Engineering Commons^™

The Analysis Of Mechanical Exfoliation Of Graphene For Various Fabrication And Automation Techniques, Lance Yarbrough

Mechanical Engineering Undergraduate Honors Theses

Mechanical Exfoliation of Graphene is an often-overlooked portion of the fabrication of quantum devices, and to create more devices quickly, optimizing this process to generate better flakes is critical. In addition, it would be valuable to simulate test pulls quickly, to gain insight on flake quality of various materials and exfoliation conditions. Physical pulls of graphene at various temperatures, pull forces, and pull repetitions were analyzed and compared to the results of ANSYS simulations, solved for similar results. Using ANSYS’ ability to predict trends in exfoliations, flake thickness and coverage using stress and deflection analyses were investigated. Generally, both strongly …

Towards A Practical Method For Monitoring Kinetic Processes In Polymers With Low-Frequency Raman Spectroscopy, Robert Vito Chimenti

Theses and Dissertations

Unlike liquids and crystalline solids, glassy materials exist in a constant state of structural nonequilibrium. Therefore, a comprehensive understanding of material kinetics is critical for understanding the structure-property-processing relationships of polymeric materials. Amorphous materials universally display low-frequency Raman features related to the phonon density of states resulting in a broad disorder band for Raman shifts below 100 cm-1, which is related to the conformational entropy and the modulus. This disorder band is dominated by the Boson peak, a feature due to phonon scattering because of disorder and can be related to the transverse sound velocity of the material, and a …

Low Cost Magnetometer Calibration And Distributed Simultaneous Multipoint Ionospheric Measurements From A Sounding Rocket Platform, Joshua W. Milford

Doctoral Dissertations and Master's Theses

Low-cost and low-size-weight-and-power (SWaP) magnetometers can provide greater accessibility for distributed simultaneous measurements in the ionosphere, either onboard sounding rockets or on CubeSats. The Space and Atmospheric Instrumentation Laboratory (SAIL) at Embry-Riddle Aeronautical University has launched a multitude of sounding rockets in recent history: one night-time mid-latitude rocket from Wallops Flight Facility in August 2022 and three mid-latitude rockets from White Sands Missile Range during the October 2023 annular solar eclipse. All rockets had a comprehensive suite of instruments for electrodynamics and neutral dynamics measurements. Among this suite was one science-grade three-axis fluxgate magnetometer (Billingsley TFM65VQS / TFM100G2) and up …

Analyzing The Influence Of Design And Operating Conditions On Combustion And Emissions In Premixed Turbulent Flames: A Comprehensive Review, Medhat Elkelawy Prof. Dr. Eng., E. A. El Shenawy Prof. Dr., Hagar Alm-Eldin Bastawissi, Ibrahim Ali Mousa Eng., Mohamed M. Abdel-Raouf Ibrahim Dr. Eng.

Journal of Engineering Research

Recently, premixed combustion has dominated the field of combustion research worldwide. The current work is a review that addresses the effects of design and operating regimes on the combustion and emission characteristics of premixed turbulent flames. The study accounts for recent developments aimed at overcoming combustor operability issues that influence emissions and flame stability. Various experimental setups have been utilized in investigations, with results pertaining to performance and emissions concerning premixed turbulent flames. Thus, the objective of this paper is to provide a comprehensive review of the effects of swirl vane angles and equivalence fuel-air ratios for tests conducted both …

Advancements In Characterization Of Ancient Potteries From Southeast Asia: A Review Of Analytical Techniques, Chitnarong Sirisathitkul

Makara Journal of Science

Ancient potteries offer valuable information regarding technological advancements, life dynamics, cultural diversity, and trade routes in the past. Earthenware, stoneware, and porcelain from Southeast Asia have been characterized using several analytical techniques, as reviewed in this article. Fluorescent and diffracted X-rays give rise to elemental and phase compositions, respectively. Examination of molecular bonds requires vibrational spectroscopy, which is useful for the identification of organic materials in ancient potteries. With the advent of portable X-ray fluorescence and Raman spectrometry, on-site analysis of archeological ceramics is now possible. For in-depth analysis, synchrotron light sources can provide new insights into artifacts through X-ray …

Effect Of Fabrication Parameters On The Ferroelectricity Of Hafnium Zirconium Oxide Films: A Statistical Study, Guillermo A. Salcedo, Ahmad E. Islam, Elizabeth Reichley, Michael Dietz, Christine M. Schubert Kabban, Kevin D. Leedy, Tyson C. Back, Weison Wang, Andrew Green, Timothy S. Wolfe, James M. Sattler

