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Theses/Dissertations

2006

Chemical Engineering

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Investigation Of Flow And Microstructure In Rheometric And Processing Flow Conditions For Liquid Crystalline Pitch, Santanu Kundu Dec 2006

Investigation Of Flow And Microstructure In Rheometric And Processing Flow Conditions For Liquid Crystalline Pitch, Santanu Kundu

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A fundamental understanding of flow and its influence on the microstructure is required to obtain carbon materials with desired properties. The objective of this research was to investigate the flow and microstructural behavior of a synthetic mesophase pitch (AR-HP) in rheometric and processing flow conditions. In addition, simulation studies were performed to establish a frame work for modeling the flow behavior of this complex material in different flow situations.
The steady-shear viscosities obtained from a cone-plate rheometer during increasing rate-sweep experiments exhibited a shear-thinning region (Region I) with a slope of about -0.2 and a plateau (Region II) region. The …