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Effect Of Anisotropic Elasticity On Dislocation Pile-Ups At Grain Boundaries, Xiaolei Chen, Stéphane Berbenni, Christian Motz, Thiebaud Richeton

Nanomechanical Testing in Materials Research and Development VII

This study deals with in-situ micromechanical tests of micron-sized bi-crystals and observations coupling SEM, AFM and EBSD. Different FCC bi-crystals are obtained from FIB machining. A SEM in-situ compression test with a low strain is performed on a micron-sized bi-crystal in order to induce single slip deformation. Spatial variations in the surface step height due to dislocation activity in localized slip bands terminating at the grain boundary (GB) are measured by AFM. This allows the determination of the Burgers vector distribution and hence the dislocation positions in the pile-up as shown in Figure 1. Furthermore, local misorientation along slip bands …