Faculty Publications

Ferroelectricity in hafnium zirconium oxide (Hf_1−xZr_xO₂) and the factors that impact it have been a popular research topic since its discovery in 2011. Although the general trends are known, the interactions between fabrication parameters and their effect on the ferroelectricity of Hf_1−xZr_xO₂ require further investigation. In this paper, we present a statistical study and a model that relates Zr concentration (x), film thickness (t_f), and annealing temperature (T_a) with the remanent polarization (P_r) in tungsten (W)-capped Hf_1−xZr_xO₂. …

Investigation Of Gas Dynamics In Water And Oil-Based Muds Using Das, Dts, And Dss Measurements, Temitayo S. Adeyemi

LSU Master's Theses

Reliable prediction of gas migration velocity, void fraction, and length of gas-affected region in water and oil-based muds is essential for effective planning, control, and optimization of drilling operations. However, there is a gap in our understanding of gas behavior and dynamics in water and oil-based muds. This is a consequence of the use of experimental systems that are not representative of field-scale conditions. This study seeks to bridge the gap via the well-scale deployment of distributed fiber-optic sensors for real-time monitoring of gas behavior and dynamics in water and oil-based mud. The aforementioned parameters were estimated in real-time using …

6d Single-Fluorogen Orientation-Localization Microscopy For Elucidating The Architecture Of Beta-Sheet Assemblies And Biomolecular Condensates, Tingting Wu, Weiyan Zhou, Jai S. Rudra, Rohit V. Pappu, Matthew D. Lew

Electrical & Systems Engineering Publications and Presentations

We develop six-dimensional single-molecule orientation-localization microscopy (SMOLM) to measure the 3D positions and 3D orientations simultaneously of single fluorophores. We show how careful optimization of phase and polarization modulation components can encode phase, polarization, and angular spectrum information from each fluorescence photon into a microscope’s dipole-spread function. We used the transient binding and blinking of Nile red (NR) to characterize the helical structure of fibrils formed by designed amphipathic peptides, KFE8^L and KFE8^D, and the pathological amyloid-beta peptide Aβ42. We also deployed merocyanine 540 to uncover the interfacial architectures of biomolecular condensates.

Adsorption Of Crystal Violet Dye From Synthetic Wastewater By Ball-Milled Royal Palm Leaf Sheath, Neloy Sen, Nawrin Rahman Shefa, Kismot Reza, Sk Md Ali Zaker Shawon, Md. Wasikur Rahman

Physics and Astronomy Faculty Publications and Presentations

The current study shows that using a batch approach to remove crystal violet dye from synthetic wastewater is feasible when using royal palm leaf sheath powder as an adsorbent. In order to investigate the effects of many parameters, including starting concentration, pH effect, dye concentration, adsorbent dose, contact time, and temperature, experiments were carried out under various operating conditions. Maximum removal was obtained at pH 6 and at a concentration of 100 ppm, which are considered as ideal values. The influence of pH and dye concentration was shown to be substantial. Langmuir, Freundlich, and Temkin isotherm models were fitted to …

Development Of An Integrated Workflow For Nucleosome Modeling And Simulations, Ran Sun

Doctoral Dissertations

Nucleosomes are the building blocks of eukaryotic genomes and thus fundamental to to all genetic processes. Any protein or drug that binds DNA must either cooperate or compete with nucleosomes. Given that a nucleosome contains 147 base pairs of DNA, there are approximately 4^147 or 10^88 possible sequences for a single nucleosome. Exhaustive studies are not possible. However, genome wide association studies can identify individual nucleosomes of interest to a specific mechanism, and today's supercomputers enable comparative simulation studies of 10s to 100s of nucleosomes. The goal of this thesis is to develop and present and end-to-end workflow that serves …

The Behavior Of ½⟨111⟩ Screw Dislocations In W–Mo Alloys Analyzed Through Atomistic Simulations, Lucas A. Heaton, Kevin Chu, Adib J. Samin

Faculty Publications

Analyzing plastic flow in refractory alloys is relevant to many different commercial and technological applications. In this study, screw dislocation statics and dynamics were studied for various compositions of the body-centered cubic binary alloy tungsten–molybdenum (W–Mo). The core structure did not appear to change for different alloy compositions, consistent with the literature. The pure tungsten and pure molybdenum samples had the lowest plastic flow, while the highest dislocation velocities were observed for equiatomic, W_0.5Mo_0.5 alloys. In general, dislocation velocities were found to largely align with a well-established dislocation mobility phenomenological model supporting two discrete dislocation mobility regimes, …

Modeling Thermosyphon And Heat Pipe Performance For Mold Cooling Applications, Dwaipayan Sarkar

Electronic Thesis and Dissertation Repository

Thermosyphons are enhanced heat transfer devices that can continuously transfer very large amounts of heat rapidly over long distances with small temperature differences. The high heat transfer rate is achieved through simultaneous boiling and condensation of the working fluid and the continuous heat transfer is achieved through recirculation of the working fluid in its liquid and vapor phase. A potentially important application of the thermosyphons has been towards reducing the cycle times of the mold cooling processes which would provide economic incentives to the automotive industry.

