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Enantioseparation Of Alkylaryl Sulfoxides Using Capillary Zone Electrophoresis, Chad Snyder
Enantioseparation Of Alkylaryl Sulfoxides Using Capillary Zone Electrophoresis, Chad Snyder
Masters Theses & Specialist Projects
Alkylaryl sulfoxides possess a chiral sulfur atom easily identifiable by capillary zone electrophoresis (CZE). Separation of chiral alkylaryl sulfoxides has already been accomplished by modified method of CZE known as micellar electrokinetic chromatography (MEKC). However, no articles have been published on the enantioseparation of alkylaryl sulfoxides using capillary zone electrophoresis.
A series of sulfoxides were synthesized, purified and identified via NMR. Enantioseparation was performed using CZE employing a 10 mmol. Phosphate buffer (pH 4.0, 25% acetonitrile, 2% sulfated-β-cyclodextrin). Synthesis of these sulfoxides will be presented along with the results of the procedure’s optimization. Separation of the sulfoxide enanitomers relies on …
Ua56/1 Facts At A Glance, Wku Institutional Research
Ua56/1 Facts At A Glance, Wku Institutional Research
WKU Archives Records
Statistical and demographic profile of WKU.
Ua56/1 Fact Book, Wku Institutional Research
Ua56/1 Fact Book, Wku Institutional Research
WKU Archives Records
Statistical and demographic profile of WKU.