Engineering Commons^™

Feasibility Study Of Using Energy Extracted From The Process Of Electrochemically Consumed Of Al 2024 For Powering Daily Used Electric Car, Yanuar Mohamad Marda, Rini Riastuti, Muhammad Hamka Ibrahim

Journal of Materials Exploration and Findings

Usage of green energy for transportation has become important due to the contribution of transportation activity to climate change. Electrochemical energy has been used as a source of green energy. The objective of this work is to evaluate sufficiency of energy provided by electrochemically consumed Al 2024 for supplying energy to daily used PHEV electric car. Study of previous articles, observation of typical amount of energy required, electrochemical galvanic cell experiments, and simple calculations have been conducted to determine produced energy feasibility. Electrical energy produced by consuming 340 gr of Al 2024 in galvanic cells has the total lifetime of …

Effect Of Sodium Alcohol Thiyl Propane Sulfonate On Electrolysis Of High Performance Copper Foil For Lithium Ion Batteries, Sen Yang, Wen-Chang Wang, Ran Zhang, Shui-Ping Qin, Min-Xian Wu, Naotoshi Mitsuzaki, Zhi-Dong Chen

Journal of Electrochemistry

Electrolytic copper foils have been widely used in printed circuit boards and lithium-ion batteries due to their simple production process and high economic value. In the process of electrolysis foil making, additives can greatly improve the performance of electrolytic copper foils. In this work, the copper foils were prepared in a self-designed plate electrodeposition device of which the operating principles were in accordance with those of actual industrial production. A series of the Virgin Make-up Solution (VMS: 312.5 g·L-1 CuSO₄·5H₂O, 100 g·L-1 H₂SO₄, 50 mg·L-1 Cl-) containing different additives was investigated to …

Investigation Of Carbon-Based Label-Free Electrochemical Aptasensors For Point-Of-Care Cancer Biomarker Detection, Shahrzad Forouzanfar

FIU Electronic Theses and Dissertations

Cancer is the second cause of death, with millions of fatalities every year. The early detection of cancer can tremendously increase the survival chances of the patients. An effective approach for early detection of cancer is developing reliable and relatively cheap biosensors that can quantify the cancer biomarkers from blood samples. These classes of the biosensor are commonly referred to as point-of-care (POC) cancer biomarker biosensors. The label-free electrochemical biosensors based on carbon dravite materials can be feasible for POC cancer biomarker biosensors. The present dissertation aims to design, develop, and optimize carbon-based biosensors for label-free detection of lactic acid …

Electrochemical Detection Of Neurotransmitters, Saikat Banerjee, Stephanie Mccracken, Md Faruk Hossain, Gymama Slaughter

Bioelectrics Publications

Neurotransmitters are important chemical messengers in the nervous system that play a crucial role in physiological and physical health. Abnormal levels of neurotransmitters have been correlated with physical, psychotic, and neurodegenerative diseases such as Alzheimer's, Parkinson's, dementia, addiction, depression, and schizophrenia. Although multiple neurotechnological approaches have been reported in the literature, the detection and monitoring of neurotransmitters in the brain remains a challenge and continues to garner significant attention. Neurotechnology that provides high-throughput, as well as fast and specific quantification of target analytes in the brain, without negatively impacting the implanted region is highly desired for the monitoring of the …

Two-Dimensional Nanomaterials And Their Composites For Electrochemical Detection Of Toxic Mercury Ions In Water, Md Tawabur Rahman

Electronic Theses and Dissertations

The presence of trace amounts of mercury ion (Hg²⁺) in drinking water has a detrimental effect on human health. The development of an electrochemical sensor for Hg²⁺ detection is still challenging to obtain ultra-trace sensitivity, excellent selectivity, wide Linear Detection Ranges (LDRs), and ultra-low detection limit. This work presents an electrochemical sensor based on two-dimensional nanomaterials and their composites for the enhanced sensing of Hg²⁺ in water. Graphene oxide (GO)-silver nanowires (AgNWs) composite and metallic 1T phase tungsten disulfide (WS2) microflowers were utilized for the fabrication of electrochemical sensors using drop-casting. Under the optimized experimental conditions, …

Portable Electrochemical System For Flexible Hybrid Electronics, Anthony Joseph Hanson

Masters Theses

This work focuses on the fabrication and design of a portable electrochemical sensing system for flexible hybrid electronic (FHE) sensors. A three-electrode chemical sensor was fabricated using copper tape on polyethylene terephthalate (PET) substrate, using laser etching process. An electronic circuit was designed to measure the sensor response through electrochemical techniques to detect different concentrations of glucose. The device was calibrated to give the user a concentration value in 5 seconds. The system was also designed to preform tests such as cyclic voltammogram and chronoamperogram for various chemicals. A Bluetooth Low Energy module was used to wirelessly transmit the results …

Fabrication And Characterization Of Electrochemical Glucose Sensors, Mohammed Marie

Graduate Theses and Dissertations

Electrochemical sensors based on the nanostructure of the semiconductor materials are of tremendous interest to be utilized for glucose monitoring. The sensors, based on the nanostructure of the semiconductor materials, are the third generations of the glucose sensors that are fast, sensitive, and cost-effect for glucose monitoring.

