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Construction Of An Initiated Chemical Vapor Deposition (Icvd) Reactor And Deposition Of Polytetrafluoroethylene (Ptfe) Thin Films Using Perfluoro-1-Octanesulfonyl Fluoride As The Initiator, Edgar Kiprop Kosgey
Construction Of An Initiated Chemical Vapor Deposition (Icvd) Reactor And Deposition Of Polytetrafluoroethylene (Ptfe) Thin Films Using Perfluoro-1-Octanesulfonyl Fluoride As The Initiator, Edgar Kiprop Kosgey
MSU Graduate Theses
Initiated Chemical Vapor Deposition (iCVD) is a surface polymerization technique that is different from other traditional chemical vapor deposition (CVD) techniques. iCVD is carried under a vacuum without the use of solvents, therefore eliminating contaminations. An initiator and a monomer are metered into a vacuum reactor chamber. Inside the reaction chamber is an array of resistively heated filaments and a cooled substrate stage. Monomer species adsorb on to the cooled substrate surface underneath the filament array. The thermal energy from the resistively heated filaments breaks the bonds in the initiator molecule, generating free radicals. These generated free radicals chemisorb to …
Design Of High Temperature Evaporator For Spectroscopic Study Of Equilibrated Vapor Phase Materials, Yarden Bosch
Design Of High Temperature Evaporator For Spectroscopic Study Of Equilibrated Vapor Phase Materials, Yarden Bosch
MSU Graduate Theses
This work details the design, assembly, and testing of a high temperature electron beam evaporator for equilibrated vapor phase evaporation of rock oxides for the purpose of astrophysical characterization of extrasolar planetary atmospheres. Infrared spectroscopy of high temperature SiO2 atmosphere created through the electron beam evaporation technique and trapped by argon ice matrix isolation was performed to generate a reference spectrum against which absorption lines in stellar spectra taken during planetary transits can be compared. Studies demonstrate that water inclusions in milky quartz (SiO2) can be used to create H2O/SiO2 equilibrated atmospheres within a Knudsen cell. Modeling of exoplanet spectra …
Investigation Of Electrical And Magneto Transport Properties Of Reduced Graphene Oxide Thin Films, Ariful Haque
Investigation Of Electrical And Magneto Transport Properties Of Reduced Graphene Oxide Thin Films, Ariful Haque
MSU Graduate Theses
Large area uniform thin films of reduced graphene oxide (RGO) was synthesized by pulsed laser deposition (PLD) technique. A number of structural properties including the defect density, average size of sp2 clusters, and degree of reduction were investigated by Raman spectroscopy and X-ray diffraction (XRD) analysis. The temperature dependent (5K - 350K) four terminal electrical transport property measurement confirms variable range hopping and thermally activated transport mechanism of the charge carriers at low (5K - 210K) and high temperature (210K - 350K) regions, respectively. The calculated localization length, density of states (DOS) near Fermi level (EF), hopping energy, and Arrhenius …
Investigation Of Lanthanide-Doped Anatase Tio2 Core-Shell Nanoparticles For Photocatalysis And Gas Sensing, Rezwanur Rahman
Investigation Of Lanthanide-Doped Anatase Tio2 Core-Shell Nanoparticles For Photocatalysis And Gas Sensing, Rezwanur Rahman
MSU Graduate Theses
Anatase TiO2 has been shown to be potential applications for photo-remediation of chemical waste as well as for photocatalytic splitting of water. The catalytic properties of TiO2 materials can be modified by doping with lanthanide (Ln) ions. In order to minimize the distortion and/or change of the structure of TiO2 nanoparticles, surface doping of anatase TiO2 nanoparticles (~ 14 nm) with several Ln ions (Nd3+, Gd3+, Eu3+, Yb3+) has been successfully made. X-ray diffraction (XRD) and Raman characterization shows that the anatase phase of treated nanoparticles is well preserved. Scanning electron microscopy (SEM) shows that the majority of the nanoparticles …