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Full-Text Articles in Physical Sciences and Mathematics
Optimizing Electrospun Ceramic Nanofiber Strength Through Two-Step Sintering, Michael Ross
Optimizing Electrospun Ceramic Nanofiber Strength Through Two-Step Sintering, Michael Ross
Materials Engineering
Two-step sintering (TSS) consists of a high-temperature step and immediate cooling to a sintering temperature for an extended sintering time, where grain growth is suppressed by severe densification during the high-temperature step. TSS is adopted to enhance mechanical properties of electrospun ceramic nanofibers (CNFs), a class of porous ceramics used for environmental remediation, optoelectronics, and filtration. PVP and Ga(NO3)3 nanofiber mesh, provided by Lawrence Livermore National Laboratory, was shaped, oxidized, and two-step sintered to form a nanocrystalline β-Ga2O3 CNF tube using a high-temperature step of 1,000oC. Sintering temperatures and times varied from …
Nano Fab Lab 63, Brian K. Deemer, Josh Clemons, Nick Brodine, Delaney Fitzsimmons
Nano Fab Lab 63, Brian K. Deemer, Josh Clemons, Nick Brodine, Delaney Fitzsimmons
Mechanical Engineering
Lawrence Livermore National Laboratories (LLNL) has several steps in the production process for ceramic nanofiber tubes that they would like to improve - electrospinning, cutting, rolling, sealing and heat treating. We undertook the challenge to deliver LLNL with a semi-automated process that efficiently integrates the steps of cutting, rolling, and sealing to save time and improve control over end dimensions. In this document, we discuss the technical background of the manufacturing steps currently followed to create nanofiber tubes, identify which steps are incorporated in our prototype and explain how they will interface with one another, define the design requirements, present …