Physical Sciences and Mathematics Commons^™

Developing And Validating A Standard Operating Procedure For Quantitative Analysis Using Central Washington University's X-Ray Diffractometer, Katherine Lucas

Undergraduate Honors Theses

X-ray diffraction (XRD) is widely applied in a variety of disciplines to identify crystalline solids in a powdered sample. Recent software advances have made quantitative analysis of samples easier and more accessible, but the quality of the result depends on the sample preparation and data collection procedure. This project focuses on testing methods of sample preparation and XRD data collection and analysis to lay the groundwork for refinement of the existing standard operating procedures at CWU. First, I determined the ball mill grinding time necessary to powder different mineral samples. The addition of hand grinding to ball mill-ground samples produced …