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Articles 31 - 39 of 39
Full-Text Articles in Engineering
Novel Design And Synthesis Of Composite Nanomaterials For Lithium And Multivalent Ion Batteries, Wangwang Xu
Novel Design And Synthesis Of Composite Nanomaterials For Lithium And Multivalent Ion Batteries, Wangwang Xu
LSU Doctoral Dissertations
Nowadays, the fast-increasing energy demand for efficient, sustainable and environmentally-friendly energy storage devices remains a significant and challenging issue. Lithium ion batteries (LIBs) have been widely used as commercial energy devices in portable electronics and also shown great promise in upcoming large-scale applications due to their advantages of environmental safety, efficiency in energy delivering and light weight. However, due to their limited capacity, energy densities and cycle ability, LIBs still need further improvement to expand their applications to a larger field, especially electric vehicle (EVs) and hybrid electric vehicles (HEVs), in which energy storage devices with large capacity and high …
Chemically Modified Cellulosic Materials As Multi-Functional Agents In Polymer Composites, Jinlong Zhang
Chemically Modified Cellulosic Materials As Multi-Functional Agents In Polymer Composites, Jinlong Zhang
LSU Doctoral Dissertations
Comparative flame retardancy of micro wood fiber plastic composites (WPCs) with fire retardants (1,2-bis(pentabromophenyl) ethane, metal hydroxides and nanoclay) was studied. The fire additives (1,2-bis(pentabromophenyl) ethane as well as magnesium hydroxide) obviously enhanced the fire retarding properties of WPCs. Especially, 1,2-bis(pentabromophenyl) ethane significantly reduced the total heat release as well as heat release rate. In addition, a synergistic effect of 1,2-bis(pentabromophenyl) and nanoclay was achieved for the enhanced fire retarding performance of WPCs.
A copolymer of cellulose nanocrystals (CNCs) and poly(N-vinylcaprolactam) (PVCL) (PVCL-g-CNCs) for use as thermally-responsive polymers with low critical solution temperatures (LCSTs) was synthesized via atom transfer radical …
Electrocatalytic Properties Of Ni-Fe Basedalloys Toward Oxygen Evolution Reaction, Xiaodan Cui
Electrocatalytic Properties Of Ni-Fe Basedalloys Toward Oxygen Evolution Reaction, Xiaodan Cui
LSU Doctoral Dissertations
In this dissertation, laser-based manufacturing was applied to develop NiFe-based alloys, with focus on their electrochemical characteristics toward oxygen evolution reaction during water electrocatalysis. The targeted electrocatalysts were designed by combining catalysis principles of absorption energy, electronic effect and geometry effect. Firstly, a one-step laser-based manufacturing method was applied to prepare a thin layer of NiFe-based electrodes with varied Ni to Fe ratios to replace high-cost noble metals as the electrocatalyst for oxygen evolution reaction (OER). Since each Ni has 0.6 d-vacancy and each Fe atom has 2.2 d-vacancies. The alloying of Ni-Fe allows electrons flowing from Ni to Fe, …
Radiation Effects In Apatite And High Entropy Alloy Under Energetic Ions And Electrons, Jianren Zhou
Radiation Effects In Apatite And High Entropy Alloy Under Energetic Ions And Electrons, Jianren Zhou
LSU Doctoral Dissertations
Radiation effects in apatite and high entropy alloy under energetic ions and electrons are studied in this doctoral dissertation to develop advanced crystalline ceramic waste forms and nuclear structural materials. Apatite is proposed as a ceramic waste form for the immobilization of radionuclides, but its performance is strongly affected by the irradiation of the incorporated radionuclides. It is thus important to understand the radiation effects in apatite structure and the underlying physics. Effects of chemical composition, grain size, interfacial structure, as well as radiation conditions on the microstructural evolution, phase transformation and damage mechanisms of apatite under alpha-decay and beta-decay …
Microstructural Characterization Of Shear Transformation Zones And Modeling Indentation Size Effect In Amorphous Polymers, Leila Malekmotiei
Microstructural Characterization Of Shear Transformation Zones And Modeling Indentation Size Effect In Amorphous Polymers, Leila Malekmotiei
LSU Doctoral Dissertations
