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Physical Sciences and Mathematics Commons

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Analytical Chemistry

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Full-Text Articles in Physical Sciences and Mathematics

Quantification Of Vitamin B12 In Two Cricket Species, Haley Smeltz Apr 2020

Quantification Of Vitamin B12 In Two Cricket Species, Haley Smeltz

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Entomophagy, or the eating of insects, has been practiced in the eastern world for centuries, however it is currently overlooked in the western nations. Studies have shown that insects, such as crickets, contain high levels of protein and minerals, however vitamin content is rarely studied. This study aims to quantify the vitamin B12 content in two cricket species, the common house cricket (Acheta domesticus) and the banded cricket (Gryllodes sigillatus). The vitamin B12 content of both cricket species will be quantified using reverse-phase high performance liquid chromatography (RP-HPLC). Prior to RP-HPLC analysis, all the …


Quantitative Analysis Of Iron In Beer Using Cloud Point Extraction, Joshua Rempfer Apr 2019

Quantitative Analysis Of Iron In Beer Using Cloud Point Extraction, Joshua Rempfer

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Determination of Iron concentration in Apocalypse Ale beer using a preconcentration method coupled with UV-Vis spectroscopy. Samples will be cross checked with MP-AES to ensure precise and accurate results.


Elemental Analysis Of Legacy Sediments At College Lake, Amelia Dalton Apr 2019

Elemental Analysis Of Legacy Sediments At College Lake, Amelia Dalton

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College Lake is a large reservoir located on the campus of the University of Lynchburg. College Lake’s ecosystem has degraded over the years due to the buildup of sediment, nutrients, and raw sewage. Increased urbanization in the area has also most likely contributed to the contaminants present within the system. Because of flooding issues during the summer of 2018, Lynchburg CIty officials drained College Lake, which caused sediment to be released downstream. To better understand the transport of heavy metals in the sediments released from College Lake, sediment core samples were taken from College Lake, Hollins Mill Park, and Sandusky …


Mobilization Of Calcium Across Mineralized Tissues In Yellow Perch, Perca Flavescens, Taylor Bopp Apr 2019

Mobilization Of Calcium Across Mineralized Tissues In Yellow Perch, Perca Flavescens, Taylor Bopp

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Bones in many higher teleost fish, such as percids and centrarchids, lack osteocytes that function as both chemo- and mechano-sensors, and thus, are not actively involved in homeostasis of blood calcium level. Nonetheless, the vertebrae of yellow perch, Perca flavescens (P. flavescens), living in darker and low calcium (Ca) water, have demonstrated adaptive modeling and remodeling of vertebrae to be more mineralized and thus enhance transmission of the axial muscle torque into the thrust force for the C-start predator escape behavior. The prey-predator interaction is expected to occur at closer range between prey fish and predator fish in …


A Chemical In Filter Paper Interferes With Trail Following Behavior In The Termite Reticulitermes Hesperus (Banks), Kathryn Vest Apr 2019

A Chemical In Filter Paper Interferes With Trail Following Behavior In The Termite Reticulitermes Hesperus (Banks), Kathryn Vest

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Termites follow chemical trails. In previous experiments we dissolved and diluted chemicals in acetone to test if they elicited trail following. Each trail was a straight line across the arena drawn with 10 µl using a glass capillary (Microcaps). We noticed a minor but stable response to trails laid with pure acetone. The response could be caused by contaminated acetone or by a chemical in the filter paper (Watman #5) that lined our arena (petri dish, 10cm diameter). We could confirm that the termites respond to acetone alone. Soxkhlet extraction for 8 hours removed the signal from the filter paper. …


Eating Crickets? Nutrient Mineral Content Of Two Cricket Species And Chapul Cricket Protein Bars Using Mp-Aes, Nathan Hopkins Apr 2018

Eating Crickets? Nutrient Mineral Content Of Two Cricket Species And Chapul Cricket Protein Bars Using Mp-Aes, Nathan Hopkins

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Global agriculture is beset by numerous challenges which must be surmounted to feed a developing world, from combating climate change to the cultivation of sustainable food products. This, in addition to protein and nutrient deficiencies in the developing world, makes considering alternative protein sources, such as a crickets, an attractive option. Crickets use a fraction of the land and water that protein sources like beef cattle do, and can be cultivated in urban environments in stacked boxes. This research investigation aims to quantify the nutrient mineral content (Iron, Sodium, Potassium, Calcium, and Magnesium) of two cricket species (Acheta domesticus …


Spectrofluorometric Analysis Of Bisphenol-A In Drinking Water Bottles, Jeff Brochetti Apr 2017

Spectrofluorometric Analysis Of Bisphenol-A In Drinking Water Bottles, Jeff Brochetti

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Spectrofluorometric Analysis of Bisphenol-A in Drinking Water Bottles

Bisphenol-A (BPA) is of environmental concern due to its ability to act as an endocrine disruptor in humans and many other animals. In the food industry, BPA is widely used in the production of plastic bottles and plastic liners in aluminum cans. Over time, trace amounts of BPA can leach from the container and into the contents inside. A new method of testing for trace amount of BPA involved the formation of an inclusion complex with ß-Cyclodextrin. With the formation of the inclusion complex, it becomes much easier to analyze low concentrations …