling industry. In this study, a reactive brazing process was developed to join polycrystalline diamond (PCD) to WC-13 wt% Co, to form the cutter for fixed-cutter drill bit applications.

Most nonmetals including polycrystalline diamond are not wet by and cannot easily be joined with conventional brazing alloys due to their chemical stability. The experimental approach was first to analyze the effect of adding an active metal (Ti, …

Studies In Modulation Of Interfacial Reactions For Certain Sulphide Minerals, Robert Owen Beyaert

Bachelors Theses and Reports, 1928 - 1970

No abstract provided.

Preliminary Examination Of The Aluminum Corner Of The Ternary System Aluminum-Silver-Indium (A1-Ag-In), Jerome J. Blake

Bachelors Theses and Reports, 1928 - 1970

In this paper the author attempts to lay the groundwork for future work on the Al-Ag-In system.

Production Of Standard-Grade Ferromanganese In An Electric Arc Furnace, Force F. Baney Jr.

Bachelors Theses and Reports, 1928 - 1970

The investigations conducted in this project were essentially concerned with the effects of various compositions of two different slag systems upon the increased recovery of manganese in a standard-grade ferromanganese.

Investigation Of The Ternary System Silver-Aluminum-Indium (Ag-Al-In), Elvin H. Beardslee

Bachelors Theses and Reports, 1928 - 1970

This thesis paper contains material pertaining to & preliminary investigation of the ternary system Ag-Al-In. Procedures in this preliminary investigation are discussed in detail.

Crystal Habit Modification Of Sodium Chlorate, Michael R. Keegan

Bachelors Theses and Reports, 1928 - 1970

All single crystals have a particular habit or morphology. The crystal habit refers to the relative degree of development of crystallographic planes into surfaces which make up the external appearance of the single crystal.

In this paper, NaClO3 is used as a parent crystal. Its simple cubic habit is modified to tetrahedral by the use of impurities of SO4=, S2O3=, Cr2O7=, and NO3-. The degree of habit change is studied as a function of impurity concentration and temperature. The problem and phenomena are explained in terms of surface chemistry and thermodynamics.

Physico-Chemical Principles Of Sixteenth Century Metallurgy, Robert E. Johnson

Bachelors Theses and Reports, 1928 - 1970

Following a review of sixteenth century metallurgical literature and a discussion of Gibbs free energy, this thesis discusses thermodynamic considerations of galena (PbS) reduction by iron from a lead assay of this period. The importance of fluxes in this assay is emphasized. The discussion covers both equilibrium and non-equilibrium conditions at 1100 degrees Celsius. Possible substitutes for iron are also covered.

Information from twenty-one small controlled lead assays is correlated with the thermodynamic discussion to determine the purpose of each constituent in the assay.

The Beneficiation Of Titaniferous-Magnetite Sands, Ronald Lloyd Nordwick

Bachelors Theses and Reports, 1928 - 1970

The purpose of this investigation of beneficiation methods is to develop and study possible economic methods for recovering an iron-titanium concentrate of sufficient purity to meet metallurgical requirements for subsequent direct reduction to pig iron and a high titanium slag.

Stress-Corrosion Cracking Of Brass, Paul A. Fossey

Bachelors Theses and Reports, 1928 - 1970

the mechanism of stress-corrosion cracking of brass has been sought for many years. Investigators have proposed many mechanisms, but each of these mechanisms has always had several drawbacks. This paper presents an account of experimental work done in the laboratory on this subject and compares it to the work of previous investigations. It evaluates the mechanisms presented by investigators and shows the failures of these mechanisms. A theory of Nitrogen Embrittlement is presented and an evaluation of this theory with experimental work follows.

Experimental Arc Furnace Smelting Of Titaniferous Iron Sands From The Northern Oregon Coast, Allan P. Herring

Bachelors Theses and Reports, 1928 - 1970

This investigation is an attempt to experimentally smelt titaniferous iron sands from the Northern Oregon Coast in a laboratory arc furnace.

The Effect Of Ph Upon Chelation Reactions In Montmorillonite Clays, Joseph Michael Keane

Bachelors Theses and Reports, 1928 - 1970

The purpose of this thesis is to investigate several chelation reactions and determine the effect of variable pH upon these reactions.

An Investigation Of The Sintering Of Iron-Wire Compacts, George L. Vivian

Bachelors Theses and Reports, 1928 - 1970

A study of the sintering of iron has been made by observing the rate of bonding of iron wires wound on iron spools. The specimens were sintered at a constant temperature of 850c in vacuum furnaces capable of producing pressures of 10-5 to 10-4 mm of mercury, and the growth of the bond between wires was observed as a function of time.

It has been concluded that the volume-diffusion mechanism is strongly operating in the sintering of iron at 850c, but in an evacuated system, the evaporation-condensation mechanism also contributes to the sintering process.

The Identification Of Montana Clays By X-Ray Analysis, David Stephen Malyevac

Bachelors Theses and Reports, 1928 - 1970

The purpose of this study is to identify the various Montana clay minerals by means of X-ray diffraction. The ultimate aim of this investigation is to identify the different clay mixtures through an analysis of their respective diffraction patterns, and diffraction patterns obtained after various chemical and thermal treatments.