Different operational and geometrical parameters such as the input heating power, fill ratio (FR), …

Residual Optical Absorption From Native Defects In Cdsip2 Crystals, Timothy D. Gustafson, Nancy C. Giles, Elizabeth M. Scherrer, Kevin T. Zawilski, Peter G. Schunemann, Kent L. Averett, Jonathan E. Slagle, Larry E. Halliburton

Faculty Publications

CdSiP₂ crystals are used in optical parametric oscillators to produce tunable output in the mid-infrared. As expected, the performance of the OPOs is adversely affected by residual optical absorption from native defects that are unintentionally present in the crystals. Electron paramagnetic resonance (EPR) identifies these native defects. Singly ionized silicon vacancies (V^-_Si) are responsible for broad optical absorption bands peaking near 800, 1033, and 1907 nm. A fourth absorption band, peaking near 630 nm, does not involve silicon vacancies. Exposure to 1064 nm light when the temperature of the CdSiP₂ crystal is near 80K converts …

Disaggregating Longer-Term Trends From Seasonal Variations In Measured Pv System Performance, Chibuisi Chinasaokwu Okorieimoh, Brian Norton, Michael Conlon

Articles

Photovoltaic (PV) systems are widely adopted for renewable energy generation, but their performance is influenced by complex interactions between longer-term trends and seasonal variations. This study aims to remove these factors and provide valuable insights for optimising PV system operation. We employ comprehensive datasets of measured PV system performance over five years, focusing on identifying the distinct contributions of longer-term trends and seasonal effects. To achieve this, we develop a novel analytical framework that combines time series and statistical analytical techniques. By applying this framework to the extensive performance data, we successfully break down the overall PV system output into …

Effective Drag Coefficient Prediction On Single-View 2d Images Of Snowflakes, Cameron Hudson

Graduate College Dissertations and Theses

The drag coefficient of snowflakes is an crucial particle descriptor that can quantify the relationships with the mass, shape, size, and fall speed of snowflake particles. Previous studies has relied on estimating and improving empirical correlations for the drag coefficient of particles, utilizing 3D images from the Multi-Angled Snowflake Camera Database (MASCDB) to estimate snowflake properties such as mass, geometry, shape classification, and rimming degree. However, predictions of the drag coefficient with single-view 2D images of snowflakes has proven to be a challenging problem, primarily due to the lack of data and time-consuming, expensive methods used to estimate snowflake shape …

Electrochromic Polymers: From Electrodeposition To Hybrid Solid Devices, Haradou Sare, Dongmei Dong

Faculty Scholarship for the College of Science & Mathematics

This paper reports on the linear colorimetric and electrochromic (EC) characteristics of electrodeposited polyaniline (PANI) films. This paper also investigates the infrared EC properties of acid-doped PANI films. The electrochemical polymerization method was employed to create a porous and thin PANI film layer onto PET-ITO substrates. This layer was capped with WO3 film to create a gel electrolyte sandwich structure that demonstrates the compatibility of PANI films with cathodic WO3 films in full devices. The electrodeposition of the film was fabricated by applying different voltages and time, with the optimal film quality achieved with the 1.7 V voltage and a …

Reducing Food Scarcity: The Benefits Of Urban Farming, S.A. Claudell, Emilio Mejia

Journal of Nonprofit Innovation

Urban farming can enhance the lives of communities and help reduce food scarcity. This paper presents a conceptual prototype of an efficient urban farming community that can be scaled for a single apartment building or an entire community across all global geoeconomics regions, including densely populated cities and rural, developing towns and communities. When deployed in coordination with smart crop choices, local farm support, and efficient transportation then the result isn’t just sustainability, but also increasing fresh produce accessibility, optimizing nutritional value, eliminating the use of ‘forever chemicals’, reducing transportation costs, and fostering global environmental benefits.

