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Kinetics Determination Of Soybean Oil Transesterification In The Design Of A Continuous Biodiesel Production Process, Irwin Jacob, Ed Clausen, Danielle Julie Carrier
Kinetics Determination Of Soybean Oil Transesterification In The Design Of A Continuous Biodiesel Production Process, Irwin Jacob, Ed Clausen, Danielle Julie Carrier
Biological and Agricultural Engineering Undergraduate Honors Theses
One-step batch transesterification consisting of three stepwise reversible reactions of pure soybean oil with methanol was conducted at two different mixing speeds (600 and 300 rpm) to produce soybean oil fatty acid methyl esters (biodiesel). In both batch reactions, sodium methoxide (1.09 wt% based on soybean oil) was used as the catalyst, the reaction temperature was 60oC, and the methanol-to-oil molar ratio was 6:1. The objectives were to determine and/or investigate: 1) the mechanism and order of the reaction, 2) the reaction rate constants, 3) the effect of changes in mixing intensity on the reaction rate, 4) the comparison of …
A Study Of Inhomogeneity Effects On Packed High Performance Liquid Chromatography Columns, Tyler House
A Study Of Inhomogeneity Effects On Packed High Performance Liquid Chromatography Columns, Tyler House
Chemical Engineering Undergraduate Honors Theses
The packing quality of a High Performance Liquid Chromatography column has significant impact on the resulting separations. In practice, problems in a packing occur through normal usage of a column. Resulting chromatograms from inhomogeneities exhibit varying problems such as extreme tailing and double peaks. Early detection of such problems is critical to fixing problems before their effect harms efficiency, but a fully developed theory of how inhomogeneities affect separations does not exist. The purpose of this work was to experimentally characterize HPLC column inhomogeneities and to begin preliminary simulations of HPLC columns with the computer simulation package STAR-CD. To do …