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Direct Determination Of Pentachlorophenol By Differential Pulse Polarography, Albert L. Wade
Direct Determination Of Pentachlorophenol By Differential Pulse Polarography, Albert L. Wade
Theses and Dissertations
Concern over environmental contamination leading to the introduction of pentachlorophenol into human and animal systems has resulted in the need for a rapid and direct method for determining trace concentrations of this highly toxic compound. A direct electrochemical procedure has been developed for determining trace conccentrations of this phenol dovm to 0.27 ppm. This method uses the electrochemical techniques of differential pulse polarography at the dropping mercury electrode, and differential pulse voltammetry at the carbon paste electrode to reduce pentachlorophenol for this determination. Cyclic voltammetry at the hanging mercury drop electrode has been used to characterize the reaction behavior of …