The first aim of this work is developing a procedure for experimental and analytical characterization of nano-scale microstructures which mediate large scale deformation in amorphous polymers. Glassy polymers are extensively used as high impact resistant, low density, and clear materials in industries. Nevertheless, their response under severe loading conditions is yet to be appropriately unraveled. Due to the lack of long-range order in the microstructures of glassy solids, their plastic deformation is different from that in crystalline solids. Shear Transformation Zones (STZs) are believed to be the main plasticity carriers in amorphous solids and defined as the localized atomic or …
Voltage-Controlled Deposition Of Nanoparticles For Next Generation Electronic Materials, Subhodip Maulik
Voltage-Controlled Deposition Of Nanoparticles For Next Generation Electronic Materials, Subhodip Maulik
LSU Doctoral Dissertations
This work presents both a feasibility study and an investigation into the voltage-controlled spray deposition of different nanoparticles, namely, carbon nanotubes (CNTs), as well as molybdenum disulfide (MoS2) and tungsten disulfide (WS2) from the transition metal dichalcogenides (TMDCs) family of materials. The study considers five different types of substrates as per their potential application to next-generation device electronics. The substrates selected for this research were: 1) aluminum as a conducting substrate, 2) silicon as a semiconducting substrate, 3) glass, silicon dioxide (SiO2), and syndiotactic poly methyl methacrylate (syndiotactic PMMA) as insulating substrates.
Since the …
Nanostructured Materials Derived From Metal-Organic Frameworks For Energy And Environmental Applications, Zhiqiang Xie
Nanostructured Materials Derived From Metal-Organic Frameworks For Energy And Environmental Applications, Zhiqiang Xie
LSU Doctoral Dissertations
Nowadays, energy and environmental issues have become the top priority among a series of global issues. Fossil fuels as the dominant source are depleted fast and usually lead to some environmental problems. Heavy metal pollution has posed a severe threat to environment and public health. Metal-organic frameworks (MOFs), as a very promising category of porous materials, have attracted more and more interest in research communities due to their extremely high surface areas, diverse nanostructures and unique properties. To meet the ever-increasing energy demand and tackle the heavy metal pollution in water, MOFs can function as ideal templates to prepare various …
Friction Stir Welding Manufacturing Advancement By On-Line High Temperature Phased Array Ultrasonic Testing And Correlation Of Process Parameters To Joint Quality, Daniel James Huggett
Friction Stir Welding Manufacturing Advancement By On-Line High Temperature Phased Array Ultrasonic Testing And Correlation Of Process Parameters To Joint Quality, Daniel James Huggett
LSU Doctoral Dissertations
Welding, a manufacturing process for joining, is widely employed in aerospace, aeronautical, maritime, nuclear, and automotive industries. Optimizing these techniques are paramount to continue the development of technologically advanced structures and vehicles. In this work, the manufacturing technique of friction stir welding (FSW) with aluminum alloy (AA) 2219-T87 is investigated to improve understanding of the process and advance manufacturing efficiency. AAs are widely employed in aerospace applications due to their notable strength and ductility. The extension of good strength and ductility to cryogenic temperatures make AAs suitable for rocket oxidizer and fuel tankage. AA-2219, a descendent of the original duralumin …
Design And Validation Of Novel Potential High Entropy Alloys, Boliang Zhang
Design And Validation Of Novel Potential High Entropy Alloys, Boliang Zhang
LSU Doctoral Dissertations
The design approach and validation of single phase senary refractory high entropy alloys (HEAs) MoNbTaTiVW and HfNbTaTiVZr were presented in first part of this dissertation. The design approach was to combine phase diagram inspection of available binary and ternary systems and Calculation of Phase Diagrams (CALPHAD) prediction. Experiments using X-ray diffraction and scanning electron microscopy techniques verified single phase microstructure in body centered cubic lattice for both alloys. The observed elemental segregation agrees well with the solidification prediction using Scheil model. The lattice constant, density and microhardness were measured to be 0.3216 nm, 4.954 GPa and 11.70 g/cm3 for …