Imagine Doris, who is …

Numerical Study Of Owls' Leading-Edge Serrations, Asif Shahriar Nafi, Nikolaos Beratlis, Elias Balaras, Roi Gurka

Physics and Engineering Science

Owls' silent flight is commonly attributed to their special wing morphology combined with wingbeat kinematics. One of these special morphological features is known as the leading-edge serrations: rigid miniature hook-like patterns found at the primaries of the wings' leading-edge. It has been hypothesized that leading-edge serrations function as a passive flow control mechanism, impacting the aerodynamic performance. To elucidate the flow physics associated with owls' leading-edge serrations, we investigate the flow-field characteristic around a barn owl wing with serrated leading-edge geometry positioned at 20° angle of attack for a Reynolds number of 40 000. We use direct numerical simulations, where …

Combined Risk Based Inspection And Fault Tree Analysis For Repetitive 3-Phase Line Piping Leakage At West Java Offshore Topside Facility, Dona Yuliati, Akhmad Herman Yuwono, Datu Rizal Asral, Donanta Dhaneswara

Journal of Materials Exploration and Findings (JMEF)

Hydrocarbon releases might result in serious consequences in various aspects. In addition to the contribution to environmental pollution, repetitive leakages need high repair costs. This study aim is to minimize potential repetitive leakage for other typical 3-phase piping systems. We conducted the risk assessment by adopting Risk Based Inspection (RBI) API 581 to identify risk level, calculating piping lifetime, recommended inspection plan and mitigations. The most relevant root causes can be obtained through quantitative Fault Tree Analysis (FTA). Observation and investigation was taken from eight 3-phase piping systems that experienced repetitive leakages. It has been found that the risk level …

Nitrogen Gas Quenching Pressure Effect On Bs S155 Alloy Steel In Vacuum Furnace, Agus Mulyadi Hasanudin, Eddy Sumarno Siradj

Journal of Materials Exploration and Findings (JMEF)

The production of metal and alloy products requires the use of heat treatment, when during the heat treatment process, quenching is a crucial step. The quenching medium can be anything from water, a salt bath, oil, air and gas. In a vacuum furnace, pressurized gas, most frequently nitrogen (N₂) gas, serves as one of the quenching mediums. One of the drawbacks of the quenching process is the distortion and dimensional change of the parts. This paper aims to investigate the influence of nitrogen gas quenching pressure on the distortion and dimensional change of aerospace actuator gear planet parts …

Volumetric Imaging Using The Pupil-Matched Remote Focusing Technique In Light-Sheet Microscopy, Sayed Hassan Dibaji Foroushani

Optical Science and Engineering ETDs

ABSTRACT

The dissertation explores innovative techniques in light sheet microscopy, a pivotal tool in biomedical imaging, to enhance its speed, resolution, and efficiency in capturing dynamic biological processes. Light sheet microscopy allows for quick 3D imaging of biological specimens ranging from cells to organs with high spatiotemporal resolution, large field-of-view, and minimal damage, making it vital for in vivo imaging.

The first project introduces a novel optical concept designed to optimize Axially Swept Light Sheet Microscopy (ASLM). This technique is crucial for imaging specimens ranging from live cells to chemically cleared organs due to its versatility across different immersion media. …

Fe Analysis Of Tsunami Generation During The Genesis Flood, Tim Lewis, John Baumgardner

Proceedings of the International Conference on Creationism

Within the framework of catastrophic plate tectonics, large tsunamis are a plausible mechanism for producing fossil-bearing sediments of the Flood rock record. The focus of this research is to model the behavior of an overriding slab in response to a rapidly subducting plate with the aim of understanding in more detail the tsunami generation process. Key to this process is the locking and unlocking of the overriding and subducting slabs. The unlocking results in the rapid rise of the sea bottom and generation of a tsunami. Several key questions arise in this context that the model seeks to answer. What …

Modeling The Process Of Rapid Geomagnetic Reversal During The Genesis Flood, Eric T. Katzaman, John Baumgardner

Proceedings of the International Conference on Creationism

Remnant magnetization in the Earth’s igneous rocks document that the Earth’s magnetic field reversed its polarity many times during the Genesis Flood. Previous creationist research has argued that strong convective buoyancy within the Earth’s liquid outer core during the Flood can cause the expulsion of magnetic flux outward from the core into the overlying mantle which produces rapid reversals of the Earth’s surface dipolar magnetic field. This poster reports the status of our efforts to model this dynamic process in 3D spherical geometry using a magnetohydrodynamic numerical solver.