Investigation Of Inclusions In Armco Ingot Iron, Edwin J. Duncan

Bachelors Theses and Reports, 1928 - 1970

Various chemical and electrolytic separation methods were investigated in an attempt to separate the in­clusions in Armco ingot iron. Residues obtained were X-rayed for identification purposes. The microstruc­tures of this iron were studied with the object of de­termining the relative sizes, locations, and possible compositions of the inclusions.

The Design And Construction Of An Electrolytic Cell For Aluminum Reduction, Thomas H. Melrose

Bachelors Theses and Reports, 1928 - 1970

The purpose of this investigation was to design and construct a laboratory size electrolytic cell in which to reduce alumina, using the same basic materials that are used in a commercial size cell. The cell was designed to have a capacity of approxi­mately 100 grams of metallic aluminum produced every 8 hours. The cell was constructed so it could be operated continuously.

Effect Of Recovery On The Recrystallized Grain-Size Of High Purity Aluminum, Rodney L. Helterline

Bachelors Theses and Reports, 1928 - 1970

When a cold-worked metal is annealed, it’s physical properties hange as a result of a new grain structure. The annealing treatment is divided into three stages according to the changes that occur in the distorted metal: (1) recovery, (2) recrystallization, and (3) grain growth.

Geology Of The Ragged Point Oil Field Musselshell County, Montana, David M. Amos

Bachelors Theses and Reports, 1928 - 1970

The Ragged Point oil field is located in Northwest Musselshell County, in the Lake Basin field of central Mon­tana, and on the western border of the Great Plains region. The surface topography is that of a plain marked by erosion and moderate folding. The stratigraphy of central Montana shows periodic marine invasions from the Cordilleran trough, with normal marine limestones interbedded with sandstone sand shales. These sediments are over 12,000 feet thick, with the Creta­ceous Eagle and Colorado formations exposed at the surface on the Ragged Point anticline. Undifferentiated Cambrian lime­stones and shales are the oldest rocks encountered in drilling.

Polarography Of Indium, John Jackson

Bachelors Theses and Reports, 1928 - 1970

The purpose of this thesis is to study the various aspects of the polarography of indium. The eventual goal would be to develop a method of analyzing indium in unknowns. The investigation is approached by studying the indium ions in various electrolytes and in various concentrations.

The Application Of Electric Energy To The Metallurgy Plants In Montana, Edwin J. Duncan

Bachelors Theses and Reports, 1928 - 1970

Since the year 1800, metallurgy has been affiliated with electricity. In fact, the two industries have grown side by side, being naturally dependent upon each other and having a parallel growth.

The Construction And Operation Of A Universal Specimen Mount With Protective Lead Shield For The Purpose Of Determining Pole Figures Using The Schulz-Decker Transmission Technique, Richard L. Fausner

Bachelors Theses and Reports, 1928 - 1970

It was the purpose of this study to construct a universal mount, to construct a protective lead shield, to operate the instrument, and to provide a pole figure using the transmission method of Schulz and Decker. There are at present several lengthy x-ray methods of determining the grain orientation of metals. These methods are mainly photographic. In order to provide a rapid means of obtaining the necessary information concerning the grain orientation of a metal, a universal mount was constructed.

The Lucky Hit Mine Of Jefferson County, Montana, Bruce B. Goddard

Bachelors Theses and Reports, 1928 - 1970

Many mines in the Cardwell Mining District have been more or less steady producers of gold, silver, lead and zinc since 18SO. The area first came into prominence with the discovery of gold at the Mayflower Mine in 1896. Soon after the Mayflower discovery, many claims were located in the nearby Saint Paul Gulch area, northeast of Whitehall. The Lucky Hit Mine is located in Saint Paul Gulch area of the Cardwell Mining District.

Nonmetallic Mineral Resources Of Montana (Except Fuels), F. L. Rytlewski

Bachelors Theses and Reports, 1928 - 1970

Essentially, the paper is composed of seven parts, each of which concerns a group of related nonmetallic minerals such as ceramic materials, gemstones, or abra­sives. Following the data pertaining to the minerals of each group are index mars locating the major mineral deposits which are known to date. Production and reserve figures are listed by tables in cases where such information is available.

The Flotation Concentration Of A Complex Low-Grade Lead Zinc Ore, Edward James Fong

Bachelors Theses and Reports, 1928 - 1970

This report is concerned primarily with the beneficiation of a low-grade complex lead-zinc ore. The depletion of high grade veins has caused the mineral engineer to seek deposits deeper in the earth's crust or to find lower grade deposits. The other alternative has placed more research problems on Mineral Dressing Engineers in particularly the iron, copper, lead and zinc fields.

Host Rocks And Gangue Minerals Associated With Copper Deposits In Plutonic Igneous Rocks, Richard D. Montgomery

Bachelors Theses and Reports, 1928 - 1970

All of the information on the various districts has come directly from published reports. The investigation was suggested by Mr. Forbes Robertson. The geographical extent of the deposits was confined to the western United States. Many of these deposits are of the disseminated porphyry type. A few of the de­posits, such as at Butte, Montana, were of the fissure vein type.

Studies Of Tempering Behavior Of Steel X-9165 Of N-A-X 9100 Series, James A. Ndulue

Bachelors Theses and Reports, 1928 - 1970

One of the reasons why steel is the most versatile of all the metals available for engineering applications is because of the wide range of properties that can be obtained from it by proper heat treatment.