Glucose sensors based on pure zinc oxide nanorods (NRs) grown on different substrates, such ITO, FTO, and Si/SiO2/Au, were investigated in this research. Silicon nanowire (NW)- based glucose sensors were also studied. First, an enzyme-based glucose sensor was fabricated out of glass/ITO/ZnO NRs/BSA/GOx/nafion membrane. The sensor was tested amperometrically at different glucose concentrations. …

Electrochemical Behavior Of Dense Electrodes For Impedancemetric Nox Sensors, Nabamita Pal

Doctoral Dissertations

NOx (NO and NO2) exhaust gas sensors for diesel powered vehicles have traditionally consisted of porous platinum (Pt) electrodes along with a dense ZrO2 based electrolyte. Advancement in diesel engine technology results in lower NOx emissions. Although Pt is chemically and mechanically tolerant to the extreme exhaust gas environment, it is also a strong catalyst for oxygen reduction, which can interfere with the detection of NOx at concentrations below 100 ppm. Countering this behavior can add to the complexity and cost of the conventional NO x sensor design. Recent studies have shown that dense electrodes are less prone to heterogeneous …

Composite Gel Polymer Electrolyte For Lithium Ion Batteries, Roya Naderi

Electronic Theses and Dissertations

Batteries have been ubiquitously utilized in enormous applications such as portable electronics, satellites, computers, medical instruments, and electric cars. The development of battery technology has been through a long journey since the 17th century, paving its way to commercialization of lithium ion batteries in 1991 by Sony. Rechargeable lithium ion batteries represent the most favorable type of batteries for portable applications due to their high energy density compared to other alkali metals. In 1997, lithium polymer batteries with solid polymer/composite electrolyte were introduced where the safety drawbacks of the liquid electrolyte were eliminated but the ionic conductivity of the batteries …

Implementation Of Traditional Printing Techniques For The Development Of Flexible Printed Sensors, Sai Guruva Reddy Avuthu

Dissertations

Printed electronics has gained a remarkable interest over the past decade for the fabrication of cost efficient electronic devices, with a major focus on the development of flexible sensors. This dissertation focuses on the fabrication of flexible sensors using traditional printing processes such as screen, inkjet and gravure printing.

A flexible organic thin film transistor (OTFT) was successfully fabricated on a polyethylene terephthalate (PET) substrate and employed as a humidity sensor. Aluminum gate electrode was thermally evaporated on PET and UV clear dielectric layer was spin coated. Source and drain silver interdigitated electrodes were screen printed. 6,13-bis(triisopropylsilylethynyl) pentacene, a humidity …

Thread Based Battery For Low Power E-Textile Applications, Pranav Laxmanan, Girish Chitnis, Rahim Rahimi, Babak Ziaie

The Summer Undergraduate Research Fellowship (SURF) Symposium

Textile electronic systems, or e-textiles, are on the rise but their utility is limited by its power demand. Potential applications include point-of-care diagnostic systems that would enable medical monitoring at the site of care. A small, inexpensive, and easy to use battery would enhance the capabilities of e-textile. Here we propose a thread based battery that attempts to satisfy these requirements. The thread based battery uses chemistry similar to an alkaline battery. The fabrication process involves patterning of current collector (silver epoxy or carbon ink) followed by zinc electroplating and manganese dioxide deposition. Thread present in between these two electrodes …

Electrochemical Immunosensing Of Cortisol In An Automated Microfluidic System Towards Point-Of-Care Applications, Abhay Vasudev

FIU Electronic Theses and Dissertations

This dissertation describes the development of a label-free, electrochemical immunosensing platform integrated into a low-cost microfluidic system for the sensitive, selective and accurate detection of cortisol, a steroid hormone co-related with many physiological disorders. Abnormal levels of cortisol is indicative of conditions such as Cushing’s syndrome, Addison’s disease, adrenal insufficiencies and more recently post-traumatic stress disorder (PTSD). Electrochemical detection of immuno-complex formation is utilized for the sensitive detection of Cortisol using Anti-Cortisol antibodies immobilized on sensing electrodes. Electrochemical detection techniques such as cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) have been utilized for the characterization and sensing of the …

In-Situ Ellipsometry Characterization Of Anodically Grown Silicon Dioxide And Lithium Intercalation Into Silicon, Eric A. Montgomery

Department of Electrical and Computer Engineering: Dissertations, Theses, and Student Research

In this thesis, in-situ ellipsometry and electroanalytical investigations of two electrochemical processes are reported: including the formation of anodically grown silicon dioxide and the intercalation of lithium into silicon. Analysis of the ellipsometry data shows that the anodically grown silicon dioxide layer is uniform and has similar properties as thermally grown silicon dioxide. The lithium-ion intercalation data reveals non-uniform thin film formation, which requires further studies and development of appropriate ellipsometric optical models.

Advisers: Eva Schubert and Mathias Schubert

Synthesis And Catalytic Property Of Flaked Spindle-Like Cuo Nanocrystals, Jian-Feng Fan, Li-Qing Li, Yu-Feng Huang, Lou-Zhen Fan

Journal of Electrochemistry

A simple and efficient electrochemical route was developed for the synthesis of flaked spindle-like CuO nanocrystals using aqueous electrolyte and Cu sacrificial anode (graphite as the cathode) in an undivided cell at a constant potential mode under room temperature. The morphologies, structure and component of CuO nanocrystals obtained were characterized by SEM, XRD, respectively. Flaked spindle-like CuO nanocrystals were successfully used to modify a GC electrode to detect H2O2 with cyclic voltammetry (CV) and amperometric (AC).The results showed that products were pure monoclinic CuO nanocrystals. The linear range for the determination of hydrogen peroxide is from 1.0 μmol?L-1 to 1.0 …