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Potential Effects Of Chemical Contamination On South Florida Bonefish Albula Vulpes, Christine P. Beck
Potential Effects Of Chemical Contamination On South Florida Bonefish Albula Vulpes, Christine P. Beck
FIU Electronic Theses and Dissertations
An ecological risk assessment was conducted on the risk to fish of chemical contaminants detected in the habitat of Albula vulpes in South Florida, to evaluate whether contaminants may be a driver of declines in the recreational bonefish fishery. All available contaminant detection data from Biscayne Bay, Florida Bay, and the Florida Keys were compared to federal and state guidelines for aquatic health to identify Contaminants of Potential Ecological Concern (COPECS). For these COPECs, species sensitivity distributions were constructed and compared with recent detections at the 90th centile of exposure. Copper in Biscayne Bay was identified as the highest …
Assessment Of The Occurrence And Potential Risks Of Antibiotics And Their Metabolites In South Florida Waters Using Liquid Chromatography Tandem Mass Spectrometry, Venkata Reddy Panditi
Assessment Of The Occurrence And Potential Risks Of Antibiotics And Their Metabolites In South Florida Waters Using Liquid Chromatography Tandem Mass Spectrometry, Venkata Reddy Panditi
FIU Electronic Theses and Dissertations
An automated on-line SPE-LC-MS/MS method was developed for the quantitation of multiple classes of antibiotics in environmental waters. High sensitivity in the low ng/L range was accomplished by using large volume injections with 10-mL of sample. Positive confirmation of analytes was achieved using two selected reaction monitoring (SRM) transitions per antibiotic and quantitation was performed using an internal standard approach. Samples were extracted using online solid phase extraction, then using column switching technique; extracted samples were immediately passed through liquid chromatography and analyzed by tandem mass spectrometry. The total run time per each sample was 20 min. The statistically calculated …