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Physical Sciences and Mathematics Commons™
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Articles 1 - 3 of 3
Full-Text Articles in Physical Sciences and Mathematics
A Large-Scale Synthesis And Characterization Of Quaternary CuinXGa1−XS2 Chalcopyrite Nanoparticles Via Microwave Batch Reactions, Chivin Sun, Richard D. Westover, Gary Long, Cyril Bajracharya, Jerry D. Harris, Alex Punnoose, Rene G. Rodriguez, Joshua J. Pak
A Large-Scale Synthesis And Characterization Of Quaternary CuinXGa1−XS2 Chalcopyrite Nanoparticles Via Microwave Batch Reactions, Chivin Sun, Richard D. Westover, Gary Long, Cyril Bajracharya, Jerry D. Harris, Alex Punnoose, Rene G. Rodriguez, Joshua J. Pak
Physics Faculty Publications and Presentations
Various quaternary CuInxGa1−xS2 (0 ≤ x ≤ 1) chalcopyrite nanoparticles have been prepared from molecular single-source precursors via microwave decomposition. We were able to control the nanoparticle size, phase, stoichiometry, and solubility. Depending on the choice of surface modifiers used, we were able to tune the solubility of the resulting nanoparticles. This method has been used to generate up to 5 g of nanoparticles and up to 150 g from multiple batch reactions with excellent reproducibility. Data from UV-Vis, photoluminescence, X-ray diffraction, TEM, DSC/TGA-MS, and ICP-OES analyses have shown high reproducibility in nanoparticle size, …
Simultaneous Measurement Of Normal And Friction Forces Using A Cantilever-Based Optical Interfacial Force Microscope, Byung I. Kim, Jeremy R. Bonander, Jared A. Rasmussen
Simultaneous Measurement Of Normal And Friction Forces Using A Cantilever-Based Optical Interfacial Force Microscope, Byung I. Kim, Jeremy R. Bonander, Jared A. Rasmussen
Physics Faculty Publications and Presentations
We measured normal and friction forces simultaneously using a recently developed cantilever-based optical interfacial force microscope (COIFM) technique for studies of interfacial structures and mechanical properties of nanoscale materials. We derived how the forces can be incorporated into the detection signal using the classical Euler equation for beams. A lateral modulation with the amplitude of one nanometers was applied to create the friction forces between tip and sample. We demonstrated its capability by measuring normal and friction forces of interfacial water at the molecular scale over all distance ranges.
Magnetism Of Zno Nanoparticles: Dependence On Crystallite Size And Surfactant Coating, Aaron P. Thurber, Geoffrey L. Beausoleil Ii, Gordon A. Alanko, Joshua Anghel, Michael S. Jones, Lydia M. Johnson, Jianhui Zhang, Charles B. Hanna, Dmitri A. Tenne, Alex Punnoose
Magnetism Of Zno Nanoparticles: Dependence On Crystallite Size And Surfactant Coating, Aaron P. Thurber, Geoffrey L. Beausoleil Ii, Gordon A. Alanko, Joshua Anghel, Michael S. Jones, Lydia M. Johnson, Jianhui Zhang, Charles B. Hanna, Dmitri A. Tenne, Alex Punnoose
Physics Faculty Publications and Presentations
Many recent reports on magnetism in otherwise nonmagnetic oxides have demonstrated that nanoparticle size, surfactant coating, or doping with magnetic ions produces room-temperature ferromagnetism. Specifically, ZnO has been argued to be a room-temperature ferromagnet through all three of these methods in various experimental studies. For this reason, we have prepared a series of 1% Fe doped ZnO nanoparticle samples using a single forced hydrolysis co-precipitation synthesis method from the same precursors, while varying size (6 – 15 nm) and surface coating concentration to study the combined effects of these two parameters. Size was controlled by modifying the water concentration. Surfactant …