Dynamic Recrystallization And Grain Size Effects On Catastrophic Motion Of The Earth’S Mantle During The Flood: Advancement Of Material Models, Heechen Cho, John Baumgardner, Maria Lee, Caleb Miller, Mark Horstemeyer

Proceedings of the International Conference on Creationism

This presentation reports a numerical study to investigate the mechanical effects of dynamic recrystallization (DRX) and the grain size on the speed of flow of rock inside the earth’s solid mantle during the Genesis Flood. The strength, or viscosity, of its constituent minerals is key to understanding and modeling the dynamics of the mantle correctly. A mineral’s strength is strongly influenced by the crystal size, its lattice defects (vacancies and dislocations), and other microscale and crystal-scale phenomena. Since the viscosity difference of the earth’s deep mantle between the present day and during the Flood cataclysm is approximately 10 orders of …

Tapping The Hourglass: Disequilibrium Relaxation Following Accelerated Nuclear Decay, Nathan Mogk

Proceedings of the International Conference on Creationism

In 2005, the Radioisotopes and the Age of The Earth (RATE) research initiative published compelling evidence for at least one episode of past radioactive decay which was accelerated by orders of magnitude compared with the rates measured in recent years. Constancy of radioactive decay rates is a central assumption in radiometric dating. Accelerated nuclear decay (AND) causes systematic change in the results of radiometric dating beyond the in situ above normal accumulation of daughter products. This includes relaxation of magma reservoirs to equilibrium and excessive inheritance arising from disequilibrium excesses of daughter products of greater order than crystal-melt partition ratios. …

Language, Coded Instructions And The Interaction With Thermodynamics, Andy C. Mcintosh

Proceedings of the International Conference on Creationism

The theme of the 9th ICC is Developing and Systematizing the Creation Model of Origins. Following this theme, the proposed paper seeks to establish a rigorous and systematic approach to the important area of information and its interface with the substrate on which the information is expressed. This must first involve the understanding of the laws of thermodynamics not only for isolated systems but for closed (where only energy is allowed to cross the boundary) and open systems (where both matter and energy are allowed to cross the boundary). This is particularly an issue with the second law of …

Cause Of Large Post-Flood Jump In Earth's Carbon 14, D Russell Humphreys

Proceedings of the International Conference on Creationism

Accelerated fusion in the Sun during the flood caused large post-flood jump in Earth’s ¹⁴C

D. Russell Humphreys

Creationists studying carbon-14 dating are generally aware of the need to have a large increase in Earth’s ¹⁴C/C ratio during the post-flood Ice Age (Oard, 2021), from about 0.5% of today’s ratio in fossils (Baumgardner, 2005) to more than 95% of today’s ratio by the time of Moses, 1500 B.C. Today cosmic-ray-generated neutrons hitting ¹⁴N nuclei in the atmosphere produce most of the ¹⁴C. With today’s influx of cosmic rays, it would take about 14,000 years to build …

Genealogical Vs Phylogenetic Mutation Rates: Answering A Challenge, Robert Carter

Proceedings of the International Conference on Creationism

There is a discrepancy between the mutation rate we can measure today and the rate at which evolution is supposed to have proceeded. The former is sometimes called the genealogical mutation rate, for it is obtained by comparing individuals whom we know to be related. The latter is sometimes called the phylogenetic mutation rate. It is calculated by counting the fixed differences between two species and dividing by the estimated time since their common ancestor. Genealogical mutation rates are generally several orders of magnitude faster than phylogenetic estimates. This causes problems for the evolutionary model. For example, using the genealogical …

Human Brain Function Above All Other And The Creation Model, James D. Johansen

Proceedings of the International Conference on Creationism

The human brain functions at a level beyond any other brain in all of creation. With mankind being made in the image of God, there must be signatures of this fact in its design. Modeling the human brain that develops an architectural framework offers the potential to unpack this reality. This premise offers a rich area to explore that expands the creation model to capture the engineering framework God used in creation. This paper will focus on brain neurons and neural networks using systems engineering modeling tools.

The systems modeling language (SysML) will be used to capture a model of …

A Rapid Ice Age And Transition To Ice Sheet Growth, Steven M. Gollmer

Proceedings of the International Conference on Creationism

For the past half-century, creationists have explored different explanations for glacial erosion features across the Northern Hemisphere. The best explanation to date is a single post-flood ice age with multiple surges. The challenge with this model is the limited time available between the end of the Flood and the time of Abraham, which appears to be post ice age. Oard (1979) proposed a short post-flood ice age developing due to warm oceans, volcanic aerosols, and barren surfaces. Performing computer climate simulations, Spelman (1996), Vardiman (1998), Gollmer (2013), and Gollmer (2018) verified that enhance precipitation occurs at higher latitudes due to …