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Nitrogen Doped Carbon Nanofibers Derived From Water-Soluble Precursors, Lee Cremar, Ben Jones, Nicole Martinez, Gustavo Mejia, Hilario Cortez, Edgar Muñoz, Rocío Nava, Karen Lozano

Mechanical Engineering Faculty Publications and Presentations

Nitrogen doped carbon fibers were synthesized from polyvinyl alcohol (PVA), a water soluble precursor. The PVA fine fibers were first developed by centrifugally spinning an aqueous based solution using Forcespinning® technology. The precursor fibers were then exposed to sulfuric acid vapors to partially carbonize and stabilize the fibers for further heat treatment. For nitrogen doping, the fibers were exposed to two different heat treatment routes. One was under a nitrogen atmosphere at 850°C followed by exposure to ammonia gas at 500°C. The second route consisted of heating the treated fibers in pure ammonia gas only, up to 850°C. Both heating …